Fast-pulsing longitudinal relaxation optimized techniques: Enriching the toolbox of fast biomolecular NMR spectroscopy
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[1] R. Freeman,et al. Fast multidimensional NMR: radial sampling of evolution space. , 2005, Journal of magnetic resonance.
[2] L. Frydman,et al. Real-time 2D NMR identification of analytes undergoing continuous chromatographic separation. , 2004, Journal of the American Chemical Society.
[3] A. Redfield,et al. Dynamic range in Fourier transform proton magnetic resonance , 1975 .
[4] Rémy Sounier,et al. Sensitivity-optimized experiment for the measurement of residual dipolar couplings between amide protons , 2007, Journal of biomolecular NMR.
[5] P. Wright,et al. Sensitivity improvement in proton-detected two-dimensional heteronuclear correlation NMR spectroscopy , 1991 .
[6] R. R. Ernst,et al. Two‐dimensional spectroscopy. Application to nuclear magnetic resonance , 1976 .
[7] M. Deschamps,et al. Cooling overall spin temperature: protein NMR experiments optimized for longitudinal relaxation effects. , 2006, Journal of magnetic resonance.
[8] Ray Freeman,et al. The Radon Transform: A New Scheme for Fast Multidimensional NMR , 2004 .
[9] K. Kazimierczuk,et al. Optimization of random time domain sampling in multidimensional NMR. , 2008, Journal of magnetic resonance.
[10] M. Billeter,et al. Signal identification in NMR spectra with coupled evolution periods. , 2005, Journal of magnetic resonance.
[11] Lucio Frydman,et al. Single-scan NMR spectroscopy at arbitrary dimensions. , 2003, Journal of the American Chemical Society.
[12] M. Zweckstetter,et al. Mars - robust automatic backbone assignment of proteins , 2004, Journal of biomolecular NMR.
[13] Gaohua Liu,et al. NMR data collection and analysis protocol for high-throughput protein structure determination. , 2005, Proceedings of the National Academy of Sciences of the United States of America.
[14] V. Saudek,et al. Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions , 1992, Journal of biomolecular NMR.
[15] A. Pardi,et al. Longitudinal-relaxation-enhanced NMR experiments for the study of nucleic acids in solution. , 2009, Journal of the American Chemical Society.
[16] T. Szyperski,et al. Principles and applications of GFT projection NMR spectroscopy , 2006, Magnetic resonance in chemistry : MRC.
[17] K. Wüthrich,et al. Semi-classical nuclear spin relaxation theory revisited for use with biological macromolecules , 2002 .
[18] L. Kay,et al. Addressing the overlap problem in the quantitative analysis of two dimensional NMR spectra: Application to 15N relaxation measurements , 2004, Journal of biomolecular NMR.
[19] R. Konrat,et al. Direct methods and residue type specific isotope labeling in NMR structure determination and model-driven sequential assignment , 2008, Journal of biomolecular NMR.
[20] Alexander Grishaev,et al. CLOUDS, a protocol for deriving a molecular proton density via NMR , 2002, Proceedings of the National Academy of Sciences of the United States of America.
[21] Beat Vögeli,et al. Longitudinal (1)H relaxation optimization in TROSY NMR spectroscopy. , 2002, Journal of the American Chemical Society.
[22] J. Feigon,et al. Two-and three-dimensional HCN experiments for correlating base and sugar resonances in 15N, 13C-labeled RNA oligonucleotides , 1993, Journal of biomolecular NMR.
[23] E. Schrödinger. What is life? : the physical aspect of the living cell , 1944 .
[24] A. J. Shaka,et al. Progress on the two-dimensional filter diagonalization method. An efficient doubling scheme for two-dimensional constant-time NMR. , 2003, Journal of magnetic resonance.
[25] Lucio Frydman,et al. Progress in hyperpolarized ultrafast 2D NMR spectroscopy. , 2008, Chemphyschem : a European journal of chemical physics and physical chemistry.
[26] Ray Freeman,et al. Fast multidimensional NMR by polarization sharing , 2007, Magnetic resonance in chemistry : MRC.
[27] K. Kazimierczuk,et al. Random sampling of evolution time space and Fourier transform processing , 2006, Journal of biomolecular NMR.
[28] Ray Freeman,et al. Band-selective radiofrequency pulses , 1991 .
[29] Ray Freeman,et al. Distant echoes of the accordion: Reduced dimensionality, GFT-NMR, and projection-reconstruction of multidimensional spectra , 2004 .
[30] J. Covès,et al. Optimized set of two-dimensional experiments for fast sequential assignment, secondary structure determination, and backbone fold validation of 13C/15N-labelled proteins , 2003, Journal of biomolecular NMR.
[31] I. Campbell,et al. Short selective pulses for biochemical applications. , 1995, Journal of magnetic resonance. Series B.
[32] Gaohua Liu,et al. Probing structure and functional dynamics of (large) proteins with aromatic rings: L-GFT-TROSY (4,3)D HCCH NMR spectroscopy. , 2005, Journal of the American Chemical Society.
[33] E. Olejniczak,et al. Are methyl groups relaxation sinks in small proteins , 1990 .
[34] W. Gronwald,et al. Automated structure determination of proteins by NMR spectroscopy , 2004 .
[35] G. Wider,et al. 3D 13C-15N-heteronuclear two-spin coherence spectroscopy for polypeptide backbone assignments in 13C-15N-double-labeled proteins , 1993, Journal of biomolecular NMR.
[36] Vladislav Yu Orekhov,et al. Removal of a time barrier for high-resolution multidimensional NMR spectroscopy , 2006, Nature Methods.
[37] Nicolas Pannetier,et al. Optimized 3D-NMR sampling for resonance assignment of partially unfolded proteins. , 2007, Journal of magnetic resonance.
[38] B Brutscher,et al. Assignment of NMR spectra of proteins using triple-resonance two-dimensional experiments , 1994, Journal of biomolecular NMR.
[39] B. Brutscher,et al. Determination of an Initial Set of NOE-Derived Distance Constraints for the Structure Determination of15N/13C-Labeled Proteins , 1995 .
[40] T. Szyperski,et al. GFT NMR, a new approach to rapidly obtain precise high-dimensional NMR spectral information. , 2003, Journal of the American Chemical Society.
[41] A. Stern,et al. Resolution and sensitivity of high field nuclear magnetic resonance spectroscopy , 2004, Journal of biomolecular NMR.
[42] Ultrafast-based projection-reconstruction three-dimensional nuclear magnetic resonance spectroscopy. , 2007, The Journal of chemical physics.
[43] E. Aragón,et al. Fast 2D NMR ligand screening using Hadamard spectroscopy. , 2006, Journal of the American Chemical Society.
[44] G. Wider. Technical aspects of NMR Spectroscopy with biological macromolecules and studies of hydration in solution , 1998 .
[45] Thomas Szyperski,et al. Rapid NMR data collection. , 2005, Methods in enzymology.
[46] Lucio Frydman,et al. Interlaced Fourier transformation of ultrafast 2D NMR data. , 2005, Journal of magnetic resonance.
[47] G. L. Kenyon,et al. Studies of macromolecular structure by 13 C nuclear magnetic resonance. II. A specific labeling approach to the study of histidine residues in proteins. , 1973, Journal of the American Chemical Society.
[48] Lucio Frydman,et al. Ultrafast 2D NMR spectroscopy using a continuous spatial encoding of the spin interactions. , 2004, Journal of magnetic resonance.
[49] Paul Schanda,et al. Speeding up three-dimensional protein NMR experiments to a few minutes. , 2006, Journal of the American Chemical Society.
[50] Alan S. Stern,et al. NMR Data Processing , 1996 .
[51] R. Freeman,et al. Hadamard NMR Spectroscopy , 2003 .
[52] Harald Schwalbe,et al. Time-resolved NMR studies of RNA folding. , 2007, Biopolymers.
[53] I. Ayala,et al. Fast two-dimensional NMR spectroscopy of high molecular weight protein assemblies. , 2009, Journal of the American Chemical Society.
[54] Paul A. Keifer,et al. Pure absorption gradient enhanced heteronuclear single quantum correlation spectroscopy with improved sensitivity , 1992 .
[55] Lewis E. Kay,et al. Quantitative dynamics and binding studies of the 20S proteasome by NMR , 2007, Nature.
[56] R. Freeman,et al. Frequency-domain Hadamard spectroscopy. , 2003, Journal of magnetic resonance.
[57] R. Riek,et al. Attenuated T2 relaxation by mutual cancellation of dipole-dipole coupling and chemical shift anisotropy indicates an avenue to NMR structures of very large biological macromolecules in solution. , 1997, Proceedings of the National Academy of Sciences of the United States of America.
[58] P. Schanda,et al. HET‐SOFAST NMR for fast detection of structural compactness and heterogeneity along polypeptide chains , 2006, Magnetic resonance in chemistry : MRC.
[59] R. Freeman,et al. Projection-reconstruction of three-dimensional NMR spectra. , 2003, Journal of the American Chemical Society.
[60] J. Prestegard,et al. Quantitation of rapid proton-deuteron amide exchange using hadamard spectroscopy , 2004, Journal of biomolecular NMR.
[61] Lucio Frydman,et al. The acquisition of multidimensional NMR spectra within a single scan , 2002, Proceedings of the National Academy of Sciences of the United States of America.
[62] G. Lipari. Model-free approach to the interpretation of nuclear magnetic resonance relaxation in macromolecules , 1982 .
[63] A. Pardi,et al. Resolution-Enhanced Base-Type-Edited HCN Experiment for RNA , 2005, Journal of biomolecular NMR.
[64] Ray Freeman,et al. Wideband Excitation with Polychromatic Pulses , 1994 .
[65] A. Sherry,et al. Sensitivity enhancement of multidimensional NMR experiments by paramagnetic relaxation effects. , 2006, Journal of the American Chemical Society.
[66] Shang-Te Danny Hsu,et al. Structure and dynamics of a ribosome-bound nascent chain by NMR spectroscopy , 2007, Proceedings of the National Academy of Sciences.
[67] Thomas Szyperski,et al. G-matrix Fourier transform NMR spectroscopy for complete protein resonance assignment. , 2004, Proceedings of the National Academy of Sciences of the United States of America.
[68] D. LeMaster. Deuteration in protein proton magnetic resonance. , 1989, Methods in enzymology.
[69] K Wüthrich,et al. Protein hydration in aqueous solution. , 1992, Faraday discussions.
[70] Dominique Marion,et al. Fast acquisition of NMR spectra using Fourier transform of non-equispaced data , 2005, Journal of biomolecular NMR.
[71] L. Frydman,et al. Ultrafast solid-state 2D NMR experiments via orientational encoding. , 2006, Journal of the American Chemical Society.
[72] D. Jeannerat. Computer optimized spectral aliasing in the indirect dimension of (1)H-(13)C heteronuclear 2D NMR experiments. A new algorithm and examples of applications to small molecules. , 2007, Journal of magnetic resonance.
[73] Ray Freeman,et al. Projection-reconstruction technique for speeding up multidimensional NMR spectroscopy. , 2004, Journal of the American Chemical Society.
[74] A. Pardi,et al. Measurement of imino 1H–1H residual dipolar couplings in RNA , 2009, Journal of biomolecular NMR.
[75] J. Simorre,et al. Amino acid-type edited NMR experiments for methyl-methyl distance measurement in 13C-labeled proteins. , 2004, Journal of the American Chemical Society.
[76] R. Freeman,et al. New methods for fast multidimensional NMR , 2003, Journal of biomolecular NMR.
[77] P. Schanda,et al. Hadamard frequency-encoded SOFAST-HMQC for ultrafast two-dimensional protein NMR. , 2006, Journal of magnetic resonance.
[78] V. Sklenar,et al. Transverse relaxation optimized triple-resonance NMR experiments for nucleic acids , 2000, Journal of biomolecular NMR.
[79] Gerhard Wagner,et al. Looking into live cells with in-cell NMR spectroscopy. , 2007, Journal of structural biology.
[80] Alexander Eletsky,et al. A novel strategy for the assignment of side-chain resonances in completely deuterated large proteins using 13C spectroscopy , 2003, Journal of biomolecular NMR.
[81] P. Schanda,et al. A set of BEST triple-resonance experiments for time-optimized protein resonance assignment. , 2007, Journal of magnetic resonance.
[82] K Wüthrich,et al. Protein hydration in aqueous solution. , 1991, Science.
[83] D. Marion. Processing of ND NMR spectra sampled in polar coordinates: a simple Fourier transform instead of a reconstruction , 2006, Journal of biomolecular NMR.
[84] S. Grzesiek,et al. The Importance of Not Saturating H2o in Protein NMR : application to Sensitivity Enhancement and Noe Measurements , 1993 .
[85] Paul Schanda,et al. Protein folding and unfolding studied at atomic resolution by fast two-dimensional NMR spectroscopy , 2007, Proceedings of the National Academy of Sciences.
[86] M. Billeter,et al. MUNIN: A new approach to multi-dimensional NMR spectra interpretation , 2001, Journal of biomolecular NMR.
[87] Brian E Coggins,et al. High resolution 4-D spectroscopy with sparse concentric shell sampling and FFT-CLEAN , 2008, Journal of biomolecular NMR.
[88] Arthur G. Palmer,et al. Sensitivity improvement in proton-detected two-dimensional heteronuclear relay spectroscopy , 1991 .
[89] Jonas Fredriksson,et al. PRODECOMPv3: decompositions of NMR projections for protein backbone and side-chain assignments and structural studies , 2008, Bioinform..
[90] R. Ishima,et al. Proton spin relaxation in biopolymers at high magnetic fields , 1990 .
[91] Vladislav Yu Orekhov,et al. Optimizing resolution in multidimensional NMR by three-way decomposition , 2003, Journal of biomolecular NMR.
[92] Vladislav Yu Orekhov,et al. Hyperdimensional NMR spectroscopy with nonlinear sampling. , 2008, Journal of the American Chemical Society.
[93] Brian E Coggins,et al. Filtered backprojection for the reconstruction of a high-resolution (4,2)D CH3-NH NOESY spectrum on a 29 kDa protein. , 2005, Journal of the American Chemical Society.
[94] R. Lauffer,et al. Gadolinium(III) Chelates as MRI Contrast Agents: Structure, Dynamics, and Applications. , 1999, Chemical reviews.
[95] Ray Freeman,et al. Fast multi-dimensional Hadamard spectroscopy. , 2003, Journal of magnetic resonance.
[96] G. Bodenhausen,et al. Principles of nuclear magnetic resonance in one and two dimensions , 1987 .
[97] Paul T. Matsudaira,et al. NMR structure of the 35-residue villin headpiece subdomain , 1997, Nature Structural Biology.
[98] Martin Billeter,et al. High-throughput analysis of protein NMR spectra , 2005 .
[99] L. Frydman,et al. Principles and progress in ultrafast multidimensional nuclear magnetic resonance. , 2009, Annual review of physical chemistry.
[100] Hidekazu Hiroaki,et al. High-resolution multi-dimensional NMR spectroscopy of proteins in human cells , 2009, Nature.
[101] J. Simorre,et al. Computer assignment of the backbone resonances of labelled proteins using two-dimensional correlation experiments , 1995, Journal of biomolecular NMR.
[102] B. Brutscher,et al. Hadamard amino-acid-type edited NMR experiment for fast protein resonance assignment. , 2008, Journal of the American Chemical Society.
[103] Brian D Sykes,et al. Smartnotebook: A semi-automated approach to protein sequential NMR resonance assignments , 2003, Journal of biomolecular NMR.
[104] P. Schanda,et al. UltraSOFAST HMQC NMR and the repetitive acquisition of 2D protein spectra at Hz rates. , 2007, Journal of the American Chemical Society.
[105] R. R. Ernst,et al. Application of Fourier Transform Spectroscopy to Magnetic Resonance , 1966 .
[106] Kurt Wüthrich,et al. APSY-NMR with proteins: practical aspects and backbone assignment , 2008, Journal of biomolecular NMR.
[107] J. Boisbouvier,et al. Parallel screening and optimization of protein constructs for structural studies , 2009, Protein science : a publication of the Protein Society.
[108] J. Keeler,et al. Minimizing Sensitivity Losses in Gradient-Selected 15N-1H HSQC Spectra of Proteins , 1994 .
[109] Paul Schanda,et al. Very fast two-dimensional NMR spectroscopy for real-time investigation of dynamic events in proteins on the time scale of seconds. , 2005, Journal of the American Chemical Society.
[110] D. LeMaster,et al. Deuterium labelling in NMR structural analysis of larger proteins , 1990, Quarterly Reviews of Biophysics.
[111] R. Brüschweiler,et al. Covariance nuclear magnetic resonance spectroscopy. , 2004, The Journal of chemical physics.
[112] G. Wider,et al. Reduced dimensionality in triple-resonance NMR experiments , 1993 .
[113] L. Frydman,et al. Real-time monitoring of chemical transformations by ultrafast 2D NMR spectroscopy. , 2006, Journal of the American Chemical Society.
[114] Cheryl H Arrowsmith,et al. Solution NMR in structural genomics. , 2006, Current opinion in structural biology.
[115] Manfred Spraul,et al. Cryogenically cooled probes—a leap in NMR technology , 2005 .
[116] M. Rance,et al. Sensitivity improvement in isotropic mixing (TOCSY) experiments , 1990 .
[117] D. LeMaster. Uniform and selective deuteration in two-dimensional NMR of proteins. , 1990, Annual review of biophysics and biophysical chemistry.
[118] Christopher M Dobson,et al. Principles of protein folding, misfolding and aggregation. , 2004, Seminars in cell & developmental biology.
[119] Folding of the KIX domain: characterization of the equilibrium analog of a folding intermediate using 15N/13C relaxation dispersion and fast 1H/2H amide exchange NMR spectroscopy. , 2008, Journal of molecular biology.
[120] T. Malliavin,et al. Gifa V. 4: A complete package for NMR data set processing , 1996, Journal of biomolecular NMR.
[121] L. Mueller. Alternate HMQC experiments for recording HN and HC-correlation spectra in proteins at high throughput , 2008, Journal of biomolecular NMR.
[122] R. Freeman,et al. Resolving ambiguities in two-dimensional NMR spectra: the 'TILT' experiment. , 2005, Journal of magnetic resonance.
[123] Kurt Wüthrich,et al. The use of cross-sections and of projections in two-dimensional NMR spectroscopy , 1978 .
[124] G. Wider,et al. Managing the solvent water polarization to obtain improved NMR spectra of large molecular structures , 2005, Journal of biomolecular NMR.
[125] Sebastian Hiller,et al. Automated NMR assignment of protein side chain resonances using automated projection spectroscopy (APSY). , 2008, Journal of the American Chemical Society.
[126] Paul Schanda,et al. SOFAST-HMQC Experiments for Recording Two-dimensional Deteronuclear Correlation Spectra of Proteins within a Few Seconds , 2005, Journal of biomolecular NMR.
[127] J. Simorre,et al. Design of a Complete Set of Two-Dimensional Triple-Resonance Experiments for Assigning Labeled Proteins , 1994 .
[128] H. Senn,et al. Fast-HMQC using Ernst angle pulses: An efficient tool for screening of ligand binding to target proteins , 1997, Journal of biomolecular NMR.
[130] Arash Bahrami,et al. High-resolution iterative frequency identification for NMR as a general strategy for multidimensional data collection. , 2005, Journal of the American Chemical Society.
[131] A. Szabó,et al. Model-free approach to the interpretation of nuclear magnetic resonance relaxation in macromolecules. 1. Theory and range of validity , 1982 .
[132] A. J. Shaka,et al. The multidimensional filter diagonalization method. , 2000, Journal of magnetic resonance.
[133] An improved ultrafast 2D NMR experiment: Towards atom-resolved real-time studies of protein kinetics at multi-Hz rates , 2009, Journal of biomolecular NMR.
[134] Peter Güntert,et al. Automated assignment of NMR chemical shifts using peak-particle dynamics simulation with the DYNASSIGN algorithm , 2009, Journal of biomolecular NMR.
[135] Brian E. Coggins,et al. (4,2)D Projection--reconstruction experiments for protein backbone assignment: application to human carbonic anhydrase II and calbindin D(28K). , 2005, Journal of the American Chemical Society.
[136] R. Kaptein,et al. Extended Flip-back Schemes for Sensitivity Enhancement in Multidimensional HSQC-type Out-and-back Experiments , 2005, Journal of biomolecular NMR.
[137] V. Orekhov,et al. Targeted acquisition for real-time NMR spectroscopy. , 2006, Journal of the American Chemical Society.
[138] Dmitry M Korzhnev,et al. Probing invisible, low-populated States of protein molecules by relaxation dispersion NMR spectroscopy: an application to protein folding. , 2008, Accounts of chemical research.
[139] P. Schanda,et al. Automated spectral compression for fast multidimensional NMR and increased time resolution in real-time NMR spectroscopy. , 2007, Journal of the American Chemical Society.
[140] Philippe Pelupessy,et al. Adiabatic single scan two-dimensional NMR spectrocopy. , 2003, Journal of the American Chemical Society.
[141] David Neuhaus,et al. The Nuclear Overhauser Effect in Structural and Conformational Analysis , 1989 .
[142] Lucio Frydman,et al. Ultrafast two-dimensional nuclear magnetic resonance spectroscopy of hyperpolarized solutions , 2007 .