Sample preparation in analysis of pharmaceuticals

Sample preparation is a very important and essential step in environmental analysis. This article presents an overview of extraction methods for environmental samples, focusing especially on pharmaceuticals as there is great concern about them as pollutants.

[1]  J. Pawliszyn,et al.  SPME in environmental analysis , 2006, Analytical and bioanalytical chemistry.

[2]  A. Paschke.  Consideration of the physicochemical properties of sample matrices – an important step in sampling and sample preparation , 2003 .

[3]  L. Krutz,et al.  Solid-phase microextraction for herbicide determination in environmental samples. , 2003, Journal of chromatography. A.

[4]  Yuan-zong Li,et al.  Chromatographic characterization of sulfonamide imprinted polymers , 2001 .

[5]  W. Ding,et al.  Determination of pharmaceutical residues in waters by solid-phase extraction and large-volume on-line derivatization with gas chromatography-mass spectrometry. , 2005, Journal of chromatography. A.

[6]  Á. Ríos,et al.  Supercritical fluid extraction: a critical review of its analytical usefulness , 2004 .

[7]  Mathew Muzi Nindi,et al.  Multiresidue determination of sulfonamides in a variety of biological matrices by supported liquid membrane with high pressure liquid chromatography-electrospray mass spectrometry detection. , 2004, Talanta.

[8]  L. Mathiasson,et al.  Liquid membrane extraction in analytical sample preparation , 1999 .

[9]  Xiwen He,et al.  Comparison of trimethoprim molecularly imprinted polymers in bulk and in sphere as the sorbent for solid-phase extraction and extraction of trimethoprim from human urine and pharmaceutical tablet and their determination by high-performance liquid chromatography , 2005 .

[10]  S. Weigel,et al.  Simultaneous solid-phase extraction of acidic, neutral and basic pharmaceuticals from aqueous samples at ambient (neutral) pH and their determination by gas chromatography-mass spectrometry. , 2004, Journal of chromatography. A.

[11]  J. Namieśnik,et al.  Trends in solventless sample preparation techniques for environmental analysis. , 2007, Journal of biochemical and biophysical methods.

[12]  A. Posyniak,et al.  Dispersive solid-phase extraction for the determination of sulfonamides in chicken muscle by liquid chromatography. , 2005, Journal of chromatography. A.

[13]  K. Carlson,et al.  Quantification of human and veterinary antibiotics in water and sediment using SPE/LC/MS/MS , 2007, Analytical and bioanalytical chemistry.

[14]  Roger M. Smith,et al.  Sample preparation techniques for the determination of trace residues and contaminants in foods. , 2007, Journal of chromatography. A.

[15]  S. Barker.  Matrix solid phase dispersion (MSPD). , 2007, Journal of biochemical and biophysical methods.

[16]  Bent Halling-Sørensen,et al.  Simultaneous extraction of tetracycline, macrolide and sulfonamide antibiotics from agricultural soils using pressurised liquid extraction, followed by solid-phase extraction and liquid chromatography-tandem mass spectrometry. , 2004, Journal of chromatography. A.

[17]  A. Fernández-Alba,et al.  LC-MS analysis of basic pharmaceuticals (beta-blockers and anti-ulcer agents) in wastewater and surface water , 2007 .

[18]  J. Beausse.  Selected drugs in solid matrices: a review of environmental determination, occurrence and properties of principal substances , 2004 .

[19]  J. Pawliszyn,et al.  Bioanalytical applications of solid-phase microextraction , 2007 .

[20]  L. Pérez-Arribas,et al.  Chemically modified polymeric sorbents for sample preconcentration. , 2000, Journal of chromatography. A.

[21]  Yogesh Mohan,et al.  Microwave Assisted Extraction-An Innovative and Promising Extraction Tool for Medicinal Plant Research , 2007 .

[22]  W. Buchberger.  Novel analytical procedures for screening of drug residues in water, waste water, sediment and sludge. , 2007, Analytica chimica acta.

[23]  D. Sherrington,et al.  Synthesis and application of an oxytetracycline imprinted polymer for the solid-phase extraction of tetracycline antibiotics , 2005 .

[24]  Roger M. Smith.  Before the injection--modern methods of sample preparation for separation techniques. , 2003, Journal of chromatography. A.

[25]  K. Thomas,et al.  Determination of selected human pharmaceutical compounds in effluent and surface water samples by high-performance liquid chromatography-electrospray tandem mass spectrometry. , 2003, Journal of chromatography. A.

[26]  E. Benito-Peña,et al.  Evaluation of mixed mode solid phase extraction cartridges for the preconcentration of beta-lactam antibiotics in wastewater using liquid chromatography with UV-DAD detection , 2006 .

[27]  G. G. Stokes.  "J." , 1890, The New Yale Book of Quotations.

[28]  D. Calamari,et al.  A multiresidue analytical method using solid-phase extraction and high-pressure liquid chromatography tandem mass spectrometry to measure pharmaceuticals of different therapeutic classes in urban wastewaters. , 2005, Journal of chromatography. A.

[29]  M. Kaštelan-macan,et al.  Comparison of Different Solid-Phase Extraction Materials for Sample Preparation in the Analysis of Veterinary Drugs in Water Samples , 2006, JPC – Journal of Planar Chromatography – Modern TLC.

[30]  R. Maxwell,et al.  Multiresidue supercritical fluid extraction method for the recovery at low ppb levels of three sulfonamides from fortified chicken liver. , 1998, Journal of chromatography. B, Biomedical sciences and applications.

[31]  R. Compañó,et al.  Determination of Tetracyclines in Water Samples Using Liquid Chromatography with Fluorimetric Detection , 2005 .

[32]  R. Compañó,et al.  Analysis of macrolide antibiotics in river water by solid-phase extraction and liquid chromatography-mass spectrometry. , 2006, Journal of chromatography. A.

[33]  V. Balakrishnan,et al.  Determination of sulfonamide antibiotics in wastewater: a comparison of solid phase microextraction and solid phase extraction methods. , 2006, Journal of chromatography. A.

[34]  A. Gentili.  LC-MS methods for analyzing anti-inflammatory drugs in animal-food products , 2007 .

[35]  F. David,et al.  Stir bar sorptive extraction-thermal desorption-capillary GC-MS for profiling and target component analysis of pharmaceutical drugs in urine. , 2003, Journal of pharmaceutical and biomedical analysis.

[36]  J. T. Stewart,et al.  Supercritical fluid extraction of selected pharmaceuticals from water and serum. , 1997, Journal of chromatography. B, Biomedical sciences and applications.

[37]  S. Pedersen‐Bjergaard,et al.  Developments in hollow fibre-based, liquid-phase microextraction , 2004 .

[38]  E. Thurman,et al.  Analysis of trace levels of sulfonamide and tetracycline antimicrobials in groundwater and surface water using solid-phase extraction and liquid chromatography/mass spectrometry. , 2001, Analytical chemistry.

[39]  D. Barceló.  Emerging pollutants in water analysis , 2003 .

[40]  N. Leepipatpiboon,et al.  Validation of a liquid chromatography-mass spectrometry multi-residue method for the simultaneous determination of sulfonamides, tetracyclines, and pyrimethamine in milk. , 2007, Journal of chromatography. A.

[41]  C. Stamm,et al.  Exhaustive extraction of sulfonamide antibiotics from aged agricultural soils using pressurized liquid extraction. , 2006, Journal of chromatography. A.

[42]  Thorsten Reemtsma,et al.  Suitability of hollow fibre liquid-phase microextraction for the determination of acidic pharmaceuticals in wastewater by liquid chromatography-electrospray tandem mass spectrometry without matrix effects. , 2004, Journal of chromatography. A.

[43]  Hiroyuki Kataoka,et al.  New trends in sample preparation for clinical and pharmaceutical analysis , 2003 .

[44]  A. Boxall,et al.  Ultrasonic extraction of veterinary antibiotics from soils and pig slurry with SPE clean-up and LC-UV and fluorescence detection. , 2004, Talanta.

[45]  M. Nindi,et al.  Comparative study of sample preparation methods; supported liquid membrane and solid phase extraction in the determination of benzimidazole anthelmintics in biological matrices by liquid chromatography-electrospray-mass spectrometry. , 2006, Talanta.

[46]  F. Borrull,et al.  New hydrophilic materials for solid-phase extraction , 2005 .

[47]  M. Zhang,et al.  Monitoring of five sulfonamide antibacterial residues in milk by in-tube solid-phase microextraction coupled to high-performance liquid chromatography. , 2005, Journal of agricultural and food chemistry.

[48]  D. Barceló,et al.  Environmental behavior and analysis of veterinary and human drugs in soils, sediments and sludge , 2003 .

[49]  S. Barker,et al.  Matrix solid-phase dispersion. , 2000, Journal of chromatography. A.

[50]  M. H. Akhtar,et al.  Extraction of salinomycin from finished layers ration by microwave solvent extraction followed by liquid chromatography , 1996 .

[51]  H. Kataoka,et al.  Determination of fluoroquinolones in environmental waters by in-tube solid-phase microextraction coupled with liquid chromatography–tandem mass spectrometry , 2006 .