Versatile measurement system for the characterization of gas sensing materials

A measurement system designed for the development of novel conductometric gas sensors and of new gas sensing materials is described. The system allows to simultaneously characterize up to 8 sensors. Prototype sensors can be easily realized thanks to an ad hoc structure based on an alumina substrate equipped with electrodes, a heater and an accurate temperature sensor, on this structure the studied material can be deposited by screen printing, spin coating or dip coating. The system is designed to study the behavior of the sensors by accurately setting the operating conditions in terms of chemical environment composition, gas flow, humidity and temperature. The system is fully programmable and it individually controls the film temperatures or measures them with a resolution lower than 0.1 °C. Both chemical transients and thermal transients can be studied. These features make the system suitable for determining the principal performance indexes of a gas sensing device (e.g., sensitivity, stability, selectivity, response/recovery times, etc.) as functions of various combinations of measurement conditions (e.g., gas concentrations, temperature, humidity, flow). The proposed measurement system will find also useful applications in sensor model validation.

[1]  G. Korotcenkov Metal oxides for solid-state gas sensors: What determines our choice? , 2007 .

[2]  Ada Fort,et al.  Surface State Models For Conductance Response Of Metal Oxide Gas Sensors During Thermal Transients , 2012 .

[3]  A. Fort,et al.  Temperature profile investigation of SnO/sub 2/ sensors for CO detection enhancement , 2005, IEEE Transactions on Instrumentation and Measurement.

[4]  Valerio Vignoli,et al.  Dynamic CO recognition in presence of interfering gases by using one MOX sensor and a selected temperature profile , 2003 .

[5]  Ada Fort,et al.  Surface State Model for Conductance Responses During Thermal-Modulation of SnO$_{2}$-Based Thick Film Sensors: Part II—Experimental Verification , 2006, IEEE Transactions on Instrumentation and Measurement.

[6]  Ada Fort,et al.  Temperature profile investigation of SnO2 sensors for CO detection enhancement , 2005, IEEE Trans. Instrum. Meas..

[7]  A. Fort,et al.  Metal-oxide nanowire sensors for CO detection: Charaterization and modeling , 2010, 2010 IEEE Sensors Applications Symposium (SAS).

[8]  A. Flammini,et al.  Model and Experimental Characterization of the Dynamic Behavior of Low-Power Carbon Monoxide MOX Sensors Operated With Pulsed Temperature Profiles , 2009, IEEE Transactions on Instrumentation and Measurement.

[9]  Ada Fort,et al.  Surface State Model for Conductance Responses During Thermal-Modulation of SnO$_{2}$-Based Thick Film Sensors: Part I—Model Derivation , 2006, IEEE Transactions on Instrumentation and Measurement.