Influence of different light sources on the conversion of composite resins.

AIMS The purpose of this paper was to evaluate the influence of different light curing units on the conversion of four composite resins with different compositions (Durafill VS - Heraeus-Kulzer, Tetric Ceram - Ivoclar/Vivadent, Filtek Supreme XT - 3M ESPE e Aelite LS Packable - Bisco), using differential scanning calorimetry. MATERIALS AND METHODS A stainless steel matrix was used to prepare 48 cylindrical composite test samples (n=6), measuring 3 mm in diameter and 1 mm in thickness. The samples were photoactivated using a halogen lamp (Optilux 500 - Demetron/Kerr) and three different generations of light-emitting diodes (LEDs) (LEC-470 I - MMOptics, Radii Plus - SDI and Ultra-Lume LED 5 - Ultradent). After removal of the matrix, each sample was weighed and hermetically sealed in an aluminum pan and analyzed. The amount of heat liberated by thermopolymerisation of residual monomers after photoactivation was measured in Joules/gram (J/g). The data were submitted to Analysis of Variance (ANOVA) test (P ≤ 0.002) and the Tukey test (P < 0.05). RESULTS The Ultra-Lume LED 5 was superior on degree of conversion for all resins. The Radii Plus was equal to the Ultra-Lume LED 5, except for the resin Tetric Ceram , were the Optilux 500 was superior. The LEC-470 I was inferior for the conversion of all resins. CONCLUSION The study proves the importance of the compatibility of the different photoinitiators in resin composites with the different light sources.

[1]  J. R. Saad,et al.  Analysis of camphorquinone in composite resins as a function of shade. , 2007, Dental materials : official publication of the Academy of Dental Materials.

[2]  Carla C Schmitt,et al.  The initiating radical yields and the efficiency of polymerization for various dental photoinitiators excited by different light curing units. , 2006, Dental materials : official publication of the Academy of Dental Materials.

[3]  N. Emami,et al.  Influence of light-curing procedures and photo-initiator/co-initiator composition on the degree of conversion of light-curing resins , 2005, Journal of materials science. Materials in medicine.

[4]  H. Lygre,et al.  Identification of organic eluates from four polymer-based dental filling materials. , 2003, European journal of oral sciences.

[5]  L. G. Lopes,et al.  Conceitos atuais na polimerização de sistemas restauradores resinosos , 2003 .

[6]  A. Peutzfeldt,et al.  Light-emitting diode curing: influence on selected properties of resin composites. , 2003, Quintessence international.

[7]  C. A. de Carvalho Zavaglia,et al.  The monomeric formulation optimization of dental composite: mechanical and kinetic studies. , 2003, Artificial organs.

[8]  Y-K Lee,et al.  Degree of polymerization of resin composites by different light sources. , 2002, Journal of oral rehabilitation.

[9]  F. Rueggeberg,et al.  Shedding new light on composite polymerization. , 2002, Operative dentistry.

[10]  K. Jandt,et al.  High power light emitting diode (LED) arrays versus halogen light polymerization of oral biomaterials: Barcol hardness, compressive strength and radiometric properties. , 2002, Biomaterials.

[11]  R. L. Reis,et al.  Estatística aplicada a experimentação animal , 2002 .

[12]  M. Okazaki,et al.  Thermal analysis of dental resins cured with blue light-emitting diodes (LEDs). , 2002, Journal of biomedical materials research.

[13]  A. Delbem,et al.  [Microhardness of resins as a function of color and halogen light]. , 2002, Pesquisa odontologica brasileira = Brazilian oral research.

[14]  D. Decker,et al.  Performance analysis of acylphosphine oxides in photoinitiated polymerization , 2001 .

[15]  J Sutalo,et al.  Degree of conversion and temperature rise during polymerization of composite resin samples with blue diodes. , 2001, Journal of oral rehabilitation.

[16]  J F McCabe,et al.  Degree of conversion of composites measured by DTA and FTIR. , 2001, Dental materials : official publication of the Academy of Dental Materials.

[17]  M. Okazaki,et al.  The relationship between leachability of polymerization initiator and degree of conversion of visible light-cured resin. , 2001, Journal of biomedical materials research.

[18]  K. Chae,et al.  Properties of 2,3-butanedione and 1-phenyl-1,2-propanedione as new photosensitizers for visible light cured dental resin composites , 2000 .

[19]  T. Hayakawa,et al.  Analysis of polymerization behavior of dental dimethacrylate monomers by differential scanning calorimetry. , 1999, Journal of oral science.

[20]  V. Yamuna,et al.  Effect of initiator concentration, exposure time and particle size of the filler upon the mechanical properties of a light-curing radiopaque dental composite. , 1998, Journal of oral rehabilitation.

[21]  W. Geurtsen,et al.  Substances released from dental resin composites and glass ionomer cements. , 1998, European journal of oral sciences.

[22]  I Stangel,et al.  High-pressure infrared and FT-Raman investigation of a dental composite. , 1997, Biomaterials.

[23]  F. Rueggeberg,et al.  Effect of photoinitiator level on properties of a light-cured and post-cure heated model resin system. , 1997, Dental materials : official publication of the Academy of Dental Materials.

[24]  J. Ferracane,et al.  Wear and Marginal Breakdown of Composites with Various Degrees of Cure , 1997, Journal of dental research.

[25]  A. Maffezzoli,et al.  Thermal analysis of visible-light-activated dental composites , 1995 .

[26]  R. Mills Blue light emitting diodes--another method of light curing? , 1995, British Dental Journal.

[27]  R. Nomoto,et al.  Effect of light intensity on polymerization of light-cured composite resins. , 1994, Dental materials journal.

[28]  E. Greener,et al.  Effect of photoinitiator on degree of conversion of unfilled light-cured resin. , 1994, Journal of dentistry.

[29]  J. Vaidyanathan,et al.  Thermoanalytical characterization of visible light cure dental composites. , 1992, Journal of oral rehabilitation.

[30]  G. Koch,et al.  Cure profiles of visible-light-cured Class II composite restorations in vivo and in vitro. , 1992, Dental materials : official publication of the Academy of Dental Materials.

[31]  A. Peutzfeldt,et al.  Hardness of restorative resins: effect of camphorquinone, amine, and inhibitor. , 1989, Acta odontologica Scandinavica.

[32]  M. Taira,et al.  Analysis of Photo-initiators in Visible-light-cured Dental Composite Resins , 1988, Journal of dental research.

[33]  J. Antonucci,et al.  Extent of Polymerization of Dental Resins by Differential Scanning Calorimetry , 1983, Journal of dentistry research.

[34]  R. Bowen Properties of a silica-reinforced polymer for dental restorations. , 1963, Journal of the American Dental Association.