Formation of in situ VGCFs on carbon fibre felt by chemical vapour infiltration

In situ vapour grown carbon fi bres (VGCFs) were fabricated on carbon felt by chemical vapour in fi ltration. In this work, the different conditions of the preparation process were determined to obtain VGCFs in large quantities, namely pressure in the reactor and concentration of the aqueous catalyst precursor solution. Observations regarding the growth process of the VGCFs reveal that the catalyst particles with a round shape and diameters of 1 μ m or above are most likely to produce VGCFs. The fi nal results indicate that the diameters of VGCFs range from 80 to 150 nm and that their lengths range from 5 to 30 μ m. Furthermore, the lengthening and thickening processes of VGCFs were proved to occur simultaneously in the experiment.

[1]  M. Bechelany,et al.  Carbon felt based-electrodes for energy and environmental applications: A review , 2017 .

[2]  M. Bechelany,et al.  A highly active based graphene cathode for the electro-fenton reaction , 2015 .

[3]  X. Xiong,et al.  Microstructure, mechanical properties and oxidation behavior of carbon fiber reinforced PyC/C-TaC/PyC layered-structure ceramic matrix composites prepared by chemical vapor infiltration , 2013 .

[4]  Robert Czochara,et al.  Fullerene C60 as an inhibitor of high temperature lipid oxidation , 2012 .

[5]  Hejun Li,et al.  Grafting straight carbon nanotubes radially onto carbon fibers and their effect on the mechanical properties of carbon/carbon composites , 2012 .

[6]  J. Zou,et al.  Synthesis of in situ network-like vapor-grown carbon fiber improved LiFePO4 cathode materials by microwave pyrolysis chemical vapor deposition , 2011 .

[7]  T. L. Dhami,et al.  Development of vapor grown carbon fibers (VGCF) reinforced carbon/carbon composites , 2006 .

[8]  Q. Gong,et al.  Synthesis and characterization of in situ grown carbon nanofiber/nanotube reinforced carbon/carbon composites , 2005 .

[9]  J. P. Donohoe,et al.  Preparation, electrical and mechanical properties of vapor grown carbon fiber (VGCF)/vinyl ester composites , 2004 .

[10]  S. Mukai,et al.  Core structure of vapor grown carbon fibers and morphology dependence of tensile strength , 2003 .

[11]  Charles U. Pittman,et al.  Ablation, mechanical and thermal conductivity properties of vapor grown carbon fiber/phenolic matrix composites , 2002 .

[12]  C. A. Bernardo,et al.  Transport properties of polymer-vapour grown carbon fibre composites , 2000 .

[13]  G. Tibbetts,et al.  Mechanical properties of vapor-grown carbon fiber composites with thermoplastic matrices , 1999 .

[14]  Qian Guo,et al.  Preparation and properties of in-situ growth of carbon nanotubes reinforced hydroxyapatite coating for carbon/carbon composites. , 2017, Materials science & engineering. C, Materials for biological applications.

[15]  Uttandaraman Sundararaj,et al.  A review of vapor grown carbon nanofiber/polymer conductive composites , 2009 .

[16]  Xiao Peng Effect of boric acid on carbon fiber and thermal conductivity of C/C composites , 2008 .

[17]  J. Ting,et al.  Vapor-grown carbon-fiber reinforced carbon composites , 1995 .