Detecting Pork Adulteration in Beef for Halal Authentication Using an Optimized Electronic Nose System

Recently, the issue of food authentication has gained attention, especially halal authentication, because of cases of pork adulteration in beef. Many studies have developed rapid detection for adulterated meat. However, these studies are not yet practical and economical methods and instruments and a faster analysis process. In this context, this paper proposes the Optimized Electronic Nose System (OENS) for more accurately detecting pork adulteration in beef. OENS has advantages such as proper noise filtering, an optimized sensor array, and optimized support vector machine (SVM) parameters. Noise filtering is carried out by cross-validation with different mother wavelets, i.e., Haar, dmey, coiflet, symlet, and Daubechies. The sensor array was optimized by dimension reduction using principal component analysis (PCA). An algorithm is proposed for the optimization of the SVM parameters. An experiment was conducted by analyzing seven classes of meat, comprising seven different mixtures of beef and pork. The first and seventh classes were 100% beef and 100% pork, respectively, while the second, third, fourth, fifth, and sixth classes contained 10%, 25%, 50%, 75%, and 90% of beef in a sample of 100 grams, respectively. Sample testing was carried out for 15 minutes for each sample. The classification test results to detect beef and pork had an accuracy of 98.10% using the optimized support vector machine. Thus, OENS has a favorable performance to detect pork adulteration in beef for halal authentication.

[1]  Chastine Fatichah,et al.  Electronic nose dataset for pork adulteration in beef , 2020, Data in brief.

[2]  Riyanarto Sarno,et al.  Music mood classification using audio power and audio harmonicity based on MPEG-7 audio features and Support Vector Machine , 2017, 2017 3rd International Conference on Science in Information Technology (ICSITech).

[3]  Siti Anom Ahmad,et al.  Selection of Mother Wavelet Functions for Multi-Channel EEG Signal Analysis during a Working Memory Task , 2015, Sensors.

[4]  Riyanarto Sarno,et al.  Music fingerprinting based on bhattacharya distance for song and cover song recognition , 2019 .

[5]  Riyanarto Sarno,et al.  Estimating Gas Concentration using Artificial Neural Network for Electronic Nose , 2017 .

[6]  Riyanarto Sarno,et al.  Electronic nose for classifying beef and pork using Naïve Bayes , 2017, 2017 International Seminar on Sensors, Instrumentation, Measurement and Metrology (ISSIMM).

[7]  M. Mannaa Halal food in the tourist destination and its importance for Muslim travellers , 2020, Current Issues in Tourism.

[8]  Min Zhang,et al.  Advances of electronic nose and its application in fresh foods: A review , 2018, Critical reviews in food science and nutrition.

[9]  Riyanarto Sarno,et al.  Gas concentration analysis of resistive gas sensor array , 2016, 2016 International Symposium on Electronics and Smart Devices (ISESD).

[10]  Riyanarto Sarno,et al.  DWTLSTM for electronic nose signal processing in beef quality monitoring , 2021 .

[11]  G. McVean A Genealogical Interpretation of Principal Components Analysis , 2009, PLoS genetics.

[12]  Noor Faizah Mohd-Naim,et al.  From market to food plate: Current trusted technology and innovations in halal food analysis , 2016 .

[13]  Riyanarto Sarno,et al.  Sensor Array Optimization for Mobile Electronic Nose: Wavelet Transform and Filter Based Feature Selection Approach , 2016 .

[14]  Yukyung Choi,et al.  Identification of Pork Adulteration in Processed Meat Products Using the Developed Mitochondrial DNA-Based Primers , 2017, Korean journal for food science of animal resources.

[15]  Wei Chen,et al.  Rapid visual sensing and quantitative identification of duck meat in adulterated beef with a lateral flow strip platform. , 2019, Food chemistry.

[16]  Riyanarto Sarno,et al.  Optimizing Threshold using Pearson Correlation for Selecting Features of Electronic Nose Signals , 2019 .

[17]  Jan Mei Soon,et al.  Halal integrity in the food supply chain , 2017 .

[18]  K. Dejhan,et al.  Mother wavelet selecting method for selective mapping technique ECG compression , 2012, 2012 9th International Conference on Electrical Engineering/Electronics, Computer, Telecommunications and Information Technology.

[19]  Andrea Versari,et al.  Progress in authentication, typification and traceability of grapes and wines by chemometric approaches , 2014 .

[20]  A. Guntarti,et al.  Identification of lard on grilled beef sausage product and steamed beef sausage product using fourier transform infrared (FTIR) spectroscopy with chemometric combination , 2019, Potravinarstvo Slovak Journal of Food Sciences.

[21]  Dedy Rahman Wijaya,et al.  Stability Assessment of Feature Selection Algorithms on Homogeneous Datasets: A Study for Sensor Array Optimization Problem , 2020, IEEE Access.

[22]  Bambang Kuswandi,et al.  Immuno strip test for detection of pork adulteration in cooked meatballs , 2017 .

[23]  Riyanarto Sarno,et al.  Electronic nose dataset for beef quality monitoring in uncontrolled ambient conditions , 2018, Data in brief.

[24]  Vladimir N. Vapnik,et al.  The Nature of Statistical Learning Theory , 2000, Statistics for Engineering and Information Science.

[25]  M. Aaslyng,et al.  Assessment of meat quality by NMR—an investigation of pork products originating from different breeds , 2011, Magnetic resonance in chemistry : MRC.

[26]  Havva Tümay Temiz,et al.  A novel method for discrimination of beef and horsemeat using Raman spectroscopy. , 2014, Food chemistry.

[27]  Riyanarto Sarno,et al.  Noise filtering framework for electronic nose signals: An application for beef quality monitoring , 2019, Comput. Electron. Agric..

[28]  Dedy Rahman Wijaya,et al.  Information-Theoretic Ensemble Feature Selection With Multi-Stage Aggregation for Sensor Array Optimization , 2021, IEEE Sensors Journal.

[29]  George-John E. Nychas,et al.  Contribution of Fourier transform infrared (FTIR) spectroscopy data on the quantitative determination of minced pork meat spoilage , 2011 .

[30]  Federica Camin,et al.  Food authentication: Techniques, trends & emerging approaches , 2016 .

[31]  Jun Wang,et al.  Comparison of spectral clustering, K-clustering and hierarchical clustering on e-nose datasets: Application to the recognition of material freshness, adulteration levels and pretreatment approaches for tomato juices , 2014 .

[32]  R. Sarno,et al.  Development of wavelet transforms to predict methane in chili using the electronic nose , 2017, 2017 International Conference on Advanced Mechatronics, Intelligent Manufacture, and Industrial Automation (ICAMIMIA).

[33]  M. Hartmann,et al.  Quantitative targeted GC-MS-based urinary steroid metabolome analysis for treatment monitoring of adolescents and young adults with autoimmune primary adrenal insufficiency , 2019, Steroids.

[34]  Shaoqing Cui,et al.  Analysis of pork adulteration in minced mutton using electronic nose of metal oxide sensors , 2013 .

[35]  Filippo Attivissimo,et al.  A comparative study on mother wavelet selection in ultrasound image denoising , 2013 .

[36]  Riyanarto Sarno,et al.  Classification of Music Mood Using MPEG-7 Audio Features and SVM with Confidence Interval , 2018, Int. J. Artif. Intell. Tools.

[37]  Aaron O'Leary,et al.  PyWavelets: A Python package for wavelet analysis , 2019, J. Open Source Softw..

[38]  Riyanarto Sarno,et al.  Recent development in electronic nose data processing for beef quality assessment , 2019 .

[39]  Kenshi Hayashi,et al.  Deep learning in a sensor array system based on the distribution of volatile compounds from meat cuts using GC–MS analysis , 2020 .

[40]  A. S. Mohamed,et al.  Rapid identification of pork for halal authentication using the electronic nose and gas chromatography mass spectrometer with headspace analyzer. , 2011, Meat science.

[41]  D. Wijaya,et al.  Information Quality Ratio as a novel metric for mother wavelet selection , 2017 .

[42]  Silvio D. Rodríguez,et al.  Fast and Efficient Food Quality Control Using Electronic Noses: Adulteration Detection Achieved by Unfolded Cluster Analysis Coupled with Time-Window Selection , 2014, Food Analytical Methods.

[43]  M. Nurjuliana,et al.  Analysis of Lard’s Aroma by an Electronic Nose for Rapid Halal Authentication , 2011 .

[44]  Shoffi Sabilla The Dataset for Pork Adulteration from Electronic Nose System , 2020 .

[45]  Gaël Varoquaux,et al.  Scikit-learn: Machine Learning in Python , 2011, J. Mach. Learn. Res..

[46]  Zhenbo Wei,et al.  Combination of an E-Nose and an E-Tongue for Adulteration Detection of Minced Mutton Mixed with Pork , 2019, Journal of Food Quality.

[47]  Ana Uluwiyah,et al.  Estimating city-level poverty rate based on e-commerce data with machine learning , 2020, Electron. Commer. Res..

[48]  Yun Liu,et al.  Rapid Identification of Pork Adulterated in the Beef and Mutton by Infrared Spectroscopy , 2018 .

[49]  Yunqian Ma,et al.  Practical selection of SVM parameters and noise estimation for SVM regression , 2004, Neural Networks.

[50]  Despina P Kalogianni,et al.  Lateral flow test for meat authentication with visual detection. , 2019, Food chemistry.

[51]  J. Namieśnik,et al.  Development and validation of a GC–MS/MS method for the determination of 11 amphetamines and 34 synthetic cathinones in whole blood , 2019, Forensic Toxicology.

[52]  Simon X. Yang,et al.  Circuit and Noise Analysis of Odorant Gas Sensors in an E-Nose , 2005, Sensors (Basel, Switzerland).