Investigation of a Monturaqui Impactite by Means of Bi-Modal X-ray and Neutron Tomography

X-ray and neutron tomography are applied as a bi-modal approach for the 3D characterisation of a Monturaqui impactite formed by shock metamorphism during the impact of an iron meteorite with the target rocks in the Monturaqui crater (Chile). The particular impactite exhibits structural heterogeneities on many length scales: its composition is dominated by silicate-based glassy and crystalline materials with voids and Fe/Ni-metal and oxihydroxides particles generally smaller than 1 mm in diameter. The non-destructive investigation allowed us to apply a novel bi-modal imaging approach that provides a more detailed and quantitative understanding of the structural and chemical composition compared to standard single mode imaging methods, as X-ray and neutron interaction with matter results in different attenuation coefficients with a non-linear relation. The X-ray and neutron data sets have been registered, and used for material segmentation, porosity and metallic content characterization. The bimodal data enabled the segmentation of a large number of different materials, their morphology as well as distribution in the specimen including the quantification of volume fractions. The 3D data revealed an evaporite type of material in the impactite not noticed in previous studies. The present study is exemplary in demonstrating the potential for non-destructive characterisation of key features of complex multi-phase objects such as impactites.

[1]  Veerle Cnudde,et al.  High-resolution X-ray computed tomography in geosciences: A review of the current technology and applications , 2013 .

[2]  J. Banhart Advanced tomographic methods in materials research and engineering , 2008 .

[3]  N. Otsu A threshold selection method from gray level histograms , 1979 .

[4]  Donald E. Brownlee,et al.  Metal spherules in Wabar, Monturaqui, and Henbury impactites. [iron meteorites] , 1976 .

[5]  Timothy B. Rowe,et al.  First Early Cretaceous mammal from the eastern seaboard of the United States , 1999 .

[6]  Bernd Milkereit,et al.  An integrated geophysical and geological study of the Monturaqui impact crater, Chile , 2007 .

[7]  D. Jacobson,et al.  Neutron and X-ray Tomography (NeXT) system for simultaneous, dual modality tomography. , 2017, The Review of scientific instruments.

[8]  P. McMillan,et al.  X–ray and neutron diffraction studies and MD simulation of atomic configurations in polyamorphic Y2O3-Al2O3 systems , 2005, Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences.

[9]  A. Cormack Representation of a Function by Its Line Integrals, with Some Radiological Applications , 1963 .

[10]  G. Hounsfield Computerized transverse axial scanning (tomography): Part I. Description of system. 1973. , 1973, The British journal of radiology.

[11]  William Cassidy,et al.  A previously undescribed meteorite crater in Chile , 1966 .

[12]  Christian Koeberl,et al.  The convincing identification of terrestrial meteorite impact structures: What works, what doesn't, and why , 2010 .

[13]  W. Goodfellow,et al.  Use of platinum-group elements for impactor identification: Terrestrial impact craters and Cretaceous-Tertiary boundary , 1993 .

[14]  Bjoern Winkler,et al.  Applications of Neutron Radiography and Neutron Tomography , 2006 .

[15]  J. Vlassenbroeck,et al.  A comparative and critical study of X-ray CT and neutron CT as non-destructive material evaluation techniques , 2007, Geological Society, London, Special Publications.

[16]  G. Bonino,et al.  The 11-year solar cycle variation of cosmogenic isotope production rates in chondrites , 1994 .

[17]  Paul A. Viola,et al.  Alignment by Maximization of Mutual Information , 1997, International Journal of Computer Vision.

[18]  Guy Marchal,et al.  Automated multi-modality image registration based on information theory , 1995 .

[19]  Daniel Owen Cukierski,et al.  Textural and compositional analysis of Fe-Ni metallic spherules in impact melt from Monturaqui Crater, Chile , 2013 .

[20]  Colin Studholme,et al.  An overlap invariant entropy measure of 3D medical image alignment , 1999, Pattern Recognit..

[21]  John Banhart,et al.  Advances in neutron radiography and tomography , 2009 .

[22]  Helen Ashton,et al.  Metamorphic Rocks: A Classification and Glossary of Terms , 2008 .

[23]  R. Brett,et al.  Metallic spherules in impactite and tektite glasses , 1966 .

[24]  Stan Z. Li,et al.  Markov Random Field Modeling in Image Analysis , 2001, Computer Science Workbench.

[25]  A. Mather,et al.  150 million years of climatic stability: evidence from the Atacama Desert, northern Chile , 2005, Journal of the Geological Society.

[26]  Johannes E. Schindelin,et al.  Fiji: an open-source platform for biological-image analysis , 2012, Nature Methods.

[27]  M. A. Fiddy,et al.  The Radon Transform and Some of Its Applications , 1985 .

[28]  J. Ross,et al.  Annotated bibliography. , 1994, AJNR. American journal of neuroradiology.

[29]  Ron Jenkins,et al.  Introduction to X-ray powder diffractometry , 1996 .

[30]  T. Bunch,et al.  Petrographic and electron microprobe study of the Monturaqui impactite , 1972 .

[31]  Sylvain Désert,et al.  IMAGINE: A Cold Neutron Imaging Station at the Laboratoire Léon Brillouin , 2015 .

[32]  Nathalie A. Cabrol,et al.  A Novel Application of (U-Th)/He Geochronology to Constrain the Age of Small, Young Meteorite Impact Craters: A Case Study of the Monturaqui Crater, Chile , 2010 .

[33]  S. Deans The Radon Transform and Some of Its Applications , 1983 .

[34]  M. Colbert,et al.  Applications of high-resolution X-ray computed tomography in petrology, meteoritics and palaeontology , 2003, Geological Society, London, Special Publications.

[35]  Anders Kaestner,et al.  Bimodal Imaging at ICON Using Neutrons and X-rays , 2017 .

[36]  Matthias Ebert,et al.  Chemical projectile–target interaction and liquid immiscibility in impact glass from the Wabar craters, Saudi Arabia , 2012 .

[37]  Veerle Cnudde,et al.  High-speed neutron tomography of dynamic processes , 2005 .

[38]  David J. Hawkes,et al.  X-ray attenuation coefficients of elements and mixtures , 1981 .

[39]  Christine Marie Kloberdanz,et al.  Geochemical analysis of the Monturaqui impact crater, Chile , 2010 .

[40]  Hideyasu Kojima,et al.  Terrestrial alteration of Fe-Ni metals in Antarctic ordinary chondrites and the relationship to their terrestrial ages , 1991 .

[41]  Anton T. Kearsley,et al.  Early fracturing and impact residue emplacement: Can modelling help to predict their location in major craters? , 2004 .

[42]  Thomas Kenkmann,et al.  Chemical modification of projectile residues and target material in a MEMIN cratering experiment , 2013 .