Sulfur-assisted Fabrication of Silicon Nitride Nanorods in Autoclaves at 250 °C

Silicon nitride nanorods were fabricated from Si, NaN3, and sulfur powder at 250 °C. XRD patterns show that the final product is mixed α- and β-Si3N4. SEM, TEM, and HRTEM images reveal that the pro...

[1]  Y. Qian,et al.  Nitridation of Silica to an α‐Silicon Nitride Nanorod Using NaNH2 in the Autoclave at 700°C , 2007 .

[2]  I. Tanaka,et al.  Recent Advances in New Hard High‐Pressure Nitrides , 2006 .

[3]  Chengguo Wang,et al.  Rapid synthesis of Si3N4 dendritic crystals , 2006 .

[4]  Enric Bertran,et al.  Si3N4 single-crystal nanowires grown from silicon micro- and nanoparticles near the threshold of passive oxidation , 2005, 0811.3575.

[5]  Y. Qian,et al.  Single-crystalline alpha silicon–nitride nanowires: Large-scale synthesis, characterization, and optic properties , 2005 .

[6]  H. Miao,et al.  Synthesis of Single‐Crystalline Silicon Nitride Nanobelts Via Catalyst‐Assisted Pyrolysis of a Polysilazane , 2005 .

[7]  H. Miao,et al.  Growth of platelike and branched single-crystalline Si3N4 whiskers , 2004 .

[8]  Y. Qian,et al.  Low‐Temperature Synthesis of Nanocrystalline α‐Si3N4 Powders by the Reaction of Mg2Si with NH4Cl , 2004 .

[9]  B. Stoner,et al.  Nucleation and growth of silicon nitride nanoneedles using microwave plasma heating , 2001 .

[10]  Junqing Hu,et al.  A Novel Low‐Temperature Synthetic Route to Crystalline Si3N4 , 1999 .

[11]  Bing-Lin Gu,et al.  SYNTHESIS OF SILICON NITRIDE NANORODS USING CARBON NANOTUBE AS A TEMPLATE , 1997 .

[12]  W. Lee,et al.  Combustion synthesis of Si_3N_4 powder , 1997 .

[13]  F. Rodríguez-Reinoso,et al.  Synthesis of SiC and Si3N4: An overview , 1995 .

[14]  A. Varma,et al.  Quantitative phase analysis of Si3N4 by X-ray diffraction , 1992 .

[15]  J. Mukerji,et al.  The comparative behaviour and some parameters on the carbothermal reduction and nitridation of aluminosilicates , 1992 .

[16]  P. Morgan,et al.  Synthesis of Si3N4 with Emphasis on Si-S-N Chemistry , 1985 .

[17]  A. Jayaraman,et al.  Pressure-Induced Valence Change in Cerium Phosphide , 1976 .

[18]  K. Komeya,et al.  Synthesis of the α form of silicon nitride from silica , 1975 .

[19]  K. S. Mazdiyasni,et al.  Synthesis, Characterization, and Consolidation of Si3N4 Obtained from Ammonolysis of SiCl4 , 1973 .

[20]  A. Haas The Chemistry of Silicon-Sulfur Compounds , 1965 .

[21]  E. A. Secco Thermal decomposition of sodium azide crystals , 1962 .