Thermodynamic damage mechanism of Ni/Cr film on neutral density filter by 1064-nm pulsed laser

Abstract. We investigate the damage characteristics and mechanism of neutral density filters consisting of metal film on K9 glass substrate by 1064-nm pulsed laser. The damage morphologies present marked differences with different laser pulse energies. Specifically, with the increase of laser fluence, the damage pits density increase as well, and at the same time, the cracks appear around the pits and interconnect, which lead to the abscission of film. The damage mechanism has been studied from the viewpoint of embedded impurities in the film. The theoretical results show that the difference between the thermodynamic properties of impurities and film can lead to thermos-elastic stress, which plays important roles in deformation of film, nucleation and propagation of cracks. Last, methods have been proposed to improve the laser damage resistance by controlling the size distribution of impurity particles and increasing the film tensile strength.

[1]  A. Guenther,et al.  Pulsed laser-induced damage to thin-film optical coatings - Part I: Experimental , 1981, IEEE Journal of Quantum Electronics.

[2]  Bin Wang,et al.  Effect of defects on long-pulse laser-induced damage of two kinds of optical thin films. , 2010, Applied optics.

[3]  Donald R Uhlmann,et al.  Mechanism of Inclusion Damage in Laser Glass , 1970 .

[4]  G. M. Gaeta,et al.  Laser sources in dentistry and radiation safety regulations , 2007, SPIE BiOS.

[5]  Z. Olesiak Problems of thermodiffusion of deformable solids , 1998 .

[6]  A. Argon,et al.  Steady-state creep of alloys due to viscous motion of dislocations☆ , 1976 .

[7]  Shunsaku Koga,et al.  Validation of a high-power, time-resolved, near-infrared spectroscopy system for measurement of superficial and deep muscle deoxygenation during exercise. , 2015, Journal of applied physiology.

[8]  M. Allmen Laser-beam interactions with materials , 1987 .

[9]  Ming Zhou,et al.  Geometrical characteristics and damage morphology of nodules grown from artificial seeds in multilayer coating. , 2010, Applied optics.

[10]  Shouhuan Zhou,et al.  Phase explosion induced by high-repetition rate pulsed laser , 2010 .

[11]  Patrick Combis,et al.  Photothermal investigation of the laser-induced modification of a single gold nano-particle in a silica film , 2005 .

[12]  Nadezhda M. Bulgakova,et al.  Thin film removal mechanisms in ns-laser processing of photovoltaic materials , 2010 .

[13]  Jean Dijon,et al.  Thermomechanical model of mirror laser damage at 1.06 μm: II. Flat bottom pits formation , 1999, Laser Damage.

[14]  Guojun Zhang,et al.  Thickness dependent fatigue life at microcrack nucleation for metal thin films on flexible substrates , 2008 .

[15]  John B. Shoven,et al.  I , Edinburgh Medical and Surgical Journal.

[17]  Sigurd Wagner,et al.  Mechanisms of reversible stretchability of thin metal films on elastomeric substrates , 2006 .

[18]  Stéphanie P. Lacour,et al.  Extended cyclic uniaxial loading of stretchable gold thin-films on elastomeric substrates , 2009 .

[19]  S G Demos,et al.  Wavelength dependence of laser-induced damage: determining the damage initiation mechanisms. , 2003, Physical review letters.

[20]  Roberta Ramponi,et al.  Femtosecond laser micromachining for the realization of fully integrated photonic and microfluidic devices , 2015, Photonics West - Optoelectronic Materials and Devices.

[21]  Jean Hue,et al.  Thermomechanical model of mirror laser damage at 1.06 μm: I. Nodule ejection , 1999, Laser Damage.

[22]  J. K. Chen,et al.  NUMERICAL STUDY OF ULTRASHORT LASER PULSE INTERACTIONS WITH METAL FILMS , 2001 .

[23]  S. Papernov,et al.  Two mechanisms of crater formation in ultraviolet-pulsed-laser irradiated SiO2 thin films with artificial defects , 2005 .

[24]  R. Shvartzer,et al.  Wideband protection filter: single filter for laser damage preventing at wide wavelength range , 2007, SPIE Security + Defence.

[25]  S. Papernov,et al.  Laser-induced surface damage of optical materials: absorption sources, initiation, growth, and mitigation , 2008, Laser Damage.

[26]  J. Dieleman,et al.  Reduction of droplet emission and target roughening in laser ablation and deposition of metals , 1993 .

[27]  Jörg Krüger,et al.  Single- and multi-pulse femtosecond laser ablation of optical filter materials , 2003 .

[28]  Mark R. Kozlowski,et al.  Comparison of nodular defect seed geometries from different deposition techniques , 1996, Laser Damage.

[29]  S. Papernov,et al.  Correlations between embedded single gold nanoparticles in SiO2 thin film and nanoscale crater formation induced by pulsed-laser radiation , 2002 .

[30]  Susan D. Allen,et al.  Nanoscale laser-induced spallation in SiO2 films containing gold nanoparticles , 2006 .

[31]  N. Kaiser,et al.  Defect induced laser damage in oxide multilayer coatings for 248 nm , 1998 .

[32]  W. Shiu,et al.  A critical review of Henry’s law constants for chemicals of environmental interest , 1981 .

[33]  Craig A. Williamson,et al.  Simulating the impact of laser eye protection on color vision , 2016 .

[34]  Ariela Donval,et al.  Dynamic Sunlight Filter (DSF): a passive way to increase the dynamic range in visible and SWIR cameras , 2010, Defense + Commercial Sensing.

[35]  F. Bekker,et al.  On the solubility and resistivity of uranium in gold and platinum hosts , 1989 .

[36]  H Hu,et al.  Laser-Induced Damage of a 1064-nm ZnS/MgF(2) Narrow-Band Interference Filter. , 2001, Applied optics.