The tritium analytical system at TFRR is used to determine the purity of tritium bearing gas streams in order to provide inventory and accountability measurements. The system includes a quadrupole mass spectrometer and beta scintillator originally configured at Monsanto Mound Research Laboratory in the late 1970`s and early 1980`s. The system was commissioned and tested between 1991 and 1992 and is used daily for analysis of calibration standards, incoming tritium shipments, gases evolved from uranium storage beds and measurement of gases returned to gas holding tanks. The low resolution mass spectrometer is enhanced by the use of a metal getter pump to aid in resolving the mass 3 and 4 species. The beta scintillator complements the analysis as it detects tritium bearing species that often are not easily detected by mass spectrometry such as condensable species or hydrocarbons containing tritium. The instruments are controlled by a personal computer with customized software written with a graphical programming system designed for data acquisition and control. A discussion of the instrumentation, control systems, system parameters, procedural methods, algorithms, and operational issues will be presented. Measurements of gas holding tanks and tritiated water waste streams using ion chamber instrumentation are discussed elsewhere.