Microstructures of Rene 142 nickel-based superalloy fabricated by electron beam melting

Abstract Rene 142, a commercial, columnar grained, gas turbine airfoil Ni-based superalloy, has been fabricated from a pre-alloyed, atomized powder by additive manufacturing using electron beam melting. Monolithic components having [0 0 1] oriented, columnar grain structures exhibited a creep-optimized 59% volume fraction of cuboidal, coherent, γ ′-phase precipitates averaging 275 nm on the side, and with γ / γ ′ channel widths ranging from 25 to 75 nm. Transmission electron microscopy, utilizing bright and dark field imaging of optimally oriented γ / γ ′ interfaces showed prominent misfit coherency strains as δ-fringe patterns. Corresponding hardness measurements also indicated the possibility of creep strength comparable with the commercial alloy. The notable feature of this study was the monolithic development of desirable superalloy properties without conventional, multi-step heat treatments.

[1]  J.L. Martinez,et al.  Comparison of Microstructures and Mechanical Properties for Solid and Mesh Cobalt-Base Alloy Prototypes Fabricated by Electron Beam Melting , 2010 .

[2]  G. S. Ansell,et al.  The influence of coherency strain on the elevated temperature tensile behavior of Ni-15Cr-AI-Ti-Mo alloys , 1981 .

[3]  Toshiharu Kobayashi,et al.  Creep behaviour of Ni-base single-crystal superalloys with various γ' volume fraction , 2004 .

[4]  S. Amelinckx,et al.  Electron Microscope Transmission Images of Coherent Domain Boundaries I. Dynamical Theory , 1964 .

[5]  M. E. Shank,et al.  The development of columnar grain and single crystal high temperature materials through directional solidification , 1970 .

[6]  Madeleine Durand-Charre,et al.  The microstructure of superalloys , 1997 .

[7]  T. Pollock,et al.  Nickel-Based Superalloys for Advanced Turbine Engines: Chemistry, Microstructure and Properties , 2006 .

[8]  L. Murr,et al.  Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting , 2012 .

[9]  J. Tien,et al.  The effect of orientation and sense of applied uniaxial stress on the morphology of coherent gamma prime precipitates in stress annealed nickel-base superalloy crystals , 1971 .

[10]  R. Fischer,et al.  Investigations of MX and γ′/γ″ precipitates in the nickel-based superalloy 718 produced by electron beam melting , 2008 .

[11]  S. Amelinckx,et al.  Electron Microscope Transmission Images of Coherent Domain Boundaries II. Observations , 1964 .

[12]  A. Pineau Influence of uniaxial stress on the morphology of coherent precipitates during coarsening—elastic energy considerations , 1976 .

[13]  T. Pollock,et al.  Determination of matrix and precipitate elastic constants in (γ–γ′) Ni-base model alloys, and their relevance to rafting , 1999 .

[14]  L. Murr,et al.  Microstructural Architecture, Microstructures, and Mechanical Properties for a Nickel-Base Superalloy Fabricated by Electron Beam Melting , 2011 .

[15]  R. C. Ecob,et al.  The growth of γ′ precipitates in nickel-base superalloys , 1983 .

[16]  A. Ardell Diffraction contrast at planar interfaces of large coherent precipitates , 1967 .

[17]  L. Murr,et al.  Contributions of Light Microscopy to Contemporary Materials Characterization: The New Directional Solidification , 2012, Metallography, Microstructure, and Analysis.