Correction factors for 4-probe electrical measurements with finite size electrodes and material anisotropy: a finite element study

In four-probe (4-probe) electrical measurements, especially on highly resistive materials, it is not always possible to configure the electrodes such that the current density is uniform throughout the sample. Under such circumstances, simply considering the material's electrical resistivity to be proportional to the measured resistance with the proportionality constant given by the sample geometry can give an incorrect result. In this paper, a numerical finite element model is presented which can extract a material's true resistivity from co-linear 4-probe electrical measurements on highly resistive samples with large electrodes that extend across the sample width. The finite element model is used to investigate the influence of material anisotropy, the resistance of the sample–electrode interfaces and the relative electrode-to-sample size on the potential and current density distributions in the sample. A correction factor is introduced to account for the impact of these effects on the measured resistivity. In the limit of large interface resistance, excellent agreement is found with an analytical expression derived elsewhere (Esposito et al 2000 J. Appl. Phys. 88 2724–9). The approach presented here can be used to evaluate a variety of effects on co-linear 4-probe electrical measurements, can be extended to complex specimen geometries with arbitrary electrode arrangements and, additionally, could find use in the evaluation of data from 4-probe thermal conductivity measurements.

[1]  G. Levin On the theory of measurement of anisotropic electrical resistivity by flux transformer method , 1997 .

[2]  Arthur Uhlir,et al.  The potentials of infinite systems of sources and numerical solutions of problems in semiconductor engineering , 1955 .

[3]  Ries,et al.  New aspects of the mixed state from six-terminal measurements on Bi2Sr2CaCu2Ox single crystals. , 1992, Physical review letters.

[4]  Yicai Sun,et al.  New method of calculating the correction factors for the measurement of sheet resistivity of a square sample with a square four-point probe , 1997 .

[5]  Robert A. Weller,et al.  An algorithm for computing linear four-point probe thickness correction factors , 2001 .

[6]  P. Steendijk,et al.  The four-electrode resistivity technique in anisotropic media: theoretical analysis and application on myocardial tissue in vivo , 1993, IEEE Transactions on Biomedical Engineering.

[7]  F. Smits Measurement of sheet resistivities with the four-point probe , 1958 .

[8]  熊谷 寛夫 B.I.Bleaney and B. Bleaney: Electricity and Magnetism; Oxford University Press; London; 1957年(第1版), 676頁, 15×23cm, 63s。 , 1957 .

[9]  L. B. Valdes,et al.  Resistivity Measurements on Germanium for Transistors , 1954, Proceedings of the IRE.

[10]  L. B. Valdes,et al.  Effect of Electrode Spacing on the Equivalent Base Resistance of Point-Contact Transistors , 1952, Proceedings of the IRE.

[11]  M. B. Maple,et al.  Nonmonotonic evolution of out-of-plane resistivity with Pr doping in Y{sub 1{minus}x}Pr{sub x}Ba{sub 2}Cu{sub 3}O{sub 7{minus}{delta}} single crystals , 1997 .

[12]  Hugh O. Pierson,et al.  Handbook of carbon, graphite, diamond, and fullerenes : properties, processing, and applications , 1993 .

[13]  D. Schroder Semiconductor Material and Device Characterization , 1990 .

[14]  Nobuo Takeda,et al.  New concept for modeling the electromechanical behavior of unidirectional carbon-fiber-reinforced plastic under tensile loading , 2003 .

[15]  Y. Kim,et al.  Geometric effects on resistivity measurements with four-electrode probes in isotropic and anisotropic tissues , 1998, IEEE Transactions on Biomedical Engineering.

[16]  Luigi Muzzi,et al.  Determination of the resistivity components ρab and ρc from multiterminal measurements in Bi2Sr2CaCu2O8+x crystals , 2000 .

[17]  D. C. Northrop,et al.  Specific contact resistance measurements on semiconductors , 1989 .

[18]  S. Stankovich,et al.  Graphene-based composite materials , 2006, Nature.