Particle size analysis by laser diffraction

Abstract Particle size distribution is a fundamental property of any sediment or soil, and particle size determination can provide important clues to sediment provenance. For forensic work, the particle size distribution of sometimes very small samples requires precise determination using a rapid and reliable method with a high resolution. A protocol has been developed using a Coulter™ LS230 laser granulometer, which can analyse particles in the size range 0.04 μm–2000μm. The technique is essentially non-destructive, permitting the recovery of critical samples, and has been demonstrated to have high precision for a range of soils, sediments and powders of interest in forensic investigations.

[1]  E. Molinaroli,et al.  STREAM-SCANNING LASER SYSTEM, ELECTRIC SENSING COUNTER AND SETTLING GRAIN SIZE ANALYSIS: A COMPARISON USING REFERENCE MATERIALS AND MARINE SEDIMENTS , 2000 .

[2]  I. N. McCave,et al.  Evaluation of a Laser-Diffraction-Size Analyzer for Use with Natural Sediments: RESEARCH METHOD PAPER , 1986 .

[3]  A. Chappell Dispersing sandy soil for the measurement of particle size distributions using optical laser diffraction , 1998 .

[4]  K. Pye,et al.  Morphological and Sedimentological Changes on an Artificially Nourished Beach, Lincolnshire, UK , 2004 .

[5]  J. Allen,et al.  Iron Age to Early Modern Activity and Palaeochannels at Magor Pill, Gwent: An Exercise in Lowland Coastal-Zone Geoarchaeology , 1997, The Antiquaries Journal.

[6]  G. Friedman Differences in size distributions of populations of particles among sands of various origins: addendum to IAS Presidential Address , 1979 .

[7]  V. K. Mer Particle size: Measurement, Interpretation and application , 1964 .

[8]  Shaun Hayton,et al.  Effect of Mica on Particle-Size Analyses Using the Laser Diffraction Technique: RESEARCH METHODS PAPERS , 2001 .

[9]  G. Friedman Address of the retiring President of the International Association of Sedimentologists: Differences in size distributions of populations of particles among sands of various origins , 1979 .

[10]  R. Folk,et al.  Brazos River bar [Texas]; a study in the significance of grain size parameters , 1957 .

[11]  W. C. Krumbein Measurement and geological significance of shape and roundness of sedimentary particles , 1941 .

[12]  C. Nelson,et al.  Effect of Mica on Particle-Size Analyses Using the Laser Diffraction Technique , 2001 .

[13]  G. Gettinby,et al.  Particle-size distribution analysis of soils using laser diffraction , 1987 .

[14]  P. Komar,et al.  The Analysis of Grain-Size Measurements by Sieving and Settling-Tube Techniques , 1984 .

[15]  J. Allen Late Flandrian (Holocene) tidal palaeochannels, Gwent Levels (Severn Estuary), SW Britain: character, evolution and relation to shore , 2000 .

[16]  G. Gettinby,et al.  Determination of particle-size distribution of soils in forensic-science using classical and modern instrumental methods , 1989 .

[17]  L. Froyen,et al.  Grain-size analysis by laser diffractometry: comparison with the sieve-pipette method , 1998 .

[18]  D. Thoenes,et al.  Laser Diffraction Spectrometry: Fraunhofer Diffraction Versus Mie Scattering , 1987 .

[19]  K. Pye,et al.  Colour theory and the evaluation of an instrumental method of measurement using geological samples for forensic applications , 2004, Geological Society, London, Special Publications.

[20]  K. Wohletz,et al.  Discrimination of grain-size subpopulations in pyroclastic deposits , 1987 .

[21]  Jef Vandenberghe,et al.  Comparison of laser grain size analysis with pipette and sieve analysis: a solution for the underestimation of the clay fraction , 1997 .

[22]  E. Bui,et al.  Using quartz grain size and shape analysis to distinguish between aeolian and fluvial deposits in the Dallol Bosso of Niger (West Africa) , 1989 .

[23]  M. John Grain size determination and interpretation , 1988 .

[24]  Jean-Luc Loizeau,et al.  Evaluation of a wide range laser diffraction grain size analyser for use with sediments , 1994 .

[25]  K. Pye,et al.  GRADISTAT: a grain size distribution and statistics package for the analysis of unconsolidated sediments , 2001 .