Damage characterisation of cryogenically cycled carbon fibre/PEEK laminates

Abstract A unique insight into damage formation in CF/PEEK laminates before, during and after cryogenic cycling, using optical microscopy and 3D X-ray computed tomography (CT), is presented. Thicker laminates were found to exhibit significantly greater microcrack density and delamination when compared to thinner laminates, with lay-up and material type also being important contributing factors. Thermal residual stress induced microcracking was also found in thicker laminates post-processing. 3D rendering software was used to prove the presence of through thickness crack networks within the laminates, as well as the extent of cracking through the specimen width. Crack opening in inner and off-axis ply groups was found to be significantly less than outer plies, implying the importance of these plies in limiting laminate permeability. The presence of voids was found to influence crack nucleation and growth paths within the laminates, with full void volume characterisation presented.

[1]  V. T. Bechel,et al.  Limiting the permeability of composites for cryogenic applications , 2006 .

[2]  Harald E.N. Bersee,et al.  Residual stresses in thermoplastic composites - a study of the literature. Part III: Effects of thermal residual stresses , 2007 .

[3]  Adriaan Beukers,et al.  Residual stresses in thermoplastic composites—A study of the literature—Part I: Formation of residual stresses , 2006 .

[4]  D. R. Moore,et al.  Interlaminar fracture morphology of carbon fibre/PEEK composites , 1987 .

[5]  T. Ishikawa,et al.  Evaluation of gas leakage through composite laminates with multilayer matrix cracks: Cracking angle effects , 2006 .

[6]  Franz Dieter Fischer,et al.  Fracture statistics of brittle materials: Weibull or normal distribution. , 2002, Physical review. E, Statistical, nonlinear, and soft matter physics.

[7]  R. Kraus,et al.  Air Force Office of Scientific Research , 2015 .

[8]  William A. Curtin,et al.  Strength and reliability of fiber-reinforced composites: Localized load-sharing and associated size effects , 1997 .

[9]  H. Yoon,et al.  Mode I interlaminar fracture toughness of commingled carbon fibre/PEEK composites , 1993, Journal of Materials Science.

[10]  G. Jeronimidis,et al.  Residual Stresses in Carbon Fibre-Thermoplastic Matrix Laminates , 1988 .

[11]  Caglar Oskay,et al.  Experimental and computational investigation of progressive damage accumulation in CFRP composites , 2013 .

[12]  Ran Y. Kim,et al.  Damage trends in cryogenically cycled carbon/polymer composites , 2004 .

[13]  J. Morton,et al.  Damage and Failure Mechanisms in Scaled Angle-Ply Laminates , 1993 .

[14]  B. Sankar,et al.  Prediction of stitch crack evolution and gas permeability in multidirectional composite laminates , 2008 .

[15]  Samit Roy,et al.  Modeling of permeation and damage in graphite/epoxy laminates for cryogenic tanks in the presence of delaminations and stitch cracks , 2007 .

[16]  Ran Y. Kim,et al.  Cryogenic/elevated temperature cycling induced leakage paths in PMCs , 2005 .

[17]  Tomohiro Yokozeki,et al.  Effects of layup angle and ply thickness on matrix crack interaction in contiguous plies of composite laminates , 2005 .

[18]  Takashi Ishikawa,et al.  MECHANICAL BEHAVIOR OF CF / POLYMER COMPOSITE LAMINATES UNDER CRYOGENIC ENVIRONMENT , 1999 .

[19]  Ian Sinclair,et al.  3D damage characterisation and the role of voids in the fatigue of wind turbine blade materials , 2012 .

[20]  M. A. Verges,et al.  X-ray computed microtomography of internal damage in fiber reinforced polymer matrix composites , 2005 .

[21]  Hugh McManus,et al.  Thermally induced damage in composite laminates: Predictive methodology and experimental investigation , 1996 .

[22]  C. Heinzl,et al.  Advanced X-Ray Tomographic Methods for Quantitative Characterisation of Carbon Fibre Reinforced Polymers , 2012 .

[23]  I. Sinclair,et al.  Ultra High Resolution Computed Tomography of Damage in Notched Carbon Fiber—Epoxy Composites , 2008 .

[24]  Roberto J. Cano,et al.  Hybrid Composites for LH2 Fuel Tank Structure , 2001 .

[25]  Dimitris C. Lagoudas,et al.  Prediction of Cryogen Leak Rate through Damaged Composite Laminates , 2007 .

[26]  Conchur O Bradaigh,et al.  An XFEM-based methodology for fatigue delamination and permeability of composites , 2014 .

[27]  Johann KASTNER,et al.  Comparison of phase contrast X-ray computed tomography methods for non-destructive testing of materials , 2012 .

[28]  Samit Roy,et al.  Modeling of permeation and damage in graphite/epoxy laminates for cryogenic fuel storage , 2004 .

[29]  J. Andre Lavoie,et al.  Stitch Cracks in Constraint Plies Adjacent to a Cracked Ply , 2001 .

[30]  J. Berthelot,et al.  Statistical analysis of the progression of transverse cracking and delamination in cross-ply laminates , 2000 .

[31]  John A. Nairn,et al.  2.12 – Matrix Microcracking in Composites , 2000 .

[32]  M. Lafarie-Frenot,et al.  Doubly periodic matrix cracking in composite laminates Part 2: Thermal biaxial loading , 1996 .

[33]  Ran Y. Kim,et al.  Effect of stacking sequence on micro-cracking in a cryogenically cycled carbon/bismaleimide composite , 2003 .

[34]  M. Gurvich Strength/size effect for anisotropic brittle materials under a random stress state , 1999 .

[35]  T. Aoki,et al.  Influence of stacking sequence on leakage characteristics through CFRP composite laminates , 2006 .

[36]  A. R. Chambers,et al.  The effect of voids on the flexural fatigue performance of unidirectional carbon fibre composites developed for wind turbine applications , 2006 .