Characterization of hot deformation behavior of extruded ZK60 magnesium alloy using 3D processing maps

Abstract The hot deformation behavior of extruded ZK60 magnesium alloy was investigated by compression tests in the temperature range of 250–400 °C and strain rate range of 0.001–1 s−1. In order to describe the flow characteristics, a constitutive equation was developed and the deformation activation energy was estimated to be 126.31 kJ/mol. The three-dimensional (3D) processing maps were established on the basis of experimental data as a function of temperature, strain rate and strain. According to the 3D processing maps, it can be found that the strain has a significant influence on the efficiency of power dissipation and the regions of flow instability. From the 3D power dissipation map, one domain of dynamic recrystallization (DRX) and the other domain of superplasticity were identified and the flow instability regions were distinguished from the 3D instability map. By means of user subroutines, the 3D processing maps were integrated into the commercial finite element (FE) software MSC.Marc and the distributions of the flow instability region during processing can be predicted. In addition, the processing maps of extruded ZK60 alloy have been compared with those of as-cast alloy, which demonstrates that the hot extrusion process improves the workability of the alloy.

[1]  Z. Cui,et al.  Analysis of metal workability by integration of FEM and 3-D processing maps , 2008 .

[2]  Rong Wang,et al.  Hot deformation and processing map of as-homogenized Mg–9Gd–3Y–2Zn–0.5Zr alloy , 2013 .

[3]  Y. Lin,et al.  Modeling of flow stress of 42CrMo steel under hot compression , 2009 .

[4]  T. Mukai,et al.  Application of superplasticity in commercial magnesium alloy for fabrication of structural components , 2000 .

[5]  S. Murty,et al.  Instability map for hot working of 6061 Al-10 vol% metal matrix composite , 1998 .

[6]  S. Murty,et al.  On the development of instability criteria during hotworking with reference to IN 718 , 1998 .

[7]  Ying Wang,et al.  Hot deformation and processing maps of X-750 nickel-based superalloy , 2013 .

[8]  S. Spigarelli,et al.  Analysis of high-temperature deformation and microstructure of an AZ31 magnesium alloy , 2007 .

[9]  G. Gottstein,et al.  Correlation of plastic deformation and dynamic recrystallization in magnesium alloy ZK60 , 2001 .

[10]  Z. Gronostajski Deformation processing map for control of CuSi4.6 silicon bronze microstructure , 2005 .

[11]  Jie Zhou,et al.  Hot workability analysis of extruded AZ magnesium alloys with processing maps , 2010 .

[12]  S. M. Doraivelu,et al.  Modeling of dynamic material behavior in hot deformation: Forging of Ti-6242 , 1984 .

[13]  T. Kobayashi,et al.  Grain-Boundary Sliding in AZ31 Magnesium Alloys at Room Temperature to 523 K , 2003 .

[14]  K. P. Rao,et al.  Hot working behavior and processing map of a γ-TiAl alloy synthesized by powder metallurgy , 2011 .

[15]  K. P. Rao,et al.  Hot workability characteristics of cast and homogenized Mg–3Sn–1Ca alloy , 2008 .

[16]  S. Ramanathan,et al.  Hot deformation and processing maps of extruded ZE41A magnesium alloy , 2010 .

[17]  Xiaoqing Xu,et al.  Characterization of hot deformation behavior of a Zn–10.2Al–2.1Cu alloy using processing maps , 2012 .

[18]  Yu Sun,et al.  Characterization of hot deformation behavior of as-cast TC21 titanium alloy using processing map , 2011 .

[19]  Ali A. Roostaei,et al.  Constitutive base analysis of a 7075 aluminum alloy during hot compression testing , 2011 .

[20]  Y. Prasad,et al.  Characteristics of superplasticity domain in the processing map for hot working of as-cast Mg-11.5Li-1.5Al alloy , 2002 .

[21]  R. Raj Development of a Processing Map for Use in Warm-Forming and Hot-Forming Processes , 1981 .

[22]  V. Senthilkumar,et al.  Analysis of hot deformation behavior of Al 5083–TiC nanocomposite using constitutive and dynamic material models , 2012 .

[23]  Kozo Osakada,et al.  Forming limit of magnesium alloy at elevated temperatures for precision forging , 2002 .

[24]  S. N. Narayana Murty,et al.  Instability criteria for hot deformation of materials , 2000 .

[25]  F. Moret,et al.  Numerical modeling of powder metallurgy processes , 2000 .

[26]  W. Ding,et al.  Study of the microstructure, texture and tensile properties of as-extruded AZ91 magnesium alloy , 2008 .

[27]  Jie Zhou,et al.  Identification of optimal deforming parameters from a large range of strain, strain rate and temperature for 3Cr20Ni10W2 heat-resistant alloy , 2013 .

[28]  Y. V. R. K. Prasad,et al.  Processing maps: A status report , 2003 .

[29]  V. Balasubramanian,et al.  Feasibility of joining AZ31B magnesium metal matrix composite by friction welding , 2011 .

[30]  B. Mordike,et al.  Magnesium: Properties — applications — potential , 2001 .

[31]  F. J. Humphreys,et al.  Dynamic recrystallisation and the development of microstructure during the high temperature deformation of magnesium , 1982 .

[32]  Kun Wu,et al.  Processing maps for hot working of ZK60 magnesium alloy , 2007 .

[33]  Y. Prasad,et al.  Hot deformation behaviour of Mg–3Al alloy—A study using processing map , 2008 .

[34]  K. P. Rao,et al.  Hot Deformation Mechanisms and Microstructural Control in High‐Temperature Extruded AZ31 Magnesium Alloy , 2007 .

[35]  Qi Li,et al.  Hot workability characteristics of magnesium alloy AZ80—A study using processing map , 2010 .

[36]  V. Senthilkumar,et al.  Study on hot deformation behavior and microstructure evolution of cast-extruded AZ31B magnesium alloy and nanocomposite using processing map , 2013 .

[37]  Fuguo Li,et al.  Development and validation of a processing map for Aermet100 steel , 2010 .