Spring constant of a tuning-fork sensor for dynamic force microscopy

Summary We present an overview of experimental and numerical methods to determine the spring constant of a quartz tuning fork in qPlus configuration. The simple calculation for a rectangular cantilever is compared to the values obtained by the analysis of the thermal excitation and by the direct mechanical measurement of the force versus displacement. To elucidate the difference, numerical simulations were performed taking account of the real geometry including the glue that is used to mount the tuning fork.

[1]  S. Okuma,et al.  A method for determining the spring constant of cantilevers for atomic force microscopy , 1996 .

[2]  Jonathan S. Colton,et al.  Characterization of microcantilevers solely by frequency response acquisition , 2005 .

[3]  P. Hansma,et al.  A nondestructive method for determining the spring constant of cantilevers for scanning force microscopy , 1993 .

[4]  A. Gent,et al.  On the Relation between Indentation Hardness and Young's Modulus , 1958 .

[5]  P. Tordjeman,et al.  Cantilever calibration for nanofriction experiments with atomic force microscope , 2005 .

[6]  N. Bekkedahl Rubber Chem. Technol , 1969 .

[7]  N. Moll,et al.  Organic structure determination using atomic-resolution scanning probe microscopy. , 2010, Nature chemistry.

[8]  J. Gilman,et al.  Nanotechnology , 2001 .

[9]  John Hedley,et al.  Accurate force measurement in the atomic force microscope: a microfabricated array of reference springs for easy cantilever calibration , 2003 .

[10]  J. Hedley,et al.  Microelectromechanical system device for calibration of atomic force microscope cantilever spring constants between 0.01 and 4 N/m , 2004 .

[11]  John E. Sader,et al.  Normal and torsional spring constants of atomic force microscope cantilevers , 2004 .

[12]  P. Schendel,et al.  Operation characteristics of piezoelectric quartz tuning forks in high magnetic fields at liquid helium temperatures , 1999, cond-mat/9907079.

[13]  Peter Liljeroth,et al.  Amplifying the Pacific Climate System Response to a Small 11-Year Solar Cycle Forcing , 2009, Science.

[14]  F. Giessibl,et al.  Application of the equipartition theorem to the thermal excitation of quartz tuning forks , 2011, 1106.3018.

[15]  Manfred H. Jericho,et al.  Device for the determination of spring constants of atomic force microscope cantilevers and micromachined springs , 2002 .

[16]  J. Bechhoefer,et al.  Calibration of atomic‐force microscope tips , 1993 .

[17]  M. Lange,et al.  Very compact design for a low-temperature tuning fork atomic force microscope , 2010 .

[18]  Markus Heyde,et al.  Recipes for cantilever parameter determination in dynamic force spectroscopy: spring constant and amplitude , 2007 .

[19]  Sverre Myhra,et al.  Determination of the spring constants of probes for force microscopy/spectroscopy , 1996 .

[20]  Franz J. Giessibl,et al.  HIGH-SPEED FORCE SENSOR FOR FORCE MICROSCOPY AND PROFILOMETRY UTILIZING A QUARTZ TUNING FORK , 1998 .

[21]  J. Gómez‐Herrero,et al.  WSXM: a software for scanning probe microscopy and a tool for nanotechnology. , 2007, The Review of scientific instruments.

[22]  Franz J. Giessibl,et al.  Forces and frequency shifts in atomic-resolution dynamic-force microscopy , 1997 .

[23]  John E. Sader,et al.  Parallel beam approximation for V‐shaped atomic force microscope cantilevers , 1995 .

[24]  R. Lévy,et al.  Measuring the spring constant of atomic force microscope cantilevers: thermal fluctuations and other methods , 2002 .

[25]  J. Sader,et al.  Calibration of rectangular atomic force microscope cantilevers , 1999 .

[26]  J. Pratt,et al.  Small mass measurements for tuning fork-based atomic force microscope cantilever spring constant calibration , 2011 .

[27]  J. Sader,et al.  Method for the calibration of atomic force microscope cantilevers , 1995 .

[28]  C. Abell,et al.  A nondestructive technique for determining the spring constant of atomic force microscope cantilevers , 2001 .

[29]  Timothy Senden,et al.  Experimental Determination of Spring Constants in Atomic Force Microscopy , 1994 .

[30]  N. Agraït,et al.  Dynamics of quartz tuning fork force sensors used in scanning probe microscopy , 2009, Nanotechnology.