Dividing wall columns in chemical process industry: A review on current activities

In spite of being an energy intensive process, distillation remains the most important separation method in the chemical process industry. Especially for the separation of mixtures with three or more components, the total energy requirement and the capital cost are very high. In this respect, dividing wall columns (DWCs) represent a very promising technology allowing a significant energy requirement reduction. This article reviews current industrial applications of DWCs and related research activities, including column configuration, design, modelling and control issues. Furthermore, the application of DWCs for azeotropic, extractive and reactive distillation is highlighted.

[1]  Jesús Rafael Alcántara-Ávila,et al.  Controllability analysis of alternate schemes to complex column arrangements with thermal coupling for the separation of ternary mixtures , 2008, Comput. Chem. Eng..

[2]  Ljubica Matijašević,et al.  Dividing wall column—A breakthrough towards sustainable distilling , 2010 .

[3]  David Shan-Hill Wong,et al.  Controllability and energy efficiency of a high-purity divided wall column , 2007 .

[4]  Raluca Isopescu,et al.  PROCESS SIMULATION OF REACTIVE DISTILLATION IN DIVIDING WALL COLUMN FOR ETBE SYNTHESIS PROCESS , 2009 .

[5]  Sigurd Skogestad,et al.  NULL SPACE METHOD FOR SELECTING OPTIMAL MEASUREMENT COMBINATIONS AS CONTROLLED VARIABLES , 2007 .

[6]  Gade Pandu Rangaiah,et al.  A Simplified Procedure for Quick Design of Dividing-Wall Columns for Industrial Applications , 2009 .

[7]  Juan Gabriel Segovia-Hernández,et al.  Implementation of a reactive dividing wall distillation column in a pilot plant , 2008 .

[8]  Sunwon Park,et al.  Dynamic simulation for the structural design of the divided wall column for different feed composition and various separation features , 2007, 2007 International Conference on Control, Automation and Systems.

[9]  Hartmut Schoenmakers,et al.  Model predictive control of integrated unit operations: Control of a divided wall column , 2004 .

[10]  Michael A. Schultz,et al.  Reduce Costs with Dividing-Wall Columns , 2002 .

[11]  Michael A. Schultz,et al.  Innovative flowschemes using dividing wall columns , 2006 .

[12]  S. Skogestad,et al.  Minimum Energy Consumption in Multicomponent Distillation. 1. Vmin Diagram for a Two-Product Column , 2003 .

[13]  Claudia Gutiérrez-Antonio,et al.  Dividing wall distillation columns for separation of azeotropic mixtures: feasibility procedure and rigorous optimization , 2009 .

[14]  Juan Gabriel Segovia-Hernández,et al.  Analysis of dynamic properties of alternative sequences to the Petlyuk column , 2005, Comput. Chem. Eng..

[15]  Jesús Rafael Alcántara-Ávila,et al.  Controllability analysis of thermodynamically equivalent thermally coupled arrangements for quaternary distillations , 2008 .

[16]  K. A. Amminudin,et al.  Design and Optimization of Fully Thermally Coupled Distillation Columns: Part 1: Preliminary Design and Optimization Methodology , 2001 .

[17]  K. A. Amminudin,et al.  Design and Optimization of Fully Thermally Coupled Distillation Columns: Part 2: Application of Dividing Wall Columns in Retrofit , 2001 .

[18]  J. Stichlmair,et al.  Separation regions and processes of zeotropic and azeotropic ternary distillation , 1992 .

[19]  Eugeny Y. Kenig,et al.  Rate-based analysis of reactive distillation sequences with different degrees of integration , 2007 .

[20]  Anton A. Kiss,et al.  REACTIVE DIVIDING-WALL COLUMNS: TOWARDS ENHANCED PROCESS INTEGRATION , 2010 .

[21]  C. Triantafyllou,et al.  The design and optimisation of fully thermally coupled distillation columns : Process design , 1992 .

[22]  Jan Harmsen,et al.  Process intensification in the petrochemicals industry: Drivers and hurdles for commercial implementation , 2010 .

[23]  Megan Jobson,et al.  Conceptual design of reactive dividing wall columns , 2006 .

[24]  Ikuho Yamada,et al.  Analysis of Divided-Wall Column for Extractive Distillation. , 2000 .

[25]  Anton A. Kiss,et al.  Energy efficient control of a BTX dividing-wall column , 2011, Comput. Chem. Eng..

[26]  Huajiang Huang,et al.  A review of separation technologies in current and future biorefineries , 2008 .

[27]  Michel Perrier,et al.  Analysis of different control possibilities for the divided wall column: feedback diagonal and dynamic matrix control , 2001 .

[28]  Anton A. Kiss,et al.  REACTIVE DIVIDING-WALL COLUMNS—HOW TO GET MORE WITH LESS RESOURCES? , 2009 .

[29]  J. Segovia-Hernández,et al.  Reactive dividing wall distillation columns: Simulation and implementation in a pilot plant☆ , 2009 .

[30]  Sigurd Skogestad,et al.  Minimum Energy Consumption in Multicomponent Distillation. 2. Three-Product Petlyuk Arrangements , 2003 .

[31]  G Parkinson Distillation: New wrinkles for an age-old technology , 2005 .

[32]  Helmut Jansen,et al.  Distillation Column Internals/Configurations for Process Intensification* , 2003 .

[33]  Ž. Olujić,et al.  Equipment improvement trends in distillation , 2009 .

[34]  Sigurd Skogestad,et al.  Operation of Integrated Three-Product (Petlyuk) Distillation Columns , 1995 .

[35]  Romildo Pereira Brito,et al.  Sensitivity and dynamic behavior analysis of an industrial azeotropic distillation column , 2007 .

[36]  Costin Sorin Bildea,et al.  A control perspective on process intensification in dividing-wall columns , 2011 .

[37]  O. Ryll,et al.  Methyl Acetate Hydrolysis in a Reactive Divided Wall Column , 2007 .

[38]  Yingxia Li,et al.  Separation of acetic acid and water by complex extractive distillation , 2004 .

[39]  Sigurd Skogestad,et al.  Optimizing control of Petlyuk distillation : Understanding the steady-state behavior , 1997 .

[40]  Hartmut Schoenmakers,et al.  Trennwandkolonnen: Entwicklungsstand und Perspektiven , 2006 .

[41]  Gerald Parkinson,et al.  Dividing-wall columns find greater appeal , 2007 .

[42]  Ikuho Yamada,et al.  Azeotropic Distillation Process with Vertical Divided-Wall Column. , 2001 .

[43]  Cristofer Bravo-Bravo,et al.  Extractive Dividing Wall Column: Design and Optimization , 2010 .

[44]  F. Petlyuk Thermodynamically Optimal Method for Separating Multicomponent Mixtures , 1965 .

[45]  Eugeny Y. Kenig,et al.  Reactive Distillation in a Dividing Wall Column: Rate-Based Modeling and Simulation , 2007 .

[46]  Juan Gabriel Segovia-Hernández,et al.  Energy-efficient complex distillation sequences: Control properties , 2008 .

[47]  Valentin Plesu,et al.  Reactive distillation process analysis in a divided wall column , 2007 .

[48]  Juan Gabriel Segovia-Hernández,et al.  Dividing Wall Distillation Columns: Optimization and Control Properties , 2008 .

[49]  William L. Luyben,et al.  New Control Structure for Divided-Wall Columns , 2009 .

[50]  Ben-Guang Rong Systematic Synthesis of Dividing-Wall Columns for Multicomponent Distillations , 2010 .

[51]  Bärbel Kolbe,et al.  Novel distillation concepts using one-shell columns , 2004 .

[52]  Sigurd Skogestad,et al.  Optimal operation of Petlyuk distillation: steady-state behavior , 1999 .

[53]  Gade Pandu Rangaiah,et al.  Retrofitting conventional column systems to dividing-Wall Columns , 2009 .

[54]  Klaus Sattler,et al.  Thermal Separation Processes , 1995 .

[55]  Sigurd Skogestad,et al.  Complex distillation arrangements: Extending the petlyuk ideas , 1997 .

[56]  Fouad M. Khoury Multistage Separation Processes, Third Edition , 2004 .

[57]  Sigurd Skogestad,et al.  Minimum Energy Consumption in Multicomponent Distillation. 3. More Than Three Products and Generalized Petlyuk Arrangements , 2003 .

[58]  G. Kaibel,et al.  Dividing wall columns: Fundamentals and recent advances , 2010 .

[59]  Sigurd Skogestad,et al.  CONCEPTUAL DESIGN AND COMPARISON OF FOUR-PRODUCTS DIVIDING WALL COLUMNS FOR SEPARATION OF A MULTICOMPONENT AROMATICS MIXTURE , 2010 .

[60]  William L. Luyben,et al.  Temperature Control of the BTX Divided-Wall Column , 2010 .

[61]  Anton A. Kiss,et al.  Comparison of Control Strategies for Dividing-Wall Columns , 2010 .

[62]  Michel Perrier,et al.  Study of the divided wall column controllability: influence of design and operation , 2000 .

[63]  Helmut Jansen,et al.  Industrieller Einsatz von Trennwandkolonnen und thermisch gekoppelten Destillationskolonnen , 2003 .

[64]  Megan Jobson Dividing wall distillation comes of age , 2005 .

[65]  Qunxiong Zhu,et al.  Seeking synergistic effect- : A key principle in process intensification , 2007 .

[66]  Luis Puigjaner,et al.  Control and optimization of the divided wall column , 1999 .

[67]  Robin Smith,et al.  Operation and Control of Dividing Wall Distillation Columns: Part 1: Degrees of Freedom and Dynamic Simulation , 1998 .

[68]  Ilkka Turunen,et al.  A New Method for Synthesis of Thermodynamically Equivalent Structures for Petlyuk Arrangements , 2006 .

[69]  Juan Gabriel Segovia-Hernández,et al.  Thermodynamic analysis and hydrodynamic behavior of a reactive dividing wall distillation column , 2009 .

[70]  Helmut Jansen,et al.  UNFIXED DIVIDING WALL TECHNOLOGY FOR PACKED AND TRAY DISTILLATION COLUMNS , 2006 .