Dimensionless Framework for Seed Recipe Design and Optimal Control of Batch Crystallization

In order to study and propose guidelines for the design and control of batch crystallization systems with different growth and nucleation parameters, optimal control theory and a dimensionless batc...

[1]  Åke C. Rasmuson,et al.  Nucleation and growth of succinic acid in a batch cooling crystallizer , 1991 .

[2]  H. Kramer,et al.  Estimation of nucleation kinetics from crystal size distribution transients of a continuous crystallizer , 1991 .

[3]  D. L. Ma,et al.  Optimal control and simulation of multidimensional crystallization processes , 2002 .

[4]  Optimal control for batch crystallization with size-dependent growth kinetics , 2011, Proceedings of the 2011 American Control Conference.

[5]  Angelo Chianese,et al.  Determination of Critical Seed Loading Ratio for the Production of Crystals of Uni-Modal Size Distribution in Batch Cooling Crystallization of Potassium Alum , 2002 .

[6]  H. Seki,et al.  Robust optimal temperature swing operations for size control of seeded batch cooling crystallization , 2015 .

[7]  Seeded batch crystallization of ammonium aluminum sulfate from aqueous solution , 2009 .

[8]  Sohrab Rohani,et al.  Crystal Population Balance Formulation and Solution Methods: A Review , 2017 .

[9]  Jörg Raisch,et al.  Control of batch crystallization—A system inversion approach , 2006 .

[10]  J. Chew,et al.  Comparison between Open-Loop Temperature Control and Closed-Loop Supersaturation Control for Cooling Crystallization of Glycine , 2007 .

[11]  Crystallization kinetics of calcium nitrate tetrahydrate from MSMPR crystallizer , 1985 .

[12]  K. Piotrowski,et al.  Crystallization of vitamin C in a continuous DT MSMPR crystallizer – Size independent growth kinetic model approach , 2008 .

[13]  R. Braatz,et al.  Direct design of pharmaceutical antisolvent crystallization through concentration control , 2006 .

[14]  Richard D Braatz,et al.  Advances and new directions in crystallization control. , 2012, Annual review of chemical and biomolecular engineering.

[15]  Frank L. Lewis,et al.  Optimal Control: Lewis/Optimal Control 3e , 2012 .

[16]  Marco Mazzotti,et al.  Design and Optimization of a Combined Cooling/Antisolvent Crystallization Process , 2009 .

[17]  Milan Zelany,et al.  A concept of compromise solutions and the method of the displaced ideal , 1974, Comput. Oper. Res..

[18]  J. Raisch,et al.  Optimal control of univariate and multivariate population balance systems involving external fines removal , 2017 .

[19]  J. Garside,et al.  Crystallization Kinetics from MSMPR Crystallizers , 1980 .

[20]  Allan S. Myerson,et al.  Crystallization of Cyclosporine in a Multistage Continuous MSMPR Crystallizer , 2011 .

[21]  K. Rani,et al.  Multiobjective Optimization of Unseeded and Seeded Batch Cooling Crystallization Processes , 2017 .

[22]  N. Bajçinca.  Analytic solutions to optimal control problems in crystal growth processes , 2013 .

[23]  Satoshi Hoshino,et al.  Evaluation of controlled cooling for seeded batch crystallization incorporating dissolution , 2012 .

[24]  Kieran W Hutton,et al.  Simultaneous Parameter Estimation and Optimization of a Seeded Antisolvent Crystallization , 2012 .

[25]  Brian Glennon,et al.  Estimation of Nucleation and Growth Kinetics of Benzoic Acid by Population Balance Modeling of a Continuous Cooling Mixed Suspension, Mixed Product Removal Crystallizer , 2015 .

[26]  Indraneel Das.  On characterizing the “knee” of the Pareto curve based on Normal-Boundary Intersection , 1999 .

[27]  Christianto Wibowo,et al.  Design of integrated crystallization systems , 2001 .

[28]  Pareto-Optimal Fronts for Simple Crystallization Systems Using Pontryagin’s Minimum Principle , 2019, Industrial & Engineering Chemistry Research.

[29]  Zoltan K. Nagy,et al.  Recent advances in the monitoring, modelling and control of crystallization systems , 2013 .

[30]  M. Giulietti,et al.  Modeling of crystal growth and nucleation rates for pentaerythritol batch crystallization , 2010 .

[31]  A new framework and a simpler method for the development of batch crystallization recipes , 2011 .

[32]  Jeffrey D. Ward,et al.  The best objective function for seeded batch crystallization , 2013 .

[33]  Wolfgang Marquardt,et al.  Dynamic optimization using adaptive control vector parameterization , 2005, Comput. Chem. Eng..

[34]  Debasis Sarkar,et al.  Multi-objective optimization of seeded batch crystallization processes , 2006 .

[35]  Z. Nagy,et al.  Comparative performance of concentration and temperature controlled batch crystallizations , 2008 .

[36]  J. Rawlings,et al.  Model identification and control of solution crystallization processes: a review , 1993 .

[37]  J. Mullin,et al.  Crystal growth rate studies with potassium sulphate in a fluidized bed crystallizer , 1972 .

[38]  J. D. Ward,et al.  Choosing an operating policy for seeded batch crystallization , 2006 .

[39]  J. W. Mullin,et al.  Programmed cooling of batch crystallizers , 1971 .

[40]  Z. Nagy.  Crystallization Control Approaches and Models , 2017 .

[41]  B. Glennon,et al.  Novel, Calibration-Free Strategies for Supersaturation Control in Antisolvent Crystallization Processes , 2013 .

[42]  Daniel J. Griffin,et al.  Feedback Control of Multicomponent Salt Crystallization , 2015 .

[43]  Optimization of Simple Batch Crystallization Systems Considering Crystal Shape and Nucleation , 2020 .

[44]  Wang Zhixiang,et al.  Quantitative design of seed load for solution cooling crystallization based on kinetic analysis , 2010 .

[45]  Thermodynamic Polymorph Selection in Enantiotropic Systems Using Supersaturation-Controlled Batch and Semibatch Cooling Crystallization , 2019, Crystal Growth & Design.

[46]  C. Porte,et al.  Effect of seeded surface area on crystal size distribution in glycine batch cooling crystallization: a seeding methodology , 2004 .

[47]  Noriaki Kubota,et al.  Seeding policy in batch cooling crystallization , 2001 .

[48]  F. Puel,et al.  Improving batch cooling seeded crystallization of an organic weed-killer using on-line ATR FTIR measurement of supersaturation , 2001 .

[49]  Richard D. Braatz,et al.  Modelling and control of combined cooling and antisolvent crystallization processes , 2008 .

[50]  Crystallization kinetics of evaporation rubidium chloride in the MSMPR crystallizer , 2019, Revue Roumaine de Chimie.

[51]  J. Koski.  Defectiveness of weighting method in multicriterion optimization of structures , 1985 .

[52]  Size Distribution of Needle-Shape Crystals of Monosodium L-Glutamate Obtained by Seeded Batch Cooling Crystallization , 2004 .

[53]  J. Dennis,et al.  A closer look at drawbacks of minimizing weighted sums of objectives for Pareto set generation in multicriteria optimization problems , 1997 .

[54]  Jean-Pierre Corriou,et al.  A new look at optimal control of a batch crystallizer , 2008 .

[55]  Jose A. Romagnoli,et al.  A model-based approach for controlling particle size distribution in combined cooling-antisolvent crystallization processes , 2018, Chemical Engineering Science.

[56]  S. Katz,et al.  Some problems in particle technology: A statistical mechanical formulation , 1964 .

[57]  K. Berglund,et al.  ATR-FTIR for Determining Optimal Cooling Curves for Batch Crystallization of Succinic Acid , 2002 .

[58]  Jeffrey D. Ward,et al.  Comparison of objective functions for batch crystallization using a simple process model and Pontryagin's minimum principle , 2017, Comput. Chem. Eng..

[59]  J. D. Ward,et al.  Critical seed loading from nucleation kinetics , 2014 .

[60]  Jörg Raisch,et al.  Control of batch cooling crystallization processes based on orbital flatness , 2003 .