Correlation between forming quality and spatter dynamics in laser powder bed fusion

Abstract Laser powder bed fusion (LPBF) has broad application prospects due to its high fabrication accuracy and excellent performance, but the dynamic mechanical properties of LPBF components are relatively low due to defects of the melt track such as protrusions and depressions, whose generation mechanisms remain unclear. In this work, we investigate the correlation between the ex situ melt track properties and the in situ high-speed, high-resolution characterization. We correlate the protrusion at the starting position of the melt track with the droplet ejection behaviour and backward surging melt. We also reveal that the inclination angles of the depression walls are consistent with the ejection angles of the backward-ejected spatter. Furthermore, we quantify the vapour recoil pressure by in situ characterization of the deflection of the typical forward-ejected spatter. Our results clarify the intrinsic correlation of the melt track properties, which is important for the stable LPBF formation with few defects.

[1]  H. Maier,et al.  On the mechanical behaviour of titanium alloy TiAl6V4 manufactured by selective laser melting: Fatigue resistance and crack growth performance , 2013 .

[2]  Di Wang,et al.  Investigation into spatter behavior during selective laser melting of AISI 316L stainless steel powder , 2015 .

[3]  Ting Zhu,et al.  Additively manufactured hierarchical stainless steels with high strength and ductility. , 2018, Nature materials.

[4]  C. Colin,et al.  As-Fabricated and Heat-Treated Microstructures of the Ti-6Al-4V Alloy Processed by Selective Laser Melting , 2011 .

[5]  J. Kruth,et al.  A study of the microstructural evolution during selective laser melting of Ti–6Al–4V , 2010 .

[6]  R. Hague,et al.  3D printing of Aluminium alloys: Additive Manufacturing of Aluminium alloys using selective laser melting , 2019, Progress in Materials Science.

[7]  Guoqing Wang,et al.  Thermal behavior and grain growth orientation during selective laser melting of Ti-6Al-4V alloy , 2018, Journal of Materials Processing Technology.

[8]  Jie Yin,et al.  High-power laser-matter interaction during laser powder bed fusion , 2019, Additive Manufacturing.

[9]  F. Walther,et al.  Very high cycle fatigue and fatigue crack propagation behavior of selective laser melted AlSi12 alloy , 2017 .

[10]  E. Brandl,et al.  Additive manufactured AlSi10Mg samples using Selective Laser Melting (SLM): Microstructure, high cycle fatigue, and fracture behavior , 2012 .

[11]  Zemin Wang,et al.  A comparison on metallurgical behaviors of 316L stainless steel by selective laser melting and laser cladding deposition , 2017 .

[12]  Zemin Wang,et al.  Microstructures and mechanical properties of Ti6Al4V alloy fabricated by multi-laser beam selective laser melting , 2017 .

[13]  Y. Zhao,et al.  Microstructures and properties of SLM-manufactured Cu-15Ni-8Sn alloy , 2020 .

[14]  Geok Soon Hong,et al.  In-situ monitoring of laser-based PBF via off-axis vision and image processing approaches , 2019, Additive Manufacturing.

[15]  Jun Ni,et al.  Spatter formation in selective laser melting process using multi-laser technology , 2017 .

[16]  Shian Gao,et al.  Revealing internal flow behaviour in arc welding and additive manufacturing of metals , 2018, Nature Communications.

[17]  R. Poprawe,et al.  Laser additive manufacturing of metallic components: materials, processes and mechanisms , 2012 .

[18]  Haihong Zhu,et al.  Microstructure and properties in QCr0.8 alloy produced by selective laser melting with different heat treatment , 2019, Journal of Alloys and Compounds.

[19]  Alexander M. Rubenchik,et al.  Metal vapor micro-jet controls material redistribution in laser powder bed fusion additive manufacturing , 2017, Scientific Reports.

[20]  Michael Towrie,et al.  In situ X-ray imaging of defect and molten pool dynamics in laser additive manufacturing , 2018, Nature Communications.

[21]  Zemin Wang,et al.  Formation and control of martensite in Ti-6Al-4V alloy produced by selective laser melting , 2016 .

[22]  N. Parab,et al.  Bulk-Explosion-Induced Metal Spattering During Laser Processing , 2019, Physical Review X.

[23]  M. Ramulu,et al.  Fatigue performance evaluation of selective laser melted Ti–6Al–4V , 2014 .

[24]  Michael F Toney,et al.  An instrument for in situ time-resolved X-ray imaging and diffraction of laser powder bed fusion additive manufacturing processes. , 2018, The Review of scientific instruments.

[25]  J. Schoenung,et al.  On the limitations of Volumetric Energy Density as a design parameter for Selective Laser Melting , 2017 .

[26]  Georg Schlick,et al.  Influence of the shielding gas flow on the removal of process by-products in the selective laser melting process , 2016 .

[27]  Zhicong Pang,et al.  Comparative study on the influence of subsequent thermal cycling on microstructure and mechanical properties of selective laser melted 316L stainless steel , 2017 .

[28]  Kevin W Eliceiri,et al.  NIH Image to ImageJ: 25 years of image analysis , 2012, Nature Methods.

[29]  A. Kaplan,et al.  Spatter in laser welding , 2011 .

[30]  Zhiheng Hu,et al.  Effect of Zirconium addition on crack, microstructure and mechanical behavior of selective laser melted Al-Cu-Mg alloy , 2017 .

[31]  S. Katayama,et al.  Dynamics of keyhole and molten pool in laser welding , 1998 .

[32]  A. Matsunawa,et al.  The role of recoil pressure in energy balance during laser materials processing , 1997 .

[33]  Hang Zheng,et al.  Effects of scan speed on vapor plume behavior and spatter generation in laser powder bed fusion additive manufacturing , 2018, Journal of Manufacturing Processes.

[34]  Sheldon Wu,et al.  Modulating laser intensity profile ellipticity for microstructural control during metal additive manufacturing , 2017 .

[35]  Kamel Fezzaa,et al.  In-situ characterization and quantification of melt pool variation under constant input energy density in laser powder bed fusion additive manufacturing process , 2019, Additive Manufacturing.

[37]  D. Bäuerle Laser Processing and Chemistry , 1996 .

[38]  R. Hague,et al.  A Study on the Laser Spatter and the Oxidation Reactions During Selective Laser Melting of 316L Stainless Steel, Al-Si10-Mg, and Ti-6Al-4V , 2015, Metallurgical and Materials Transactions A.

[39]  Yang Liu,et al.  Influence of spatter particles contamination on densification behavior and tensile properties of CoCrW manufactured by selective laser melting , 2020 .

[40]  R. Brooks,et al.  The physical properties of alloys in the liquid and “mushy” states , 1996 .

[41]  J. S. Zuback,et al.  Additive manufacturing of metallic components – Process, structure and properties , 2018 .

[42]  Usman Ali,et al.  Identification and characterization of spatter particles and their effect on surface roughness, density and mechanical response of 17-4 PH stainless steel laser powder-bed fusion parts , 2019, Materials Science and Engineering: A.

[43]  Zhiheng Hu,et al.  Experimental investigation on selective laser melting of 17-4PH stainless steel , 2017 .

[44]  Di Wang,et al.  Mechanisms and characteristics of spatter generation in SLM processing and its effect on the properties , 2017 .

[45]  Alexander M. Rubenchik,et al.  Denudation of metal powder layers in laser powder bed fusion processes , 2016 .

[46]  L. Froyen,et al.  Selective laser melting of iron-based powder , 2004 .

[47]  Sergei I. Anisimov,et al.  Instabilities in Laser-Matter Interaction , 1995 .

[48]  Y. Kawahito,et al.  Observation and understanding in laser welding of pure titanium at subatmospheric pressure. , 2017, Optics express.

[49]  Michael F Toney,et al.  Dynamics of pore formation during laser powder bed fusion additive manufacturing , 2019, Nature Communications.

[50]  Yang Liu,et al.  Study on the influence of process parameters on the clearance feature in non-assembly mechanism manufactured by selective laser melting , 2017 .

[51]  R. M. Ward,et al.  Fluid and particle dynamics in laser powder bed fusion , 2018 .

[52]  T. Pollock,et al.  3D printing of high-strength aluminium alloys , 2017, Nature.

[53]  Ryan Wicker,et al.  Multiprocess 3D printing for increasing component functionality , 2016, Science.

[54]  Kamel Fezzaa,et al.  Transient dynamics of powder spattering in laser powder bed fusion additive manufacturing process revealed by in-situ high-speed high-energy x-ray imaging , 2018, Acta Materialia.

[55]  Chandrika Kamath,et al.  Observation of keyhole-mode laser melting in laser powder-bed fusion additive manufacturing , 2014 .

[56]  Kamel Fezzaa,et al.  Pore elimination mechanisms during 3D printing of metals , 2019, Nature Communications.

[57]  Kamel Fezzaa,et al.  Real-time monitoring of laser powder bed fusion process using high-speed X-ray imaging and diffraction , 2017, Scientific Reports.

[58]  J. Kruth,et al.  Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder , 2013 .

[59]  Bianca Maria Colosimo,et al.  On the use of spatter signature for in-situ monitoring of Laser Powder Bed Fusion , 2017 .

[60]  Kamel Fezzaa,et al.  Keyhole threshold and morphology in laser melting revealed by ultrahigh-speed x-ray imaging , 2019, Science.

[61]  Zhiheng Hu,et al.  Selective Laser Melting of Cu 10Zn alloy powder using high laser power , 2019, Powder Technology.