Digital holographic microscopy for sub-µm scale high aspect ratio structures in transparent materials

Abstract This paper discusses a digital holographic microscopy approach for comprehensive and non-destructive inspection of spatially confined structures, which are characterized by the high aspect ratio of their lateral dimensions ( ∼ 1:30) and are fabricated out of transparent materials. Two-photon polymerization is chosen as a high-resolution lithographic technology for manufacturing of corresponding structures out of positive photoresin. The proposed holographic inspection method does not require any numerical methods for aberration correction and thus demonstrates rapid phase map evaluation ( ∼ 250 ms per cycle). Applicability and performance of the method has been successfully tested on a set of samples modelled to resemble step-index structures similar to the lab-on-chip basic elements, e.g. waveguides. In terms of lateral resolution a diffraction-limited operation of the proposed imaging system is ensured while vertical accuracy of 1.61 nm has been demonstrated.

[1]  Claas Falldorf,et al.  Digital Holography and Wavefront Sensing: Principles, Techniques and Applications , 2014 .

[2]  U. Schnars,et al.  Direct recording of holograms by a CCD target and numerical reconstruction. , 1994, Applied optics.

[3]  R. Osellame,et al.  Femtosecond laser micromachining : photonic and microfluidic devices in transparent materials , 2012 .

[4]  R. Zengerle,et al.  Microfluidic lab-on-a-chip platforms: requirements, characteristics and applications. , 2010, Chemical Society reviews.

[5]  B. Kemper,et al.  Digital holographic microscopy for live cell applications and technical inspection. , 2008, Applied optics.

[6]  Wolfgang Osten,et al.  Recent advances in digital holography [invited]. , 2014, Applied optics.

[7]  T. Kreis Handbook of Holographic Interferometry: Optical and Digital Methods , 2004 .

[8]  D. Murphy Fundamentals of Light Microscopy and Electronic Imaging , 2001 .

[9]  John A Rogers,et al.  Diffraction phase microscopy: monitoring nanoscale dynamics in materials science [invited]. , 2014, Applied optics.

[10]  Max Born,et al.  Principles of optics - electromagnetic theory of propagation, interference and diffraction of light (7. ed.) , 1999 .

[11]  E. Cuche,et al.  Digital holography for quantitative phase-contrast imaging. , 1999, Optics letters.

[12]  Patrik Langehanenberg,et al.  Characterisation of light emitting diodes (LEDs) for application in digital holographic microscopy for inspection of micro and nanostructured surfaces , 2008 .

[13]  Myung K. Kim,et al.  Wavelength-scanning digital interference holography for tomographic three-dimensional imaging by use of the angular spectrum method. , 2005, Optics letters.

[14]  Peter P. Maksimyak,et al.  Common-path holographic objective for conventional photographic camera , 2017, Optical Engineering + Applications.

[15]  Etienne Cuche,et al.  Numerical parametric lens for shifting, magnification, and complete aberration compensation in digital holographic microscopy. , 2006, Journal of the Optical Society of America. A, Optics, image science, and vision.

[16]  Han Yen Tu,et al.  Phase measurement accuracy in digital holographic microscopy using a wavelength-stabilized laser diode , 2013 .

[17]  Application of white-light scanning interferometer on transparent thin-film measurement. , 2012, Applied optics.

[18]  James C. Wyant,et al.  White light interferometry , 2002, SPIE Defense + Commercial Sensing.

[19]  Peter J. de Groot,et al.  The Meaning and Measure of Vertical Resolution in Optical Surface Topography Measurement , 2017 .

[20]  G. Marowsky Planar waveguides and other confined geometries : theory, technology, production, and novel applications , 2015 .

[21]  Nektarios Koukourakis,et al.  Single-shot holography for depth resolved three dimensional imaging. , 2009, Optics express.

[22]  Pietro Ferraro,et al.  Compensation of the inherent wave front curvature in digital holographic coherent microscopy for quantitative phase-contrast imaging. , 2003, Applied optics.

[23]  B. Chichkov,et al.  Three-dimensional photofabrication with femtosecond lasers for applications in photonics and biomedicine , 2007 .

[24]  Robert Schmitt,et al.  Quantitative comparison of measurement methods for the evaluation of micro- and nanostructures written with 2PP , 2016, SPIE Photonics Europe.

[25]  Koji Sugioka,et al.  Three-dimensional femtosecond laser processing for lab-on-a-chip applications , 2018 .

[26]  R. Leach Optical measurement of surface topography , 2011 .

[27]  M. Hofmann,et al.  Depth-filtering in common-path digital holographic microscopy. , 2017, Optics express.

[28]  Louis A. Romero,et al.  Robust two-dimensional weighted and unweighted phase unwrapping that uses fast transforms and iterative methods , 1994 .

[29]  Munther A. Gdeisat,et al.  Fast two-dimensional phase-unwrapping algorithm based on sorting by reliability following a noncontinuous path. , 2002, Applied optics.

[30]  Baoli Yao,et al.  Simple and fast spectral domain algorithm for quantitative phase imaging of living cells with digital holographic microscopy. , 2017, Optics letters.

[31]  Partha P. Banerjee,et al.  Recent Advances in Digital Holography , 2014 .

[32]  Myung K. Kim Digital Holographic Microscopy: Principles, Techniques, and Applications , 2011 .

[33]  David C. Joy,et al.  Scanning Electron Microscopy and X-Ray Microanalysis , 2017 .

[34]  Victor Bellitto,et al.  Atomic Force Microscopy - Imaging, Measuring and Manipulating Surfaces at the Atomic Scale , 2012 .

[35]  Michael Atlan,et al.  Off-axis digital hologram reconstruction: some practical considerations. , 2011, Applied optics.

[36]  Hui Xie,et al.  Advances in the atomic force microscopy for critical dimension metrology , 2016 .

[37]  Adolf Friedrich Fercher Optical coherence tomography. , 1996 .

[38]  Liang Leon Yuan,et al.  Laser Scanning Holographic Lithography for Flexible 3D Fabrication of Multi-Scale Integrated Nano-structures and Optical Biosensors , 2016, Scientific Reports.

[39]  A. Asundi,et al.  Studies of digital microscopic holography with applications to microstructure testing. , 2001, Applied optics.

[40]  Claas Falldorf,et al.  Digital Holography and Wavefront Sensing , 2015 .

[41]  Renu John,et al.  Optofluidic bioimaging platform for quantitative phase imaging of lab on a chip devices using digital holographic microscopy. , 2016, Applied optics.

[42]  E. Cuche,et al.  Axial sub-nanometer accuracy in digital holographic microscopy , 2008 .

[43]  Andreas Ostendorf,et al.  Effect of a thin reflective film between substrate and photoresin on two-photon polymerization , 2018, Additive Manufacturing.

[44]  Peter P. Maksimyak,et al.  A direct-view customer-oriented digital holographic camera , 2018, International Conference on Correlation Optics.