Elastic stiffness and damping measurements in titanium alloys using atomic force acoustic microscopy

Abstract Atomic force acoustic microscopy (AFAM) has been used to study the distribution of elastic stiffness and damping properties across different phases, such as α & β phases in a β titanium alloy (Ti 10V 4.5Fe 1.5Al) and α , β and α ′ phases in an α  +  β alloy (Ti 6Al 4V). Contact-resonance spectra were obtained with a 100 nm spatial resolution in various specimens of the two titanium alloys heat-treated at different temperatures. The study indicates that the metastable β phase has the minimum modulus and maximum damping followed by α ′ and α -phases. Employing the rule of mixtures, the average modulus measured by AFAM was then compared with the modulus obtained by ultrasonic velocity measurements. The error in the average modulus values obtained by both techniques is discussed.

[1]  Manika Prasad,et al.  Measurement of Young's modulus of clay minerals using atomic force acoustic microscopy , 2002 .

[2]  Ute Rabe,et al.  Atomic Force Acoustic Microscopy , 2013 .

[3]  R. Tilley Understanding Solids; The Science of Materials , 2004 .

[4]  Anish Kumar,et al.  Characterization of solutionizing behavior in VT14 titanium alloy using ultrasonic velocity and attenuation measurements , 2003 .

[5]  W. Arnold,et al.  On the Contribution of Friction to the Contact Damping in Atomic Force Acoustic Microscopy , 2010 .

[6]  Sunghak Lee,et al.  Effect of precipitates on damping capacity and mechanical properties of Ti–6Al–4V alloy , 2008 .

[7]  Anish Kumar,et al.  Mapping of elasticity and damping in an α + β titanium alloy through atomic force acoustic microscopy , 2015, Beilstein journal of nanotechnology.

[8]  E. Collings,et al.  Materials Properties Handbook: Titanium Alloys , 1994 .

[9]  Philip A. Yuya,et al.  Viscoelastic property mapping with contact resonance force microscopy. , 2011, Langmuir : the ACS journal of surfaces and colloids.

[10]  Joseph A. Turner,et al.  Atomic force acoustic microscopy methods to determine thin-film elastic properties , 2003 .

[11]  S. Ankem,et al.  Phase Stability and Stress-Induced Transformations in Beta Titanium Alloys , 2015 .

[12]  W. Arnold,et al.  Observation of local internal friction and plasticity onset in nanocrystalline nickel by atomic force acoustic microscopy , 2009 .

[13]  Philip A. Yuya,et al.  Relationship between Q-factor and sample damping for contact resonance atomic force microscope measurement of viscoelastic properties , 2011 .

[14]  Anish Kumar,et al.  Mapping of Elastic Stiffness in an α+β Titanium Alloy using Atomic Force Acoustic Microscopy , 2008 .

[15]  Anish Kumar,et al.  Elasticity mapping of delta precipitate in alloy 625 using atomic force acoustic microscopy with a new approach to eliminate the influence of tip condition , 2014 .

[16]  Z. Guo,et al.  Material properties for process simulation , 2009 .

[17]  Mathias Göken,et al.  Imaging and measurement of local mechanical material properties by atomic force acoustic microscopy , 2002 .

[18]  Anthony B. Kos,et al.  SPRITE: a modern approach to scanning probe contact resonance imaging , 2014 .

[19]  Philip A. Yuya,et al.  Contact-resonance atomic force microscopy for viscoelasticity , 2008 .

[20]  M. Mohammed,et al.  Beta Titanium Alloys: The Lowest Elastic Modulus for Biomedical Applications: A Review , 2014 .

[21]  Anish Kumar,et al.  A new methodology for identification of β-transus temperature in α + β and β titanium alloys using ultrasonic velocity measurement , 2008 .

[22]  Ji Fu,et al.  Nanomechanical mapping of glass fiber reinforced polymer composites using atomic force acoustic microscopy , 2014 .

[23]  Anish Kumar,et al.  Measurement of local internal friction in metallic glasses , 2014 .

[24]  N. Saunders,et al.  An Integrated Approach To The Calculation Of Materials Properties For Ti-Alloys , 2003 .

[25]  Anish Kumar,et al.  Ultrasonic Characterization of Microstructural Changes in Ti-10V-4.5Fe-1.5Al β-Titanium Alloy , 2015, Metallurgical and Materials Transactions A.

[26]  Hirotsugu Ogi,et al.  Elastic–stiffness mapping by resonance-ultrasound microscopy with isolated piezoelectric oscillator , 2003 .

[27]  D. Raabe,et al.  Theory-guided bottom-up design of β-titanium alloys as biomaterials based on first principles calculations: Theory and experiments , 2007 .

[28]  M. Gepreel,et al.  First-principles study on the effect of alloying elements on the elastic deformation response in β-titanium alloys , 2015 .

[29]  S. Hanada,et al.  Beta Ti Alloys with Low Young's Modulus , 2004 .

[30]  W. Arnold,et al.  Local elastic properties of a metallic glass. , 2011, Nature materials.

[31]  R. Pederson Microstructure and phase transformation of Ti-6Al-4V , 2002 .

[32]  Rajamallu Karre,et al.  First principles theoretical investigations of low Young's modulus beta Ti-Nb and Ti-Nb-Zr alloys compositions for biomedical applications. , 2015, Materials science & engineering. C, Materials for biological applications.

[33]  Keiichi Nakamoto,et al.  Resonance frequency and Q factor mapping by ultrasonic atomic force microscopy , 2001 .

[34]  A. Singh,et al.  Microstructure and texture of rolled and annealed β titanium alloy Ti-10V-4.5Fe-1.5Al , 1999 .

[35]  Anish Kumar,et al.  Elasticity mapping of precipitates in polycrystalline materials using atomic force acoustic microscopy , 2008 .