Strategies for fabricating atom probe specimens with a dual beam FIB.

A FIB-based lift-out method for preparing atom probe specimens at site specific locations such as coarse precipitates, grain boundaries, interphase interfaces, denuded zones, heat affected zones, implanted, near surface and subsurface regions, shear bands, etc. has been developed. FIB-based methods for the fabrication of atom probe specimens from thin ribbons, sheet stock, and powders have been developed.

[1]  H. Nordén,et al.  Preparation of contamination-free tungsten specimens for the field-ion microscope , 1967 .

[2]  H. Fraser,et al.  Atom Probe Tomography Characterization of Multilayer Films , 2003, Microscopy and Microanalysis.

[3]  J. Walls,et al.  The preparation of field electron/field-ion emitters by ion etching , 1974 .

[4]  Peter H. Bartels,et al.  Field ion microscopy;: Principles and applications, , 1969 .

[5]  Lucille A. Giannuzzi,et al.  Introduction to Focused Ion Beams , 2005 .

[6]  J. Papazian The preparation of field‐ion‐microscope specimens containing grain boundaries , 1971 .

[7]  D. Larson,et al.  Atom probe analysis of planar multilayer structures , 2000 .

[8]  G. Smith,et al.  Three-dimensional atom probe studies of metallic multilayers , 1999 .

[9]  R. Buchheit,et al.  Site-Specific FIB Preparation of Atom Probe Samples , 2004, Microscopy and Microanalysis.

[10]  K. F. Russell,et al.  Sharpening of field-ion specimens and positioning of features of interest by ion-beam milling , 2000 .

[11]  R. Hull,et al.  Applications of focused ion beams in microelectronics production, design and development , 1995 .

[12]  H. Fraser,et al.  Some aspects of atom probe specimen preparation and analysis of thin film materials. , 2004, Ultramicroscopy.

[13]  M. Hellsing High resolution microanalysis of binder phase in as sintered WC–Co cemented carbides , 1988 .

[14]  G. Smith,et al.  Atom Probe Microanalysis: Principles and Applications to Materials Problems , 1989 .

[15]  Lucille A. Giannuzzi,et al.  A review of focused ion beam milling techniques for TEM specimen preparation , 1999 .

[16]  D. Larson,et al.  Focused ion-beam specimen preparation for atom probe field-ion microscopy characterization of multilayer film structures , 1999 .

[17]  A. Melmed The art and science and other aspects of making sharp tips , 1991 .

[18]  K. Hono,et al.  A method for preparing atom probe specimens for nanoscale compositional analysis of metallic thin films , 1993 .

[19]  H. Andren,et al.  A specimen preparation technique for atom probe analysis of the near-surface region of cemented carbides , 1996 .

[20]  J. D. Olson,et al.  First Data from a Commercial Local Electrode Atom Probe (LEAP) , 2004, Microscopy and Microanalysis.

[21]  D. Larson,et al.  Advances in Atom Probe Specimen Fabrication from Planar Multilayer Thin Film Structures , 2001, Microscopy and Microanalysis.

[22]  A. Petford-Long,et al.  Information storage materials: nanoscale characterisation by three-dimensional atom probe analysis , 2004 .

[23]  M. Blamire,et al.  Field-ion specimen preparation using focused ion-beam milling , 1999 .

[24]  A. Henjered,et al.  A controlled specimen preparation technique for interface studies with atom-probe field-ion microscopy , 1983 .

[25]  T. C. Anthony,et al.  Three-dimensional atom probe field-ion microscopy observation of Cu/Co multilayer film structures , 1998 .

[26]  T. C. Anthony,et al.  Focused ion-beam milling for field-ion specimen preparation:: preliminary investigations , 1998 .

[27]  David J. Larson,et al.  Local Electrode Atom Probes , 1998, Microscopy and Microanalysis.

[28]  C. Bulle-lieuwma,et al.  Novel scheme for the preparation of transmission electron microscopy specimens with a focused ion beam , 1993 .