The fabrication of back etching 3C-SiC-on-Si diaphragm employing KOH + IPA in MEMS capacitive pressure sensor

The 680 µm thick wafer is back-etched, leaving the thin film 3C-SiC as the flexible diaphragm to detect pressure. The etching processes are performed with three different KOH concentrations (35, 45 and 55 %), without and with 10 % IPA surfactant and the etching temperatures of 50 and 80 °C. Graphs are plotted on the effect of the etch rate and etch depth against these three parameters. In addition, the surface roughnesses of the diaphragms at these conditions are measured, photographed and analyzed. The results show that the back-etching of a 3C-SiC-on-Si wafer is fastest at higher temperature and KOH concentration and without IPA surfactant, but at the price of higher surface roughness. The addition of 10 % IPA reduces the surface roughness significantly. We also notice the increasing presence of micro-pipes at higher KOH concentration and etching temperature. The experiments are performed using bulge test method that induces the effects of dimensional layout diaphragm of 2,000 and 2,500 µm, the curve shows a good resemblance each other at pressure of 5.0 MPa. The maximum difference linearity of 2,000 and 2,500 µm is 98.7 and 97.1 %, respectively. It is revealed that the small layout dimensional can sustain the diaphragm at high pressure compare with large dimensional layout of 3,000 and 3,500 µm with the linearity is about 73.2 and 62.6 %, respectively.

[1]  N. Ohtani,et al.  Mechanism of Molten KOH Etching of SiC Single Crystals: Comparative Study with Thermal Oxidation , 1999 .

[2]  E. Janzén,et al.  Anisotropic Etching of SiC , 2000 .

[3]  P. Ramasamy,et al.  Electrochemical Etching of 6H-SiC Using Aqueous KOH Solutions with Low Surface Roughness , 2003 .

[4]  D. Zhuang,et al.  Wet etching of GaN, AlN, and SiC : a review , 2005 .

[5]  J. Kelly,et al.  Photoelectrochemistry of 4H-SiC in KOH solutions , 2007 .

[6]  O. Paul,et al.  Reliability of MEMS Materials: Mechanical Characterization of Thin-Films using the Wafer Scale Bulge Test and Improved Microtensile Techniques , 2007 .

[7]  Oliver Paul,et al.  Thin‐Film Characterization Using the Bulge Test , 2007 .

[8]  Chang Chia‐Yuan,et al.  超低電力 低雑音増幅器応用のためのInAs-チャンネル高電子移動度トランジスタ , 2009 .

[9]  W. Fang,et al.  Improvement of Specimen Preparation Process for Bulge Test Using the Combination of XeF2 and Deep Reactive Ion Etching , 2009 .

[10]  Janna R. B. Casady,et al.  Surface Morphology Improvement and Repeatable Doping Characterization of 4H-SiC Epitaxy Grown on 4° Off-Axis 4H-SiC Wafers , 2009 .

[11]  Burhanuddin Yeop Majlis,et al.  Piezoeletric Micropump for Drug Delivery System Fabricated Using Two Optical Masks , 2009 .

[12]  T. Bessho,et al.  Dislocation Revelation from (0001) Carbon-face of 4H-SiC by Using Vaporized KOH at High Temperature , 2012 .

[13]  M. M. Noor,et al.  The effect of isopropyl alcohol on anisotropic etched silicon for the fabrication of microheater chamber , 2012, 2012 10th IEEE International Conference on Semiconductor Electronics (ICSE).

[14]  Defect Revelation and Evaluation of 4H Silicon Carbide by Optimized Molten KOH Etching Method , 2013 .

[15]  K. S. Rao,et al.  Investigation of micropipe and defects in molten KOH etching of 6H n-silicon carbide (SiC) single crystal , 2013 .

[16]  F. Mohd-Yasin,et al.  Characterization of ProTEX® PSB Thin Film as a Photosensitive Layer for MEMS Capacitive Pressure Sensor Diaphragm Based on SiC-on-Si Wafer , 2013 .

[17]  Burhanuddin Yeop Majlis,et al.  ProTEK PSB coating as an alternative polymeric protection mask for KOH bulk etching of silicon , 2013 .