Modeling batch crystallization processes: Assumption verification and improvement of the parameter estimation quality through empirical experiment design

[1]  David W.T. Rippin,et al.  Simulation of single- and multiproduct batch chemical plants for optimal design and operation☆ , 1983 .

[2]  Narayan S. Tavare,et al.  BATCH CRYSTALLIZERS: A REVIEW , 1987 .

[3]  M. Kitamura,et al.  Growth process of ammonium sulfate crystals produced by secondary nucleation in stirred-tank crystallizer , 1991 .

[4]  J. Rawlings,et al.  Model identification and control of solution crystallization processes: a review , 1993 .

[5]  Robert J. Farrell,et al.  Modeling, simulation and kinetic parameter estimation in batch crystallization processes , 1994 .

[6]  Kohei Ogawa,et al.  The effect of mixedness on crystal size distribution in a continuous crystallizer , 1998 .

[7]  D. L. Ma,et al.  Optimal seeding in batch crystallization , 1999 .

[8]  Herman J. M. Kramer,et al.  The effect of the impeller speed on the product crystal size distribution (CSD) a 22 liter draft tube (DT) crystallizer , 1999 .

[9]  A. Mersmann,et al.  Brittle fracture in crystallization processes Part B. Growth of fragments and scale-up of suspension crystallizers , 1999 .

[10]  Alfons Mersmann,et al.  Brittle fracture in crystallization processes Part A. Attrition and abrasion of brittle solids , 1999 .

[11]  H. Kramer,et al.  Design of industrial crystallisers for a given product quality , 1999 .

[12]  Doraiswami Ramkrishna,et al.  Population Balances: Theory and Applications to Particulate Systems in Engineering , 2000 .

[13]  S. K. Bermingham,et al.  A design procedure and predictive models for solution crystallisation processes , 2000 .

[14]  A. M. Neumann.  Characterizing Industrial Crystallizers of Different Scale and Type , 2001 .

[15]  Masakuni Matsuoka,et al.  Secondary Growth Phenomena in Industrial Crystallization and Their Effects on Crystal Quality , 2002 .

[16]  Matthias Kind,et al.  Determination of the attrition behaviour of ammonium sulphate and of pentaerythritol crystals using a Forced Circulation Crystalliser , 2004 .

[17]  R. Braatz,et al.  Parameter Estimation and Optimization of a Loosely Bound Aggregating Pharmaceutical Crystallization Using in Situ Infrared and Laser Backscattering Measurements , 2004 .

[18]  H. Kramer,et al.  Application of Seeding as a Process Actuator in a Model Predictive Control Framework for Fed‐Batch Crystallization of Ammonium Sulphate , 2007 .

[19]  Yusuke Asakuma,et al.  Attrition behavior by micro-hardness parameters in suspension-crystallization processes , 2007 .

[20]  Keisuke Fukui,et al.  Fragmentation behavior of aggregated crystal in suspension crystallization processes , 2008 .

[21]  A. N. Kalbasenka,et al.  Model-Based Control of Industrial Batch Crystallizers : Experiments on Enhanced Controllability by Seeding Actuation , 2009 .