Effect of Pre-Heat-Treatment on Kinetics of Graphitization

it to 680•Ž in flowing nitrogen (PV-7). Four samples having different pre-heat-treatment conditions were selected; the original coke PV-7 , the second one prepared from PV-7 by the heat treatment at 1500•Ž for 60 min (PV-15) , the third also from PV-7 by the treatment at 2060•Ž for 60 min (PV-7-20) , and the fourth by the heat treatment of PV-15 at 2060•Ž for 60 min (PV-15-20). Each sample was heat-treated in a high purity graphite crucible at temperatures ranging from 1800•Ž to 2400•Ž for a variety of residence time under reduced