Microstructure Development in Electron Beam-Melted Inconel 718 and Associated Tensile Properties

During the electron beam melting (EBM) process, builds occur at temperatures in excess of 800°C for nickel-base superalloys such as Inconel 718. When coupled with the temporal differences between the start and end of a build, a top-to-bottom microstructure gradient forms. Characterized in this study is a microstructure gradient and associated tensile property gradient common to all EBM Inconel 718 builds, the extent of which is dependent on build geometry and the specifics of a build’s processing history. From the characteristic microstructure elements observed in EBM Inconel 718 material, the microstructure gradient can be classified into three distinct regions. Region 1 (top of a build) is comprised of a cored dendritic structure that includes carbides and Laves phase within the interdendritic regions. Region 2 is an intermediate transition zone characterized by a diffuse dendritic structure, dissolution of the Laves phase, and precipitation of $$\delta $$δ needle networks within the interdendritic regions. The bulk structure (Region 3) is comprised of a columnar grain structure lacking dendritic characteristics with $$\delta $$δ networks having precipitated within the grain interiors. Mechanically, at both 20°C and 650°C, the yield strength, ultimate tensile strength, and elongation at failure exhibit the general trend of increasing with increasing build height.

[1]  Jay Patel,et al.  Additive manufacturing , 2016, XRDS.

[2]  D. S. Sarma,et al.  Effect of solution treatment temperature on microstructure and mechanical properties of hot isostatically pressed superalloy Inconel* 718 , 2004 .

[3]  S. David,et al.  Characterization of the microstructure evolution in a nickel base superalloy during continuous cooling conditions , 2001 .

[4]  Liu Wei,et al.  Delta phase precipitation in Inconel 718 , 2004 .

[5]  Yixiong Wu,et al.  Effect of Cooling Rate on the Microstructure of Laser-Remelted INCONEL 718 Coating , 2013, Metallurgical and Materials Transactions A.

[6]  W. Kurz,et al.  SINGLE-CRYSTAL LASER DEPOSITION OF SUPERALLOYS: PROCESSING-MICROSTRUCTURE MAPS , 2001 .

[7]  Ryan B. Wicker,et al.  Microstructures of Rene 142 nickel-based superalloy fabricated by electron beam melting , 2013 .

[8]  D. Korzekwa,et al.  Truchas – a multi-physics tool for casting simulation , 2009 .

[9]  J. Tien,et al.  Superalloys, supercomposites and superceramics , 1989 .

[10]  Ryan R. Dehoff,et al.  Thermal effects on microstructural heterogeneity of Inconel 718 materials fabricated by electron beam melting , 2014 .

[11]  Y. Han,et al.  AN INVESTIGATION OF THE HOMOGENIZATION AND DEFORMATION OF ALLOY 718 INGOTS , 1994 .

[12]  Honghua Zhang,et al.  Deformation characteristics of δ phase in the delta-processed Inconel 718 alloy , 2010 .

[13]  L. Murr,et al.  Microstructural Architecture, Microstructures, and Mechanical Properties for a Nickel-Base Superalloy Fabricated by Electron Beam Melting , 2011 .

[14]  R. Field,et al.  The Effects of Long Time Exposure on Alloy 718 , 1994 .

[15]  M. Sundararaman,et al.  Overlapping of γ′ precipitate variants in Inconel 718 , 1993 .

[16]  Robert F. Singer,et al.  Additive manufacturing of nickel-based superalloy Inconel 718 by selective electron beam melting: Processing window and microstructure , 2014 .

[17]  Ming Gao,et al.  The microstructure and mechanical properties of deposited-IN718 by selective laser melting , 2012 .

[18]  W. Cao,et al.  Differential Thermal Analysis (DTA) Study of the Homogenization Process in Alloy 718 , 1991 .

[19]  M. Chaturvedi,et al.  Strengthening mechanisms in Inconel 718 superalloy , 1983 .

[20]  L. Murr,et al.  Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting , 2012 .

[21]  Wilfried Kurz,et al.  Theory of Microstructural Development during Rapid Solidification , 1986 .

[22]  R. Fischer,et al.  Investigations of MX and γ′/γ″ precipitates in the nickel-based superalloy 718 produced by electron beam melting , 2008 .

[23]  S. Suresh Babu,et al.  Rationalization of Microstructure Heterogeneity in INCONEL 718 Builds Made by the Direct Laser Additive Manufacturing Process , 2014, Metallurgical and Materials Transactions A.

[24]  Moataz M. Attallah,et al.  Laser Powder Bed Fabrication of Nickel‐Base Superalloys: Influence of Parameters; Characterisation, Quantification and Mitigation of Cracking , 2012 .

[25]  S. David,et al.  Welding: Solidification and microstructure , 2003 .

[26]  Srikumar Banerjee,et al.  Precipitation of the δ-Ni3Nb phase in two nickel base superalloys , 1988 .

[27]  A. Argon,et al.  Strengthening Mechanisms in Crystal Plasticity , 2007 .

[28]  J. Hunt,et al.  Steady state columnar and equiaxed growth of dendrites and eutectic , 1984 .

[29]  David W. Rosen,et al.  Additive Manufacturing Technologies: Rapid Prototyping to Direct Digital Manufacturing , 2009 .

[30]  R. Thompson Microfissuring of Alloy 718 in the Weld Heat-Affected Zone , 1988 .

[31]  A. Pineau,et al.  Gamma double prime precipitation kinetic in Alloy 718 , 2008 .