Study on the Grain Rotation of High-Purity Tantalum during Compression Deformation

A compression experiment with electron backscatter diffraction (EBSD) measurements was designed to characterize the effect of the microtexture on the grain rotation process. The rotation degrees of more than 180 grains before and after the compression were calculated. Results showed that grains with different crystallographic orientations experienced various rotation degrees. Furthermore, grains in certain microtexture regions also had varying degrees of rotation. The compression led to the lattice rotation and change in orientation of individual grains, but the relative misorientation between grains has not changed much in the microtexture region. The microtexture region, as a whole, participated in the compression process. The similar slipping behavior of the grains in the region promoted the slip transmission between the neighboring grains. Thus, the amount of piled-up dislocations at grain boundaries inside the microtexture region are less than that at grain boundaries outside the microtexture region, leading to a small stored energy density for grain boundaries inside the microtexture region.

[1]  Zhiyong Chen,et al.  Deformation mechanism, orientation evolution and mechanical properties of annealed cross-rolled Mg-Zn-Zr-Y-Gd sheet during tension , 2021, Journal of Magnesium and Alloys.

[2]  S. Chandrasekar,et al.  Cutting of tantalum: Why it is so difficult and what can be done about it , 2020 .

[3]  F. Dunne,et al.  A crystal plasticity investigation of slip system interaction, GND density and stored energy in non-proportional fatigue in Nickel-based superalloy , 2020 .

[4]  S. Simões,et al.  Recent Advances in EBSD Characterization of Metals , 2020, Metals.

[5]  Shi-feng Liu,et al.  Effect of strain path change on the through-thickness microstructure during tantalum rolling , 2020 .

[6]  Guoqun Zhao,et al.  Evolution of grain structure, micro-texture and second phase during porthole die extrusion of Al–Zn–Mg alloy , 2019 .

[7]  W. Ding,et al.  Towards high ductility in magnesium alloys - The role of intergranular deformation , 2019 .

[8]  Shi-feng Liu,et al.  Orientation-dependent grain boundary characteristics in tantalum upon the change of strain path , 2019, Materials Characterization.

[9]  A. Teverovsky Effect of Moisture on AC Characteristics of Chip Polymer Tantalum Capacitors , 2019, IEEE Transactions on Components, Packaging and Manufacturing Technology.

[10]  T. Langdon,et al.  Processing Magnesium and Its Alloys by High‐Pressure Torsion: An Overview , 2018, Advanced Engineering Materials.

[11]  Shi-feng Liu,et al.  Inhomogeneous deformation of {111} grain in cold rolled tantalum , 2018, Journal of Materials Science & Technology.

[12]  Q. Liu,et al.  Strain path dependence of microstructure and annealing behavior in high purity tantalum , 2017 .

[13]  Y. Ikuhara,et al.  Direct observation of individual dislocation interaction processes with grain boundaries , 2016, Science Advances.

[14]  K. Hagihara,et al.  Electron backscatter diffraction pattern analysis of the deformation band formed in the Mg-based long-period stacking ordered phase , 2016 .

[15]  B. Cui,et al.  Dislocation Grain Boundary Interactions in Irradiated Metals , 2016 .

[16]  H. Y. Fan,et al.  Elimination of Elongated Bands by Clock Rolling in High-Purity Tantalum , 2015, Metallurgical and Materials Transactions A.

[17]  T. Bieler,et al.  Grain boundaries and interfaces in slip transfer , 2014 .

[18]  Shi-feng Liu,et al.  A comparative study of clock rolling and unidirectional rolling on deformation/recrystallization microstructure and texture of high purity tantalum plates , 2013 .

[19]  Bert Verlinden,et al.  Deformation banding in a Nb polycrystal deformed by successive compression tests , 2012 .

[20]  A. Najafizadeh,et al.  Flow stress analysis of TWIP steel via the XRD measurement of dislocation density , 2010 .

[21]  A. Martínez-de-Guerenu,et al.  Effect of stored energy and recovery on the overall recrystallization kinetics of a cold rolled low carbon steel , 2008 .

[22]  C. Wickersham,et al.  Effect of grain orientation on tantalum magnetron sputtering yield , 2006 .

[23]  J. Mendez,et al.  Analysis of the different slip systems activated by tension in a α/β titanium alloy in relation with local crystallographic orientation , 2005 .

[24]  S. Schmidt,et al.  Lattice rotations of individual bulk grains Part II: correlation with initial orientation and model comparison , 2004 .

[25]  S. Choi,et al.  Evaluation of stored energy in cold-rolled steels from EBSD data , 2004 .

[26]  C. A. Michaluk Correlating discrete orientation and grain size to the sputter deposition properties of tantalum , 2002 .

[27]  H. Poulsen,et al.  In Situ Measurement of Grain Rotation During Deformation of Polycrystals , 2001, Science.

[28]  A. Wilkinson,et al.  Quantitative deformation studies using electron back scatter patterns , 1991 .