Mycotoxins in cereals and related foodstuffs: A review on occurrence and recent methods of analysis

[1]  Fluorescence Polarization Immunoassay of Mycotoxins: A Review , 2009, Toxins.

[2]  A. Gomaa,et al.  Validation of analytical method for determination of ochratoxin A in cereals by C 18 solid phase extraction and high-performance liquid chromatography with fluorescence detection , 2008 .

[3]  S. Chiacchiera,et al.  Occurrence of Fusarium spp. and fumonisin in durum wheat grains. , 2011, Journal of agricultural and food chemistry.

[4]  M. Savard.  Deoxynivalenol fatty acid and glucoside conjugates , 1991 .

[5]  N. H. Spliid,et al.  Occurrence of different trichothecenes and deoxynivalenol-3-β-d-glucoside in naturally and artificially contaminated Danish cereal grains and whole maize plants , 2012, Mycotoxin Research.

[6]  S. Cunha,et al.  Development and validation of a method based on a QuEChERS procedure and heart-cutting GC-MS for determination of five mycotoxins in cereal products. , 2010, Journal of separation science.

[7]  Z. Kunsági,et al.  Quantification of T-2 and HT-2 mycotoxins in cereals by liquid chromatography-multimode ionization-tandem mass spectrometry , 2012 .

[8]  Wong Chee Seng.  QuEChERS extraction and HPLC-FLD determination of Ochratoxin A in cereals and cereal Products. , 2012 .

[9]  G. Engelhardt,et al.  Occurrence of Zearalenone-4-β-d-glucopyranoside in Wheat , 2002 .

[10]  Z. Usman,et al.  Natural occurrence of ochratoxin A in some marketed Nigerian foods , 2013 .

[11]  L. Rastrelli,et al.  Application of dispersive liquid-liquid microextraction for the determination of aflatoxins B1, B2, G1 and G2 in cereal products. , 2011, Journal of chromatography. A.

[12]  C. Juan,et al.  Determination of trichothecenes and zearalenones in grain cereal, flour and bread by liquid chromatography tandem mass spectrometry. , 2012, Food chemistry.

[13]  Veronica M T Lattanzio,et al.  Identification and characterization of new Fusarium masked mycotoxins, T2 and HT2 glycosyl derivatives, in naturally contaminated wheat and oats by liquid chromatography-high-resolution mass spectrometry. , 2012, Journal of mass spectrometry : JMS.

[14]  D. Parent-Massin,et al.  Co-exposure of Fusarium mycotoxins: in vitro myelotoxicity assessment on human hematopoietic progenitors. , 2012, Toxicon : official journal of the International Society on Toxinology.

[15]  Jingao Dong,et al.  Occurrence of major mycotoxins in maize from Hebei Province, China , 2011 .

[16]  M. Spiteller,et al.  Multi-mycotoxin analysis in complex biological matrices using LC-ESI/MS: experimental study using triple stage quadrupole and LTQ-Orbitrap. , 2009, Journal of separation science.

[17]  J. Hajšlová,et al.  Transfer of Fusarium mycotoxins and ‘masked’ deoxynivalenol (deoxynivalenol-3-glucoside) from field barley through malt to beer , 2008, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[18]  Selamat Jinap,et al.  Qualitative and Quantitative Analysis of Mycotoxins. , 2009, Comprehensive reviews in food science and food safety.

[19]  S. Saeger,et al.  Natural occurrence of mycotoxins and their masked forms in food and feed products , 2012 .

[20]  C. Gottschalk,et al.  Occurrence of type A, B and D trichothecenes in barley and barley products from the Bavarian market , 2012, Mycotoxin Research.

[21]  M. Pascale,et al.  Detection methods for mycotoxins in cereal grains and cereal products , 2009 .

[22]  G. Font,et al.  Pressurized liquid extraction followed by liquid chromatography–mass spectrometry for determination of zearalenone in cereal flours , 2010 .

[23]  Pascal Mottier,et al.  Development and comparison of two multiresidue methods for the analysis of 17 mycotoxins in cereals by liquid chromatography electrospray ionization tandem mass spectrometry. , 2010, Journal of agricultural and food chemistry.

[24]  S. Hoth,et al.  Survey of T-2 and HT-2 toxins by LC–MS/MS in oats and oat products from European oat mills in 2005–2009 , 2011, Food additives & contaminants. Part B, Surveillance.

[25]  M. Spanjer,et al.  LC–MS/MS multi-method for mycotoxins after single extraction, with validation data for peanut, pistachio, wheat, maize, cornflakes, raisins and figs , 2008, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[26]  M. Busman,et al.  Rapid and advanced tools for mycotoxin analysis: a review , 2010, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[27]  E. Ferrer,et al.  Emerging Fusarium mycotoxins in organic and conventional pasta collected in Spain. , 2013, Food and chemical toxicology : an international journal published for the British Industrial Biological Research Association.

[28]  Xing-Fang Li,et al.  Liquid chromatography-electrospray mass spectrometric studies of ginkgolides and bilobalide using simultaneous monitoring of proton, ammonium and sodium adducts. , 2002, The Analyst.

[29]  I. Ferreira,et al.  Optimization and validation of a method based in a QuEChERS procedure and gas chromatography–mass spectrometry for the determination of multi-mycotoxins in popcorn , 2012 .

[30]  M. Suman,et al.  Development and validation of a liquid chromatography/linear ion trap mass spectrometry method for the quantitative determination of deoxynivalenol-3-glucoside in processed cereal-derived products. , 2013, Food chemistry.

[31]  S. Tran,et al.  Determination of optimal conditions for hydrolysis of conjugated deoxynivalenol in corn and wheat with trifluoromethanesulfonic acid , 2011 .

[32]  M. Castillo,et al.  Trichothecenes in breakfast cereals from the Spanish retail market , 2012 .

[33]  Trevor K. Smith,et al.  A survey of free and conjugated deoxynivalenol in the 2008 corn crop in Ontario, Canada. , 2012, Journal of the science of food and agriculture.

[34]  S. Barker.  Matrix solid phase dispersion (MSPD). , 2007, Journal of biochemical and biophysical methods.

[35]  Yongjiang Wu,et al.  Simultaneous determination of 10 mycotoxins in grain by ultra-high-performance liquid chromatography–tandem mass spectrometry using 13C15-deoxynivalenol as internal standard , 2010, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[36]  Tim Smyth,et al.  Safety and quality. , 2002, Australian health review : a publication of the Australian Hospital Association.

[37]  C. V. Van Peteghem,et al.  A validated multianalyte LC-MS/MS method for quantification of 25 mycotoxins in cassava flour, peanut cake and maize samples. , 2011, Journal of agricultural and food chemistry.

[38]  S. Jinap,et al.  Determination of mycotoxins in cereals by liquid chromatography tandem mass spectrometry , 2012 .

[39]  C. Cavaliere,et al.  Determination of type B trichothecenes and macrocyclic lactone mycotoxins in field contaminated maize , 2005 .

[40]  W. Kong,et al.  Analysis of zearalenone and α-zearalenol in 100 foods and medicinal plants determined by HPLC-FLD and positive confirmation by LC-MS-MS. , 2013, Journal of the science of food and agriculture.

[41]  S. Marín,et al.  Occurrence of deoxynivalenol in durum wheat from Morocco , 2013 .

[42]  Rudolf Krska,et al.  Quantitation of mycotoxins in food and feed from Burkina Faso and Mozambique using a modern LC-MS/MS multitoxin method. , 2012, Journal of agricultural and food chemistry.

[43]  V. Gerbi,et al.  Quantification by solid phase micro extraction and stable isotope dilution assay of norisoprenoid compounds in red wines obtained from Piedmont rare varieties. , 2012, Food chemistry.

[44]  S. Jinap,et al.  SIMULTANEOUS DETERMINATION OF AFLATOXINS, OCHRATOXIN A, AND ZEARALENONE IN CEREALS USING A VALIDATED RP-HPLC METHOD AND PHRED DERIVATIZATION SYSTEM , 2013 .

[45]  Somenath Mitra,et al.  Sample preparation techniques in analytical chemistry , 2003 .

[46]  J. Pleadin,et al.  CORRELATION OF DEOXYNIVALENOL AND FUMONISIN CONCENTRATION DETERMINED IN MAIZE BY ELISA METHODS , 2012, Journal of immunoassay & immunochemistry.

[47]  C. Hummert,et al.  Analysis of Fusarium Toxins Using LC-MS-MS: Application to Various Food and Feed Matrices , 2004 .

[48]  J. Rubert,et al.  Application of an HPLC–MS/MS method for mycotoxin analysis in commercial baby foods , 2012 .

[49]  R. Krska,et al.  Mycotoxins and fungal metabolites in groundnut- and maize-based snacks from Nigeria , 2013, Food additives & contaminants. Part B, Surveillance.

[50]  I. K. Cigić,et al.  An Overview of Conventional and Emerging Analytical Methods for the Determination of Mycotoxins , 2009, International journal of molecular sciences.

[51]  Rudolf Krska,et al.  Rapid test strips for analysis of mycotoxins in food and feed , 2009, Analytical and bioanalytical chemistry.

[52]  J. Hajšlová,et al.  Effects of milling and baking technologies on levels of deoxynivalenol and its masked form deoxynivalenol-3-glucoside. , 2011, Journal of agricultural and food chemistry.

[53]  V. Lattanzio,et al.  Simultaneous determination of aflatoxins, ochratoxin A and Fusarium toxins in maize by liquid chromatography/tandem mass spectrometry after multitoxin immunoaffinity cleanup. , 2007, Rapid communications in mass spectrometry : RCM.

[54]  S. Patel,et al.  Deoxynivalenol and other Fusarium mycotoxins in bread, cake, and biscuits produced from UK-grown wheat under commercial and pilot scale conditions , 2009 .

[55]  S. Piletsky,et al.  Analytical methods for determination of mycotoxins: a review. , 2009, Analytica chimica acta.

[56]  V. Rossi.  Pest risk assessment of Monilinia fructicola for the EU territory and identification and evaluation of risk management options , 2011 .

[57]  M. Masrournia,et al.  Fabrication of a novel nanocomposite based on sol-gel process for hollow fiber-solid phase microextraction of aflatoxins: B1 and B2, in cereals combined with high performane liquid chromatography-diode array detection. , 2011, Journal of chromatography. B, Analytical technologies in the biomedical and life sciences.

[58]  M. Ibáñez,et al.  Determination of mycotoxins in different food commodities by ultra-high-pressure liquid chromatography coupled to triple quadrupole mass spectrometry. , 2009, Rapid communications in mass spectrometry : RCM.

[59]  F. Berthiller,et al.  Masked mycotoxins: A review , 2012, Molecular nutrition & food research.

[60]  M. Das,et al.  Occurrence of deoxynivalenol in cereals and exposure risk assessment in Indian population , 2013 .

[61]  V. Lattanzio,et al.  Current analytical methods for trichothecene mycotoxins in cereals , 2009 .

[62]  G. Cano-Sancho,et al.  Determination of aflatoxins, deoxynivalenol, ochratoxin A and zearalenone in wheat and oat based bran supplements sold in the Spanish market. , 2013, Food and chemical toxicology : an international journal published for the British Industrial Biological Research Association.

[63]  I. Chianella,et al.  Use of itaconic acid-based polymers for solid-phase extraction of deoxynivalenol and application to pasta analysis. , 2008, Analytica chimica acta.

[64]  G. He,et al.  Doehlert matrix design for optimization of the determination of bound deoxynivalenol in barley grain with trifluoroacetic acid (TFA). , 2007, Journal of agricultural and food chemistry.

[65]  S. de Saeger,et al.  Development and validation of a QuEChERS based liquid chromatography tandem mass spectrometry method for the determination of multiple mycotoxins in spices. , 2013, Journal of chromatography. A.

[66]  R. Krska,et al.  Application of an LC-MS/MS based multi-mycotoxin method for the semi-quantitative determination of mycotoxins occurring in different types of food infected by moulds. , 2010 .

[67]  Rudolf Krska,et al.  Stable isotope dilution assay for the accurate determination of mycotoxins in maize by UHPLC-MS/MS , 2012, Analytical and Bioanalytical Chemistry.

[68]  C. Pan,et al.  A review of sample preparation methods for the pesticide residue analysis in foods , 2012 .

[69]  E. Ferrer,et al.  Co-occurrence and risk assessment of mycotoxins in food and diet from Mediterranean area. , 2012, Food chemistry.

[70]  M. Zón,et al.  Novel Studies about the Electrooxidation of a Deoxynivalenol (DON) Mycotoxin Reduction Product Adsorbed on Glassy Carbon and Carbon Paste Electrodes , 2008 .

[71]  Elena Lizarraga,et al.  Simultaneous determination of type-A and type-B trichothecenes in barley samples by GC-MS , 2011 .

[72]  S. Cunha,et al.  Sample Preparation Approaches for the Analysis of Pesticide Residues in Olives and Olive Oils , 2010 .

[73]  S. Jinap,et al.  Optimisation of the determination of deoxynivalenol in wheat flour by HPLC and a comparison of four clean-up procedures , 2009 .

[74]  A. G. Frenich,et al.  Simple and high-throughput method for the multimycotoxin analysis in cereals and related foods by ultra-high performance liquid chromatography/tandem mass spectrometry , 2009 .

[75]  R. Krska,et al.  Simultaneous determination of deoxynivalenol, zearalenone, and their major masked metabolites in cereal-based food by LC–MS–MS , 2009, Analytical and bioanalytical chemistry.

[76]  S. Cunha,et al.  Multipesticide residue analysis in maize combining acetonitrile-based extraction with dispersive liquid-liquid microextraction followed by gas chromatography-mass spectrometry. , 2011, Journal of chromatography. A.

[77]  Antonio V. Herrera-Herrera,et al.  Dispersive Solid‐Phase Extraction , 2015 .

[78]  J. Smedsgaard,et al.  Multi-mycotoxin analysis of maize silage by LC-MS/MS , 2010, Analytical and bioanalytical chemistry.

[79]  R. Krska,et al.  Liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS) determination of phase II metabolites of the mycotoxin zearalenone in the model plant Arabidopsis thaliana , 2006, Food additives and contaminants.

[80]  Michele Suman,et al.  Fluorescence Polarization Immunoassay for Rapid, Accurate and Sensitive Determination of Ochratoxin A in Wheat , 2014, Food Analytical Methods.

[81]  R. Cooks,et al.  Orbitrap mass spectrometry: instrumentation, ion motion and applications. , 2008, Mass spectrometry reviews.

[82]  J. Rubert,et al.  Evaluation of matrix solid-phase dispersion (MSPD) extraction for multi-mycotoxin determination in different flours using LC-MS/MS. , 2011, Talanta.

[83]  F. Ricci,et al.  Current methods of analysis for the determination of trichothecene mycotoxins in food , 2011 .

[84]  C. Delerue-Matos,et al.  Extraction of ochratoxin A in bread samples by the QuEChERS methodology. , 2012, Food chemistry.

[85]  Steven J Lehotay,et al.  Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce. , 2003, Journal of AOAC International.

[86]  A. Ritieni,et al.  Fungal diversity and natural occurrence of fusaproliferin, beauvericin, deoxynivalenol and nivalenol in wheat cultivated in Santa Fe Province, Argentina , 2010, Mycotoxin Research.

[87]  M. A. Mohd,et al.  Advanced Gas Chromatography - Progress in Agricultural, Biomedical and Industrial Applications , 2012 .

[88]  G. Engelhardt,et al.  Simultaneous determination of type A, B and D trichothecenes and their occurrence in cereals and cereal products , 2009 .

[89]  G. Tan,et al.  SIMULTANEOUS DETECTION OF TYPE A AND TYPE B TRICHOTHECENES IN CEREALS BY LIQUID CHROMATOGRAPHY COUPLED WITH ELECTROSPRAY IONIZATION QUADRUPOLE TIME OF FLIGHT MASS SPECTROMETRY (LC-ESI-QTOF-MS/MS) , 2012 .

[90]  An Fao Perspective.  WORLD AGRICULTURE : TOWARDS 2015/2030 , 2015 .

[91]  Rudolf Krska,et al.  A liquid chromatography/tandem mass spectrometric multi-mycotoxin method for the quantification of 87 analytes and its application to semi-quantitative screening of moldy food samples , 2007, Analytical and bioanalytical chemistry.

[92]  Josep Rubert,et al.  Analysis of mycotoxins in barley using ultra high liquid chromatography high resolution mass spectrometry: comparison of efficiency and efficacy of different extraction procedures. , 2012, Talanta.

[93]  R. Krska,et al.  Occurrence of free and conjugated Fusarium mycotoxins in cereal-based food , 2010, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[94]  D. Centonze,et al.  Determination of aflatoxins in cereal flours by solid-phase microextraction coupled with liquid chromatography and post-column photochemical derivatization-fluorescence detection. , 2009, Journal of chromatography. A.

[95]  Rudolf Krska,et al.  Determination of multi-mycotoxin occurrence in cereals, nuts and their products in Cameroon by liquid chromatography tandem mass spectrometry (LC-MS/MS) , 2013 .

[96]  M. Pojić,et al.  Near Infrared Spectroscopy—Advanced Analytical Tool in Wheat Breeding, Trade, and Processing , 2013, Food and Bioprocess Technology.

[97]  J. Ma,et al.  Natural occurrence of masked deoxynivalenol in Chinese wheat and wheat-based products during 2008-2011 , 2012 .

[98]  S. Patel,et al.  Occurrence of Fusarium mycotoxins in maize imported into the UK, 2004–2007 , 2009, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[99]  R. Köppen,et al.  Development and certification of a reference material for Fusarium mycotoxins in wheat flour , 2013, Analytical and Bioanalytical Chemistry.

[100]  Mohammad Rezaee,et al.  Evolution of dispersive liquid-liquid microextraction method. , 2010, Journal of chromatography. A.

[101]  R. Krska,et al.  Rapid simultaneous determination of major type A- and B-trichothecenes as well as zearalenone in maize by high performance liquid chromatography-tandem mass spectrometry. , 2005, Journal of chromatography. A.

[102]  R. Krska,et al.  Masked mycotoxins: determination of a deoxynivalenol glucoside in artificially and naturally contaminated wheat by liquid chromatography-tandem mass spectrometry. , 2005, Journal of agricultural and food chemistry.

[103]  Ian D. Wilson,et al.  Encyclopedia of separation science , 2000 .

[104]  S. Lehotay,et al.  Validation of a fast and easy method for the determination of residues from 229 pesticides in fruits and vegetables using gas and liquid chromatography and mass spectrometric detection. , 2005, Journal of AOAC International.

[105]  H. Mol,et al.  Toward a generic extraction method for simultaneous determination of pesticides, mycotoxins, plant toxins, and veterinary drugs in feed and food matrixes. , 2008, Analytical chemistry.

[106]  A. Ariño,et al.  Aflatoxin contamination in different fractions of rice from Pakistan and estimation of dietary intakes , 2012, Mycotoxin Research.

[107]  Liberty Sibanda,et al.  Lateral-flow colloidal gold-based immunoassay for the rapid detection of deoxynivalenol with two indicator ranges. , 2008, Analytica chimica acta.

[108]  J. Gilbert,et al.  Mycotoxins and Phycotoxins , 1998 .

[109]  G. Font,et al.  Further data on the levels of emerging Fusarium mycotoxins enniatins (A, A1, B, B1), beauvericin and fusaproliferin in breakfast and infant cereals from Morocco , 2011 .

[110]  T. Rundberget,et al.  Instrumental methods for determination of nonmacrocyclic trichothecenes in cereals, foodstuffs and cultures , 1998 .

[111]  J. Seeley,et al.  Recent advances in flow-controlled multidimensional gas chromatography. , 2012, Journal of chromatography. A.

[112]  Pierluigi Meriggi,et al.  Dynamics of fungi and related mycotoxins during cereal storage in silo bags , 2013 .

[113]  Jana Šandrejová,et al.  Recent advances in dispersive liquid–liquid microextraction using organic solvents lighter than water. A review , 2012 .

[114]  G. Shephard,et al.  Preliminary exposure assessment of deoxynivalenol and patulin in South Africa , 2010, Mycotoxin Research.

[115]  Á. Ríos,et al.  Supercritical fluid extraction of macrocyclic lactone mycotoxins in maize flour samples for rapid amperometric screening and alternative liquid chromatographic method for confirmation. , 2008, Journal of chromatography. A.

[116]  Hong Zhang,et al.  Development of a microwave-assisted-extraction-based method for the determination of aflatoxins B1, G1, B2, and G2 in grains and grain products , 2013, Analytical and Bioanalytical Chemistry.

[117]  J. Hajšlová,et al.  Deoxynivalenol, deoxynivalenol-3-glucoside, and enniatins: the major mycotoxins found in cereal-based products on the Czech market. , 2011, Journal of agricultural and food chemistry.

[118]  A. Visconti,et al.  Fate of deoxynivalenol, T-2 and HT-2 toxins and their glucoside conjugates from flour to bread: an investigation by high-performance liquid chromatography high-resolution mass spectrometry , 2013, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[119]  S. Tittlemier,et al.  Fusarium damage in cereal grains from Western Canada. 1. Phylogenetic analysis of moniliformin-producing fusarium species and their natural occurrence in mycotoxin-contaminated wheat, oats, and rye. , 2013, Journal of agricultural and food chemistry.

[120]  N. Cayot,et al.  Analytical comparison and sensory representativity of SAFE, SPME, and Purge and Trap extracts of volatile compounds from pea flour. , 2012, Food chemistry.

[121]  S. Simsek,et al.  Analysis of Deoxynivalenol and Deoxynivalenol-3-glucoside in wheat , 2012 .

[122]  A. Capriotti,et al.  Recent trends in matrix solid-phase dispersion , 2013 .

[123]  Milena Zachariasova,et al.  Analysis of multiple mycotoxins in cereals under ambient conditions using direct analysis in real time (DART) ionization coupled to high resolution mass spectrometry. , 2010, Talanta.

[124]  G. Font,et al.  Exposure estimates to Fusarium mycotoxins through cereals intake. , 2013, Chemosphere.

[125]  Fusheng Chen,et al.  Preparation for aflatoxin B(1)-cationized bovine serum albumin based on Mannich-type reaction. , 2007, Journal of immunological methods.

[126]  R. Krska,et al.  Development and validation of a liquid chromatography/tandem mass spectrometric method for the determination of 39 mycotoxins in wheat and maize. , 2006, Rapid communications in mass spectrometry : RCM.

[127]  J. Mañes,et al.  Pressurized liquid extraction coupled to liquid chromatography for the analysis of ochratoxin A in breakfast and infants cereals from Morocco , 2010 .

[128]  J. Hajšlová,et al.  Novel approaches in analysis of Fusarium mycotoxins in cereals employing ultra performance liquid chromatography coupled with high resolution mass spectrometry. , 2010, Analytica chimica acta.

[129]  Toshitsugu Tanaka,et al.  Development of a liquid chromatography/time-of-flight mass spectrometric method for the simultaneous determination of trichothecenes, zearalenone and aflatoxins in foodstuffs. , 2006, Rapid communications in mass spectrometry : RCM.

[130]  Roger M. Smith,et al.  3.40 – Sample Preparation for Food Contaminant Analysis , 2012 .

[131]  M. Rezaee,et al.  Determination of organic compounds in water using dispersive liquid-liquid microextraction. , 2006, Journal of chromatography. A.

[132]  Robert K. Boyd,et al.  Trace Quantitative Analysis by Mass Spectrometry , 2008 .

[133]  E. Ferrer,et al.  Risk assessment associated to the intake of the emerging Fusarium mycotoxins BEA, ENs and FUS present in infant formula of Spanish origin , 2012 .

[134]  H. Humpf,et al.  Analysis of the Fusarium mycotoxin moniliformin in cereal samples using 13C2-moniliformin and high-resolution mass spectrometry. , 2012, Journal of agricultural and food chemistry.

[135]  J. Mañes,et al.  Occurrence of fumonisins B1, B2 and B3 in breakfast and infant cereals from Morocco , 2012 .

[136]  R. Krska,et al.  Rapid surface plasmon resonance immunoassay for the determination of deoxynivalenol in wheat, wheat products, and maize-based baby food. , 2010, Journal of agricultural and food chemistry.

[137]  N. Saxena,et al.  Detection of Ochratoxin A in wheat samples in different regions of India , 2012 .

[138]  Y. Sago,et al.  Detection of a new Fusarium masked mycotoxin in wheat grain by high-resolution LC–Orbitrap™ MS , 2011, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[139]  D. Del Rio,et al.  Masked mycotoxins are efficiently hydrolyzed by human colonic microbiota releasing their aglycones. , 2013, Chemical research in toxicology.

[140]  V. Lattanzio,et al.  Determination of trichothecenes in cereals and cereal-based products by liquid chromatography–tandem mass spectrometry , 2008, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[141]  J. Mañes,et al.  First report on the presence of emerging Fusarium mycotoxins enniatins (A, A1, B, B1), beauvericin and fusaproliferin in rice on the Moroccan retail markets , 2011 .

[142]  Zhaowei Zhang,et al.  Advanced hyphenated chromatographic-mass spectrometry in mycotoxin determination: current status and prospects. , 2013, Mass spectrometry reviews.

[143]  A. Capriotti,et al.  Development and validation of a liquid chromatography/atmospheric pressure photoionization-tandem mass spectrometric method for the analysis of mycotoxins subjected to commission regulation (EC) No. 1881/2006 in cereals. , 2010, Journal of chromatography. A.

[144]  Elena Lizarraga,et al.  Co-occurrence of aflatoxins, ochratoxin A and zearalenone in breakfast cereals from spanish market , 2011 .

[145]  G. Cano-Sancho,et al.  Presence and co-occurrence of aflatoxins, deoxynivalenol, fumonisins and zearalenone in gluten-free and ethnic foods , 2012 .

[146]  A. Dossena,et al.  LC/ESI-MS/MS analysis outlines the different fumonisin patterns produced by F. verticillioides in culture media and in maize kernels. , 2012, Journal of mass spectrometry : JMS.

[147]  A. E. Abidi,et al.  First survey on the presence of ochratoxin A and fungi in raw cereals and peanut available in the Republic of Niger , 2013 .

[148]  M. Busman,et al.  Observation of T-2 Toxin and HT-2 Toxin Glucosides from Fusarium sporotrichioides by Liquid Chromatography Coupled to Tandem Mass Spectrometry (LC-MS/MS) , 2011, Toxins.

[149]  J. M. Soriano,et al.  Use of the modified quick easy cheap effective rugged and safe sample preparation approach for the simultaneous analysis of type A- and B-trichothecenes in wheat flour. , 2010, Journal of chromatography. A.

[150]  G. Font,et al.  Multi-mycotoxin analysis in wheat semolina using an acetonitrile-based extraction procedure and gas chromatography-tandem mass spectrometry. , 2012, Journal of chromatography. A.

[151]  J. Frece,et al.  Fusarium mycotoxins' occurrence in cereals harvested from Croatian fields , 2013 .

[152]  J. Hajšlová,et al.  Deoxynivalenol oligoglycosides: new "masked" fusarium toxins occurring in malt, beer, and breadstuff. , 2012, Journal of agricultural and food chemistry.

[153]  J. Gilbert,et al.  Immunoaffinity column clean-up techniques in food analysis: A review. , 2010, Journal of chromatography. B, Analytical technologies in the biomedical and life sciences.

[154]  H. Bacha,et al.  Natural occurrence of citrinin in Tunisian wheat grains , 2012 .

[155]  G. Font,et al.  Analysis of fumonisins B(1), B(2) and B(3) in corn-based baby food by pressurized liquid extraction and liquid chromatography/tandem mass spectrometry. , 2008, Journal of chromatography. A.

[156]  R. Krska,et al.  Formation, determination and significance of masked and other conjugated mycotoxins , 2009, Analytical and bioanalytical chemistry.

[157]  Julia Hepperle,et al.  Extracting fumonisins from maize: efficiency of different extraction solvents in multi-mycotoxin analytics , 2013, Mycotoxin Research.

[158]  B. Gaspardo,et al.  A rapid method for detection of fumonisins B1 and B2 in corn meal using Fourier transform near infrared (FT-NIR) spectroscopy implemented with integrating sphere. , 2012, Food chemistry.

[159]  R. Krska,et al.  Application of a liquid chromatography–tandem mass spectrometric method to multi-mycotoxin determination in raw cereals and evaluation of matrix effects , 2007, Food additives and contaminants.

[160]  A. R. Long,et al.  Isolation of drug residues from tissues by solid phase dispersion. , 1989, Journal of chromatography.

[161]  J. Halket,et al.  Handbook of derivatives for chromatography , 1978 .

[162]  G. Galaverna,et al.  Hyphenated chromatographic techniques for structural characterization and determination of masked mycotoxins. , 2012, Journal of chromatography. A.

[163]  Y Liu,et al.  Feasibility of FT–Raman spectroscopy for rapid screening for DON toxin in ground wheat and barley , 2009, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[164]  M. Ferrari,et al.  Simultaneous determination of deoxynivalenol, zearalenone, T-2 and HT-2 toxins in breakfast cereals and baby food by high-performance liquid chromatography and tandem mass spectrometry. , 2010, Journal of mass spectrometry : JMS.

[165]  H. Jeleń,et al.  Determination of trichothecenes in wheat grain without sample cleanup using comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry. , 2008, Journal of chromatography. A.

[166]  C. Delerue-Matos,et al.  Determination of Ochratoxin A in Bread: Evaluation of Microwave-Assisted Extraction Using an Orthogonal Composite Design Coupled with Response Surface Methodology , 2013, Food and Bioprocess Technology.

[167]  Emanuela Gobbi,et al.  Prediction of milled maize fumonisin contamination by multispectral image analysis. , 2010 .

[168]  R. Dabeka,et al.  Application of isotope dilution mass spectrometry: determination of ochratoxin A in the Canadian Total Diet Study , 2011, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[169]  Y. Zhang,et al.  Simultaneous determination of multi-component mycotoxin contaminants in foods and feeds by ultra-performance liquid chromatography tandem mass spectrometry. , 2007, Journal of chromatography. A.

[170]  Linda Monaci,et al.  Determination of deoxynivalenol, T-2 and HT-2 toxins in a bread model food by liquid chromatography-high resolution-Orbitrap-mass spectrometry equipped with a high-energy collision dissociation cell. , 2011, Journal of chromatography. A.