In-process detection of microstructural changes in laser cladding of in-situ Inconel 718/TiC metal matrix composite coating

Abstract Online monitoring of thermal history during laser cladding of Inconel 718/TiC metal matrix composite (MMC) produced by in-situ process was carried out. Effects of weight percentage of Ti+C and process parameters on the thermal history, and its correlation with the evolution of microstructure were studied. Further, changes in the evolution of microstructure and excessive dilution were identified online by monitoring various features of the thermo-cycle profile, i.e. occurrence of undercooling with change in microstructure from dispersed fine particles to dendritic structure caused by assembling of floating TiC particles at slow cooling, molten pool lifetime and shift in solidification shelf location because of compositional changes caused by excessive dilution. Coating with dispersed fine TiC particles exhibited high hardness and good wear characteristics compared to the one with dendritic structure. Further, dendritic growth of TiC particles resulted in embrittlement of the coating. Cladding was also carried out in laser power modulated mode to enhance the cooling rate, thereby refining the microstructure. Identification of optimum parameters through real-time monitoring of molten pool thermal history and its physical state (liquid/solid) during laser power modulation to ensure refinement of microstructure was studied. SEM and XRD analyses were carried out for analysing the microstructure and phases.

[1]  Ashish Kumar Nath,et al.  Online monitoring of thermo-cycles and its correlation with microstructure in laser cladding of nickel based super alloy , 2017 .

[2]  Fangzhou Han,et al.  In situ production of Fe–TiC surface composite coatings by tungsten-inert gas heat source , 2006 .

[3]  Ashish Kumar Nath,et al.  Online assessment of TiC decomposition in laser cladding of metal matrix composite coating , 2017 .

[4]  A. Nath,et al.  Development of a hard nano-structured multi-component ceramic coating by laser cladding , 2009 .

[5]  M. Savalani,et al.  In situ formation of titanium carbide using titanium and carbon-nanotube powders by laser cladding , 2012 .

[6]  M. Mojtahedi,et al.  Solidification microstructure of in-situ laser-synthesized Fe-TiC hard coating , 2016 .

[7]  Shih-Hsien Chang,et al.  Effects of Particle Size on Mechanical Properties of a TiC Containing Tool Steel by Hot Isostatic Press , 2008 .

[8]  Liang Hou,et al.  Additive manufacturing and its societal impact: a literature review , 2013 .

[9]  Jenn‐Ming Yang,et al.  In-situ formation of novel TiC-particle-reinforced 316L stainless steel bulk-form composites by selective laser melting , 2017 .

[10]  G. Flamant,et al.  Real-time optical pyrometer in laser machining , 1994 .

[11]  C. Cui,et al.  In situ TiC particles reinforced grey cast iron composite fabricated by laser cladding of Ni-Ti-C system , 2007 .

[12]  J. Sabbaghzadeh,et al.  Effect of pulsed laser parameters on in-situ TiC synthesis in laser surface treatment , 2011 .

[13]  Mohammad H. Farshidianfar,et al.  Real-time monitoring and prediction of martensite formation and hardening depth during laser heat treatment , 2017 .

[14]  Juan Pou,et al.  Theoretical and experimental analysis of high power diode laser (HPDL) hardening of AISI 1045 steel , 2007 .

[15]  D. Bandyopadhyay,et al.  The Ti-Ni-C system (titanium-nickel-carbon) , 2000 .

[16]  M. Doubenskaia,et al.  Optical monitoring of Nd : YAG laser cladding , 2004 .

[17]  A. Khajepour,et al.  The influence of combined laser parameters on in-situ formed TiC morphology during laser cladding , 2011 .

[18]  Ashish Kumar Nath,et al.  Monitoring and assessment of tungsten carbide wettability in laser cladded metal matrix composite coating using an IR pyrometer , 2017 .

[19]  G. Flamant,et al.  Surface temperature measurements during pulsed laser action on metallic and ceramic materials , 1996 .

[20]  R. Kovacevic,et al.  Hardness prediction in multi-pass direct diode laser heat treatment by on-line surface temperature monitoring , 2012 .

[21]  Xueqiang Cao,et al.  Fabrication and properties of Al2O3–TiB2–TiC/Al metal matrix composite coatings by atmospheric plasma spraying of SHS powders , 2016 .

[22]  Reinhart Poprawe,et al.  Identification and qualification of temperature signal for monitoring and control in laser cladding , 2006 .

[23]  Reinhart Poprawe,et al.  Development and qualification of a novel laser-cladding head with integrated sensors , 2007 .

[24]  M. Savalani,et al.  High temperature wear characteristics of TiC composite coatings formed by laser cladding with CNT additives , 2014 .

[25]  Aravinda Kar,et al.  Tensile Strengths for Laser-Fabricated Parts and Similarity Parameters for Rapid Manufacturing , 2001 .

[26]  A. Saidi,et al.  Reaction Synthesis of TiC and Fe-TiC Composites* , 1997 .

[27]  Z. Zou,et al.  Characterization of in situ synthesized TiC particle reinforced Fe-based composite coatings produced by multi-pass overlapping GTAW melting process , 2007 .

[28]  Huiyuan Wang,et al.  In situ synthesis of TiC/Mg composites in molten magnesium , 2003 .

[29]  R. Kocich,et al.  The Methods of Preparation of Ti-Ni-X Alloys and Their Forming , 2013 .

[30]  M. Zhang,et al.  Microstructure and wear properties of TiC/FeCrBSi surface composite coating prepared by laser cladding , 2008 .

[31]  Petri Vuoristo,et al.  Microstructure and properties of hard and wear resistant MMC coatings deposited by laser cladding , 2009 .

[32]  J. K. Watson,et al.  A decision-support model for selecting additive manufacturing versus subtractive manufacturing based on energy consumption. , 2018, Journal of cleaner production.

[33]  Jean-Pierre Kruth,et al.  Feedback control of Layerwise Laser Melting using optical sensors , 2010 .

[34]  A. Khajepour,et al.  Thermal monitoring of microstructure and carbide morphology in direct metal deposition of Fe-Ti-C metal matrix composites , 2017 .

[35]  Ashish Kumar Nath,et al.  Effect of laser operating mode in paint removal with a fiber laser , 2013 .

[36]  Antti Salminen,et al.  Monitoring and Adaptive Control of Laser Processes , 2014 .

[37]  Y. Pei,et al.  Gradient microstructure in laser clad TiC-reinforced Ni-alloy composite coating , 1998 .

[38]  R. Poprawe,et al.  Characterization of the process control for the direct laser metallic powder deposition , 2006 .

[39]  G. Flamant,et al.  Two-dimensional resolution pyrometer for real-time monitoring of temperature image in laser materials processing , 1997 .

[40]  Xiaolei Wu In situ formation by laser cladding of a TiC composite coating with a gradient distribution , 1999 .

[41]  A. Khajepour,et al.  Effect of laser cladding process parameters on clad quality and in-situ formed microstructure of Fe-TiC composite coatings , 2010 .

[43]  L. Martinu,et al.  Cavitation erosion mechanisms in stainless steels and in composite metal–ceramic HVOF coatings , 2016 .

[44]  Jan Bültmann,et al.  Design of an Optical system for the In Situ Process Monitoring of Selective Laser Melting (SLM) , 2011 .

[45]  Jean-Pierre Kruth,et al.  Determination of geometrical factors in Layerwise Laser Melting using optical process monitoring , 2011 .