Classical molecular replacement methods and the newer six-dimensional searches treat molecular replacement as a succession of sub-problems of reduced dimensionality. Due to their `divide-and-conquer' approach, these methods necessarily ignore (at least during their early stages) the very knowledge that a target crystal structure may comprise, for example, more than one copy of a search model, or several models of different types. An algorithm for a stochastic multi-dimensional molecular replacement search has been described previously and shown to locate solutions successfully, even in cases as complex as a 23-dimensional 4-body search. The original description of the method only dealt with a special case of molecular replacement, namely with the problem of placing n copies of only one search model in the asymmetric unit of a target crystal structure. Here a natural generalization of this algorithm is presented to deal with the full molecular replacement problem, that is, with the problem of determining the orientations and positions of a total of n copies of m different models (with n ≥ m) which are assumed to be present in the asymmetric unit of a target crystal structure. The generality of this approach is illustrated through its successful application to a 17-dimensional 3-model problem involving one DNA and two protein molecules.
[1]
Jorge Navaza,et al.
[33] AMoRe: An automated molecular replacement program package.
,
1997,
Methods in enzymology.
[2]
Axel T. Brunger,et al.
Free R value: cross-validation in crystallography.
,
1997
.
[3]
R. Mcgreevy,et al.
Structural modelling of glasses using reverse Monte Carlo simulation
,
1990,
Nature.
[4]
J. Navaza,et al.
AMoRe: an automated package for molecular replacement
,
1994
.
[5]
S. Harrison,et al.
Structure of the DNA-binding domains from NFAT, Fos and Jun bound specifically to DNA
,
1998,
Nature.
[6]
M G Rossmann,et al.
The molecular replacement method.
,
1990,
Acta crystallographica. Section A, Foundations of crystallography.