Measurement and analysis of fiber-matrix interface strength of carbon fiber-reinforced phenolic resin matrix composites

Since fiber-matrix interface strength is critical to properties of carbon fiber-reinforced composites, measurement and analysis of interface strength are crucial steps in tailored design of composites. In the present work, the single fiber push-out test and the short-beam shear test were applied to measure the fiber-matrix interface strength in uni-directionally and two-directionally carbon fiber-reinforced phenolic resin matrix composites. The technical difficulties in processing the specimen and in realizing the fiber push-out were also discussed and clarified. For obtaining the successful test, typically, the thickness of the specimen should be smaller than 100 mm. During the fiber push-out, the de-bonding and fiber sliding at the interface were analyzed from the load-displacement curve features. The results indicated that both methods could be applied to determine the interface strength. The single fiber push-out and the short-beam shear tests resulted in a similar phenomenon in regard to the interface strength of uni-directionally and two-directionally carbon fiber-reinforced phenolic resin matrix composites, but expressed different values. The low interface strength measured from the short-beam shear test could be associated with multiple interlaminar shear failures. Furthermore, it was found that the interface strength of uni-directionally carbon fiber-reinforced phenolic resin matrix composites is somewhat higher than that of two-directionally carbon fiber-reinforced phenolic resin matrix composites. The difference in the interface strength could be attributed to the thermally induced residual stresses caused by the coefficient of thermal expansion mismatch of fiber and matrix. The approaches applied in the current work can be used for the evaluation of the interface strength of carbon fiber-reinforced phenolic resin matrix composites with different fiber-matrix bonding properties.

[1]  T. Ramanathan,et al.  Investigation of the influence of acidic and basic surface groups on carbon fibres on the interfacial shear strength in an epoxy matrix by means of single-fibre pull-out test , 2001 .

[2]  S. Patankar Weibull distribution as applied to ceramic fibres , 1991 .

[3]  Edith Mäder,et al.  Characterization of fiber/matrix interface strength: applicability of different tests, approaches and parameters , 2005 .

[4]  C. Browning Composite Materials: Quality Assurance and Processing , 1983 .

[5]  Lawrence T. Drzal,et al.  Fibre-matrix adhesion and its relationship to composite mechanical properties , 1993 .

[6]  Y. Kogo,et al.  Interfacial shear strength of C/C composites , 2003 .

[7]  W. Weibull A Statistical Distribution Function of Wide Applicability , 1951 .

[8]  S. Ozcan,et al.  Measurement and analytical validation of interfacial bond strength of PAN-fiber-reinforced carbon matrix composites , 2008 .

[9]  T. Ramanathan,et al.  Investigation of the influence of surface-activated carbon fibres on debonding energy and frictional stress in polymer-matrix composites by the micro-indentation technique , 2001 .

[10]  A. Wanner,et al.  The crack development on the micro- and mesoscopic scale during the pyrolysis of carbon fibre reinforced plastics to carbon/carbon composites , 2007 .

[11]  L L.T.DRZA,et al.  Fibre-matrix adhesion and its relationship to composite mechanical properties , 2022 .

[12]  Soojin Park,et al.  Effect of acidic anode treatment on carbon fibers for increasing fiber-matrix adhesion and its relationship to interlaminar shear strength of composites , 2000 .

[13]  J. Karger‐Kocsis,et al.  Surface energetics of carbon fibers and its effects on the mechanical performance of CF/EP composites , 1996 .

[14]  D. Marshall,et al.  Measurement of Interfacial Mechanical Properties in Fiber‐Reinforced Ceramic Composites , 1987 .

[15]  Yudong Huang,et al.  The effect of carbon-fiber surface properties on the electron-beam curing of epoxy-resin composites , 2002 .