Nanoindentation technique for measuring residual stress field around a laser-induced crack in fused silica

A nanometre scale indentation technique using microprobe indentations to measure residual stresses at selected positions near u.v.-laser-induced cracks in fused silica is presented. The approach is based on the observation that the nanoindentations' penetration depths are affected by the residual stress field emanating from the laser-induced crack. A simple theoretical model based on the change of the nanoindentation penetration depth as well as the change in Young's modulus and hardness of the material is derived. The results show good agreement with the inclusion model [15] suggesting that the residual stress field around a laser-induced crack in fused silica is of shear nature. An exploratory test made on an unstressed sample (free of a laser-induced crack), yielding values for Young's modulus and hardness in accordance with handbook values, shows the high accuracy of this nanoindentation diagnostic.

[1]  B. Lawn Fracture of Brittle Solids by Brian Lawn , 1993 .

[2]  G. S. Glaesemann,et al.  Strength Variability of Indented Soda-Lime Glass , 1987 .

[3]  J. Petrovic,et al.  Controlled surface-flaw-initiated fracture in reaction-bonded Si3N4 , 1976 .

[4]  D. J. Green,et al.  Determination of Subcritical Crack Growth Parameters by In Situ Observation of Indentation Cracks , 1995 .

[5]  John C. Lambropoulos,et al.  Constitutive Law for the Densification of Fused Silica, with Applications in Polishing and Microgrinding , 1996 .

[6]  R. A. Myers,et al.  Large second-order nonlinearity in poled fused silica. , 1991, Optics letters.

[7]  Hironobu Sakata,et al.  Ellipsometric study of polished glass surfaces , 1969 .

[8]  J. Rice,et al.  Elementary engineering fracture mechanics , 1974 .

[9]  K Ishikawa,et al.  High-sensitivity two-dimensional thermal- and mechanical-stress-induced birefringence measurements in a Nd:YAG rod. , 1994, Applied optics.

[10]  D. Stone,et al.  An investigation of hardness and adhesion of sputter-deposited aluminum on silicon by utilizing a continuous indentation test , 1988 .

[11]  M. Crisp,et al.  Laser induced surface damage. , 1973, Applied optics.

[12]  B. Lawn,et al.  A Critical Evaluation of Indentation Techniques for Measuring Fracture Toughness: II, Strength Method , 1981 .

[13]  B. Zysset,et al.  Pulsed optical damage threshold of potassium niobate. , 1992, Applied optics.

[14]  M. Soileau,et al.  Laser-induced breakdown in crystalline and amorphous SiO 2 , 1980 .

[15]  Brian R. Lawn,et al.  A Critical Evaluation of Indentation Techniques for Measuring Fracture Toughness: I , 1981 .