Damage investigation and modeling of 3D woven ceramic matrix composites from X-ray tomography in-situ tensile tests

The present paper proposes an investigation of the failure events in a melt-infiltrated SiC/SiC composite. In-situ X-ray microtomography tensile tests were performed at room temperature and at 1250 • C in air. Digital Volume Correlation has been used to identify the damage mechanisms within the material at increasing loads and to propose a damage scenario. Realistic finite element meshes have been constructed from the 3D images to numerically reproduce the experiments at the meso-scale. Elastic simulations exhibit stress concentrations in the planes containing the weft tows. The first cracks and subsequent damage localization were found to appear within these planes thanks to the analysis of the in-situ tomographic data.

[1]  M. A. Verges,et al.  X-ray computed microtomography of internal damage in fiber reinforced polymer matrix composites , 2005 .

[2]  E. Maire,et al.  In Situ Experiments with X ray Tomography: an Attractive Tool for Experimental Mechanics , 2010 .

[3]  G. Morscher,et al.  In‐Plane Cracking Behavior and Ultimate Strength for 2D Woven and Braided Melt‐Infiltrated SiC/SiC Composites Tensile Loaded in Off‐Axis Fiber Directions , 2007 .

[4]  P. Zaslansky,et al.  Tensile failure observations in sintered steel foam struts revealed by sub-micron contrast-enhanced microtomography , 2016 .

[5]  Peter Cloetens,et al.  A study of fracture of unidirectional composites using in situ high-resolution synchrotron X-ray microtomography , 2006 .

[6]  P. Spriet,et al.  Applications of CMCs to Turbojet Engines: Overview of the SEP Experience , 1996 .

[7]  F. Rebillat,et al.  Oxidation mechanisms and kinetics of SiC-matrix composites and their constituents , 2004 .

[8]  Youqi Wang,et al.  Dynamic relaxation approach with periodic boundary conditions in determining the 3-D woven textile micro-geometry , 2013 .

[9]  B. Bay,et al.  Digital volume correlation: Three-dimensional strain mapping using X-ray tomography , 1999 .

[10]  W. Ludwig,et al.  In situ X-ray microtomography characterization of damage in SiCf/SiC minicomposites , 2011 .

[11]  Andrew Drach,et al.  Processing of fiber architecture data for finite element modeling of 3D woven composites , 2014, Adv. Eng. Softw..

[12]  Gregory N. Morscher,et al.  Stress-Dependent Matrix Cracking in 2D Woven Sic-Fiber Reinforced Melt-Infiltrated Sic Matrix Composites , 2013 .

[13]  Colin Studholme,et al.  An overlap invariant entropy measure of 3D medical image alignment , 1999, Pattern Recognit..

[14]  M. Wevers,et al.  Quantification of the internal structure and automatic generation of voxel models of textile composites from X-ray computed tomography data , 2015 .

[15]  J. Tracy Multi-scale Investigation of Damage Mechanisms in SiC/SiC Ceramic Matrix Composites. , 2014 .

[16]  B. Bednarcyk,et al.  Modeling of Melt-Infiltrated SiC/SiC Composite Properties , 2009 .

[17]  Edith Grippon,et al.  Endommagement et microfissuration d’un composite à matrice céramique tissé 3D : approchemulti-échelle et évaluation ultrasonore , 2013 .

[18]  Stéphane Roux,et al.  Localized strain field measurement on laminography data with mechanical regularization , 2014 .

[19]  F. Irisarri,et al.  Comparison between voxel and consistent meso-scale models of woven composites , 2015 .

[20]  Ian Sinclair,et al.  Damage accumulation in a carbon/epoxy composite: Comparison between a multiscale model and computed tomography experimental results , 2012 .

[21]  Pedro P. Camanho,et al.  Influence of geometrical parameters on the elastic response of unidirectional composite materials , 2012 .

[22]  Stéphane Roux,et al.  Three dimensional image correlation from X-Ray computed tomography of solid foam , 2008 .

[23]  Stéphane Roux,et al.  Failure Mechanisms of Plasterboard in Nail Pull Test Determined by X-ray Microtomography and Digital Volume Correlation , 2016 .

[24]  Constantinos Soutis,et al.  2D and 3D imaging of fatigue failure mechanisms of 3D woven composites , 2015 .

[25]  F. Rebillat,et al.  Application of X-ray computed micro-tomography to the study of damage and oxidation kinetics of thermostructural composites , 2014 .

[26]  R. Ritchie,et al.  Real-time Quantitative Imaging of Failure Events in Materials under Load at Temperatures above 1,600 , 2012 .

[27]  Emmanuelle Vidal-Salle,et al.  Meso-scale FE analyses of textile composite reinforcement deformation based on X-ray computed tomography , 2014 .

[28]  Jacques Lamon,et al.  A micromechanics-based approach to the mechanical behavior of brittle-matrix composites , 2001 .

[29]  Suresh G. Advani,et al.  TENSOR DESCRIPTION OF FIBER ORIENTATION IN SHORT FIBER COMPOSITES. , 1985 .

[30]  Stéphane Roux,et al.  Digital Volume Correlation Applied to X‐ray Tomography Images from Spherical Indentation Tests on Lightweight Gypsum , 2014 .

[31]  Pierre Baylou,et al.  Axis detection of cylindrical objects in 3-D images , 2008 .

[32]  P. Withers,et al.  Quantitative X-ray tomography , 2014 .

[33]  E. Maire,et al.  Finite element modelling of the actual structure of cellular materials determined by X-ray tomography , 2005 .

[34]  L. Gélébart,et al.  Effects of porosity on the elastic behaviour of CVI SiC/SiC composites , 2009 .

[35]  A. J. Moffat,et al.  High resolution tomographic imaging and modelling of notch tip damage in a laminated composite , 2010 .

[36]  M. M. Rashid,et al.  Digital volume correlation including rotational degrees of freedom during minimization , 2002 .

[37]  S. Roux,et al.  Digital image correlation and fracture: an advanced technique for estimating stress intensity factors of 2D and 3D cracks , 2009 .

[38]  R. Protz,et al.  A quantitative comparison of the capabilities of in situ computed tomography and conventional computed tomography for damage analysis of composites , 2015 .

[39]  J. Ahmad,et al.  Correlation of elastic properties of melt infiltrated SiC/SiC composites to in situ properties of constituent phases , 2010 .

[40]  G. Morscher,et al.  Correlating Electrical Resistance Change with Mechanical Damage in Woven SiC/SiC Composites: Experiment and Modeling , 2014 .

[41]  E. Maire,et al.  Modeling the properties of closed-cell cellular materials from tomography images using finite shell elements , 2008 .