Experience with irradiation of LiSoR test section no. 3

Abstract LiSoR (liquid metal–solid metal reaction) loop is a unique facility which was designed to investigate simultaneously the influence of flowing lead bismuth eutectic (LBE), static stress and irradiation by protons onto steel that might be used as structural material in a future ADS (accelerator driven system) reactor. LiSoR is worldwide the first LBE loop that is under operation while it is irradiated at the same time. Up to now five LiSoR test sections have been irradiated. In this paper the experience on LiSoR no. 3 is presented including irradiation experiment and dissembling of the test section and EDM wire cutting of the samples. Additionally the results obtained by SEM and EDX analyses on LiSoR specimen and on beam window are shown whereby the most interesting outcome is the finding of an oxide layer, which was clearly identified by X-ray mapping. This layer is located directly in the irradiated area having a total thickness less than 1 μm. Additionally solidified LBE was detected on some areas of the samples but no wetting of the steel or penetration of LBE into the steel matrix was observed. No enrichment or dissolution of steel elements such as Fe and Cr could be detected on the surface near area. The steel surface is still smooth without any indications of corrosion attack.