Mechanical Properties of Longmaxi Black Organic-Rich Shale Samples from South China under Uniaxial and Triaxial Compression States

With the exploitation of shale gas booming all over the world, more and more studies are focused on the core technology, hydraulic fracturing, to improve commercial exploitation. Shale gas resources in China are enormous. In this research, a series of tests were carried out with samples of black organic-rich shale from the Lower Silurian Longmaxi formation, south China. Samples were drilled from different directions and were subjected to uniaxial and triaxial condition with various confining pressures, aiming at studying its rock mechanics properties, so as to provide basis for research and breakthrough of hydraulic fracturing technology. According to the results of the study, the development and distribution of shale’s bedding planes significantly impact its mechanical properties. Shale samples show obvious brittle characteristics under low confining pressure, and its mechanical behavior begins to transform from brittle to plastic characteristics with increasing confining pressure. Shale samples with different inclinations (β) have different sensitivities to the confining pressure. As a result, samples with 45° inclinations (β) are least sensitive. The strength of bedding planes is significantly lower than that of shale matrix, and tensile failure and shear failure generally tend to occur along the bedding planes. When hydraulic fracturing was conducted in shale formation with depth less than 2.25 km, corresponding to original in-situ of 60 MPa, cracks will preferably occur at first along the inclination (β) angle of 45° from the maximum principal stress, and the failure mode is most likely to be shear failure without volumetric strain. And, different modes of failure will occur at different locations in the reservoir, depending on the orientation of bedding inclined from the principle stress, which can probably explain the phenomenon why there are fractures along and cross the bedding planes during hydraulic fracturing treatment. When hydraulic fracturing was conducted in shale formation with depth greater than 2.25 km, hydraulic fractures may not crack along the bedding surfaces to some extent.

[1]  Melanie J. Leng,et al.  Depositional Controls On Mudstone Lithofacies In A Basinal Setting: Implications for the Delivery of Sedimentary Organic Matter , 2014 .

[2]  J. B. Cheatham,et al.  A Three-Dimensional Anisotropic Yield Condition for Green River Shale , 1980 .

[3]  Liu Ruo-bing,et al.  Implications from Marine Shale Gas Exploration Breakthrough in Complicated Structural Area at High Thermal Stage: Taking Longmaxi Formation in Well JY1 as an Example , 2013 .

[4]  P. Wignall,et al.  Sedimentary dynamics of the Kimmeridge Clay: tempests and earthquakes , 1989, Journal of the Geological Society.

[5]  J. Macquaker,et al.  A lithofacies study of the Peterborough Member, Oxford Clay Formation (Jurassic), UK: an example of sediment bypass in a mudstone succession , 1994, Journal of the Geological Society.

[6]  T. Ramamurthy,et al.  Failure mechanism in schistose rocks , 1997 .

[7]  R. Holt,et al.  Brittleness of shales: Relevance to borehole collapse and hydraulic fracturing , 2015 .

[8]  M. H. B. Nasseri,et al.  Anisotropic strength and deformational behavior of Himalayan schists , 2003 .

[9]  Qiang Han,et al.  The mechanical properties of shale based on micro-indentation test , 2015 .

[10]  Andreas K. Kronenberg,et al.  Defomiation of Wilcox shale: Undrained strengths and effects of strain rate , 1994 .

[11]  Shicheng Zhang,et al.  Experimental study of hydraulic fracturing for shale by stimulated reservoir volume , 2014 .

[12]  Hanrong Zhang,et al.  Formation and enrichment mode of Jiaoshiba shale gas field, Sichuan Basin , 2014 .

[13]  Sarah J. Davies,et al.  Algal Blooms and “Marine Snow”: Mechanisms That Enhance Preservation of Organic Carbon in Ancient Fine-Grained Sediments , 2010 .

[14]  G. Pedersen,et al.  Thin, fine-grained storm layers in a muddy shelf sequence: an example from the Lower Jurassic in the Stenlille 1 well, Denmark , 1985, Journal of the Geological Society.

[15]  John A. Hudson,et al.  Estimating the transversely isotropic elastic intact rock properties for in situ stress measurement data reduction: A case study of the Olkiluoto mica gneiss, Finland , 2007 .

[16]  Feng Gao,et al.  Effect of the layer orientation on mechanics and energy evolution characteristics of shales under uniaxial loading , 2016 .

[17]  K. Bowker Barnett Shale gas production, Fort Worth Basin: Issues and discussion , 2007 .

[18]  R. Meehan,et al.  Strain rate effects in Kimmeridge bay shale , 1989 .

[19]  Kentaka Aruga,et al.  The U.S. Shale Gas Revolution and Its Effect on International Gas Markets , 2013 .

[20]  Guo Dong-xin,et al.  Shale gas favorable area prediction of the Qiongzhusi Formation and Longmaxi Formation of Lower Palaeozoic in Sichuan Basin,China , 2011 .

[21]  Fang Junhua,et al.  Characteristics and significance of mineral compositions of Lower Silurian Longmaxi Formation shale gas reservoir in the southern margin of Sichuan Basin , 2011 .

[22]  Erik Rybacki,et al.  What controls the mechanical properties of shale rocks? – Part II: Brittleness , 2016 .

[23]  Yuandong Zhang,et al.  A regional tectonic event of Katian (Late Ordovician) age across three major blocks of China , 2013 .

[24]  William T. Shea,et al.  Strength and anisotropy of foliated rocks with varied mica contents , 1993 .

[25]  Chen Xu,et al.  Facies patterns and geography of the Yangtze region, South China, through the Ordovician and Silurian transition , 2004 .

[26]  Desheng Hu,et al.  Opportunity, challenges and policy choices for China on the development of shale gas , 2013 .

[27]  Andreas K. Kronenberg,et al.  Experimental deformation of shale: mechanical properties and microstructural indicators of mechanisms , 1993 .

[28]  Ying Fan,et al.  The Impact of the North American Shale Gas Revolution on Regional Natural Gas Markets: Evidence from the Regime-Switching Model , 2016 .

[29]  Erik Rybacki,et al.  What controls the mechanical properties of shale rocks? – Part I: Strength and Young's modulus , 2015 .

[30]  J. E. Russell,et al.  Mechanical anisotropy of gneiss: Failure criterion and textural sources of directional behavior , 1990 .

[31]  M. E. Chenevert,et al.  Mechanical Anisotropies of Laminated Sedimentary Rocks , 1965 .

[32]  Olav-Magnar Nes,et al.  Static Vs. Dynamic Behavior of Shale , 2012 .

[33]  Stephen C. Ruppel,et al.  Mississippian Barnett Shale: Lithofacies and depositional setting of a deep-water shale-gas succession in the Fort Worth Basin, Texas , 2007 .

[34]  T. Guo,et al.  Evaluation of highly thermally mature shale-gas reservoirs in complex structural parts of the Sichuan Basin , 2013, Journal of Earth Science.

[35]  F. Donath EXPERIMENTAL STUDY OF SHEAR FAILURE IN ANISOTROPIC ROCKS , 1961 .

[36]  J. Schieber,et al.  7(e). Benthic microbial mats in black shale units from the Vindhyan Supergroup, Middle Proterozoic of India: the challenges of recognizing the genuine article , 2007 .

[37]  Seokwon Jeon,et al.  Deformation and strength anisotropy of Asan gneiss, Boryeong shale, and Yeoncheon schist , 2012 .

[38]  Haiyan Hu,et al.  Geochemistry and sedimentology of the Lower Silurian Longmaxi mudstone in southwestern China: Implications for depositional controls on organic matter accumulation , 2016 .

[39]  Bernhard M. Krooss,et al.  Shale Gas Potential of the Major Marine Shale Formations in the Upper Yangtze Platform, South China, Part III: Mineralogical, Lithofacial, Petrophysical, and Rock Mechanical Properties , 2014 .

[40]  Luke D. Connell,et al.  Experimental study of anisotropic gas permeability and its relationship with fracture structure of Longmaxi Shales, Sichuan Basin, China , 2016 .

[41]  K. Gray,et al.  The Mechanical Behavior of Anisotropic Sedimentary Rocks , 1967 .

[42]  Bo Zhang,et al.  Detrital quartz and quartz cement in Upper Triassic reservoir sandstones of the Sichuan basin: Characteristics and mechanisms of formation based on cathodoluminescence and electron backscatter diffraction analysis , 2012 .

[43]  James J. Hickey,et al.  Lithofacies summary of the Mississippian Barnett Shale, Mitchell 2 T.P. Sims well, Wise County, Texas , 2007 .

[44]  David A. T. Harper,et al.  The Global Boundary Stratotype Section and Point (GSSP) for the base of the Hirnantian Stage (the uppermost of the Ordovician System) , 2006 .