Calibration of dielectric constant measurements to improve the detection of cloud and clear points in solution crystallization

[1]  Dielectric Behavior of Solutions of Electrolytes in Solvents of Low Dielectric Constant. V. The Influence of Temperature and Concentration on Dielectric Properties , 1949 .

[2]  C. P. Smyth Dielectric Behavior and Structure: Dielectric Constant and Loss, Dipole Moment, and Molecular Structure , 1955 .

[3]  H. Fröhlich,et al.  Theory of Dielectrics: Dielectric Constant and Dielectric Loss , 1960 .

[4]  H. Akaike A new look at the statistical model identification , 1974 .

[5]  J. Nývlt,et al.  The Kinetics of industrial crystallization , 1984 .

[6]  Ethane-1,2-diol–water solvent system: relative permittivity as a function of temperature and binary composition , 1993 .

[7]  D. Craig,et al.  Dielectric Analysis of Pharmaceutical Systems , 1995 .

[8]  D. Jayaraman,et al.  Estimation of metastable zone width, interfacial energy and growth rates of KTiOPO4 crystallizing from K6P4O13 flux by hot stage microscopy , 1996 .

[9]  A. Goodwin,et al.  Phase border and density determinations in the critical region of (carbon dioxide+ethane) determined from dielectric permittivity measurements , 1997 .

[10]  T. Bose,et al.  SOLUBILITY OF SOLIDS IN SUPERCRITICAL FLUIDS FROM THE MEASUREMENTS OF THE DIELECTRIC CONSTANT : APPLICATION TO CO2-NAPHTHALENE , 1998 .

[11]  Åke C. Rasmuson,et al.  Solubility of Paracetamol in Pure Solvents , 1999 .

[12]  F. Puel,et al.  On-line ATR FTIR measurement of supersaturation during solution crystallization processes. Calibration and applications on three solute/solvent systems , 2001 .

[13]  K. Roberts,et al.  Nucleation, Growth, and Pseudo-Polymorphic Behavior of Citric Acid As Monitored in Situ by Attenuated Total Reflection Fourier Transform Infrared Spectroscopy , 2001 .

[14]  A. Myerson Handbook of Industrial Crystallization , 2002 .

[15]  B. Glennon,et al.  Characterizing the metastable zone width and solubility curve using lasentec FBRM and PVM , 2002 .

[16]  A. Mersmann,et al.  How to measure supersaturation , 2002 .

[17]  B. Marciniak,et al.  Density and ultrasonic velocity of undersaturated and supersaturated solutions of fluoranthene in trichloroethylene, and study of their metastable zone width , 2002 .

[18]  R. Braatz,et al.  Paracetamol Crystallization Using Laser Backscattering and ATR-FTIR Spectroscopy: Metastability, Agglomeration, and Control , 2002 .

[19]  A. R. Parsons,et al.  Automated Measurement of Metastable Zones for Pharmaceutical Compounds , 2003 .

[20]  H. Gürbüz,et al.  Experimental determination of the metastable zone width of borax decahydrate by ultrasonic velocity measurement , 2003 .

[21]  G. Witkamp,et al.  Inline determination of supersaturation and metastable zone width of MgSO4.12H2O with conductivity and refractive index measurement techniques , 2005 .

[22]  Kati Pöllänen,et al.  A Study on Batch Cooling Crystallization of Sulphathiazole: Process Monitoring Using ATR-FTIR and Product Characterization by Automated Image Analysis , 2006 .

[23]  M. Mazzotti,et al.  Precipitation of L‐Glutamic Acid: Determination of Nucleation Kinetics , 2006 .

[24]  B. Glennon,et al.  The Effect of Mixing on the Metastable Zone Width and Nucleation Kinetics in the Anti-Solvent Crystallization of Benzoic Acid , 2007 .

[25]  Dielectric Constants of Aqueous Diisopropanolamine, Diethanolamine, N-Methyldiethanolamine, Triethanolamine, and 2-Amino-2-methyl-1-propanol Solutions , 2007 .

[26]  L. L. Simon,et al.  Endoscopy-Based in Situ Bulk Video Imaging of Batch Crystallization Processes , 2009 .

[27]  Jianji Wang,et al.  Dielectric Constants for Binary Amino Acid−Water Solutions from (278.15 to 313.15) K , 2009 .

[28]  R. Tan,et al.  In Situ Determination of Metastable Zone Width Using Dielectric Constant Measurement , 2010 .