A ZnO thin-film driven microcantilever for nanoscale actuation and sensing

Zinc oxide (ZnO) thin film as a piezoelectric material for microelectromechanical system (MEMS) actuators and sensors was evaluated. ZnO thin films were deposited using radio frequency (RF) magnetron sputtering. Process parameters such as gas ratio, working pressure, and RF power were optimized for crystalline structure. The ZnO thin films were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). Good quality of ZnO thin films was further confirmed by a high transverse piezoelectric coefficient d 31. A microcantilever was then designed, fabricated, and characterized. Design formulas of resonant frequency, actuation, and sensing sensitivities were derived. The resonant frequency was determined by an impedance analyzer. Tip deflection on nanometer level was demonstrated with the cantilever used as an actuator. The actuation sensitivity was found to be 12.2 nm/V. As a sensor, the cantilever was calibrated against a reference accelerometer. The sensing sensitivity was characterized to be 46 mV/g. The characterization results were compared with design specifications. The differences were caused mainly by thickness control in etching. This study showed that ZnO is a promising piezoelectric material for MEMS actuators and sensors in terms of excellent process compatibility and good piezoelectric performance.

[1]  Kai Chang,et al.  Piezoelectric Transducer-Controlled Dual-Mode Switchable Bandpass Filter , 2007, IEEE Microwave and Wireless Components Letters.

[2]  John P Bentley,et al.  Principles of measurement systems , 1983 .

[3]  M. Weinberg Working equations for piezoelectric actuators and sensors , 1999 .

[4]  Ken Haenen,et al.  Wide range pressure sensor based on a piezoelectric bimorph microcantilever , 2006 .

[5]  Chengkuo Lee,et al.  A 2-D MEMS scanning mirror based on dynamic mixed mode excitation of a piezoelectric PZT thin film S-shaped actuator. , 2011, Optics express.

[6]  K. Grosh,et al.  Modeling and Characterization of Cantilever-Based MEMS Piezoelectric Sensors and Actuators , 2012, Journal of Microelectromechanical Systems.

[7]  N. Sinha,et al.  Body-Biased Complementary Logic Implemented Using AlN Piezoelectric MEMS Switches , 2009, Journal of Microelectromechanical Systems.

[8]  J.G. Smits,et al.  The constituent equations of piezoelectric heterogeneous bimorphs , 1991, IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control.

[9]  Wojtek Wlodarski,et al.  Numerical calculation of SAW sensitivity: application to ZnO/LiTaO3 transducers , 2004 .

[10]  Takeshi Morita,et al.  Miniature piezoelectric motors , 2003 .

[11]  A. Pisano,et al.  Modeling and optimal design of piezoelectric cantilever microactuators , 1997 .

[12]  C. Quate,et al.  AUTOMATED PARALLEL HIGH-SPEED ATOMIC FORCE MICROSCOPY , 1998 .

[13]  Hannes Bleuler,et al.  Non-contact atomic force microscope with a PZT cantilever used for deflection sensing, direct oscillation and feedback actuation , 2002 .

[14]  Antonio Arnau,et al.  Fundamentals on Piezoelectricity , 2004 .

[15]  W. J. Merz Piezoelectric Ceramics , 1972, Nature.

[16]  Wojtek Wlodarski,et al.  Highly sensitive layered ZnO/LiNbO3 SAW device with InOx selective layer for NO2 and H2 gas sensing , 2005 .

[17]  심성한,et al.  Fundamentals of Vibrations , 2013 .

[18]  Ryutaro Maeda,et al.  Effect of multi-coating process on the orientation and microstructure of lead zirconate titanate (PZT) thin films derived by chemical solution deposition , 2005 .

[19]  S. Trolier-McKinstry,et al.  Thin Film Piezoelectrics for MEMS , 2004 .

[20]  D. Polla,et al.  PROCESSING AND CHARACTERIZATION OF PIEZOELECTRIC MATERIALS AND INTEGRATION INTO MICROELECTROMECHANICAL SYSTEMS , 1998 .

[21]  Yilong Hao,et al.  The compatibility of ZnO piezoelectric film with micromachining process , 2003 .

[22]  William L. Hughes,et al.  Nanobelts as nanocantilevers , 2003 .

[23]  E. S. Kim,et al.  Single- and Triaxis Piezoelectric-Bimorph Accelerometers , 2008, Journal of Microelectromechanical Systems.

[24]  Todd Sulchek,et al.  High-speed tapping mode imaging with active Q control for atomic force microscopy , 2000 .

[25]  Wojtek Wlodarski,et al.  A ZnO nanorod based layered ZnO/64° YX LiNbO3 SAW hydrogen gas sensor , 2007 .

[26]  H. Morkoç,et al.  A COMPREHENSIVE REVIEW OF ZNO MATERIALS AND DEVICES , 2005 .

[27]  Takayuki Shibata,et al.  Characterization of sputtered ZnO thin film as sensor and actuator for diamond AFM probe , 2002 .

[28]  Chengkuo Lee,et al.  Characterization of piezoelectric PZT beam actuators for driving 2D scanning micromirrors , 2010 .

[29]  Jan H. J. Fluitman,et al.  Thin-film ZnO as micromechanical actuator at low frequencies , 1990 .

[30]  Rainer Waser,et al.  An integrated microelectromechanical microwave switch based on piezoelectric actuation , 2009 .

[31]  T. Itoh,et al.  Micromachined piezoelectric force sensors based on PZT thin films , 1996, IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control.

[32]  Calvin F. Quate,et al.  Atomic force microscopy for high speed imaging using cantilevers with an integrated actuator and sensor , 1996 .

[33]  Jan G. Smits,et al.  The constituent equations of piezoelectric bimorphs , 1991 .

[34]  P. Sharma Mechanics of materials. , 2010, Technology and health care : official journal of the European Society for Engineering and Medicine.

[35]  A. J. Flewittb,et al.  Recent developments on ZnO films for acoustic wave based bio-sensing and microfluidic applications: a review , 2009 .