Influence of dissolved oxygen concentration on the oxide film formed on 304 stainless steel in high temperature water

Abstract Characteristics of the oxide films formed on 304 stainless steel under different dissolved oxygen (DO) concentrations in 290 °C water were investigated. Less hematite and more spinel oxides form on fresh sample as DO decreases. Meanwhile, relative Cr content in the film increases. Spinel develops on the film preformed under 3 ppm DO when it was further immersed under DO below 5 ppb while the preformed hematite degrades. The spinel preformed under DO below 5 ppb still grows up when further immersed under 3 ppm DO while the base layer becomes more porous due to dissolution of Cr.

[1]  V. Maroni,et al.  Spectroscopic characterization of oxide films on type 304 SS exposed to water at 289° C: correlation with the Fe-Cr-H2O pourbaix diagram☆ , 1990 .

[2]  N. Ichikawa,et al.  General Corrosion of Materials under Simulated BWR Primary Water Conditions , 1994 .

[3]  T. Terachi,et al.  Characterization of Oxide Film Behaviors on 316 Stainless Steels in High Temperature Water - Influence of Hydrogen and Oxygen Considerations for Initiation of SCC , 2006 .

[4]  B. Beverskog,et al.  Pourbaix Diagrams for the Ternary System of Iron-Chromium-Nickel , 1999 .

[5]  G. McRae,et al.  The corrosion of Alloy 690 in high-temperature aqueous media : thermodynamic considerations , 2001 .

[6]  T. Yamashita,et al.  Analysis of XPS spectra of Fe2+ and Fe3+ ions in oxide materials , 2008 .

[7]  K. Lundgren,et al.  Influence of Zn on the oxide layer on AISI 316L(NG) stainless steel in simulated pressurised water reactor coolant , 2009 .

[8]  Y. J. Kim Characterization of the Oxide Film Formed on Type 316 Stainless Steel in 288°C Water in Cyclic Normal and Hydrogen Water Chemistries , 1995 .

[9]  J. Robertson The mechanism of high temperature aqueous corrosion of stainless steels , 1991 .

[10]  E. Han,et al.  Effects of temperature on the oxide film properties of 304 stainless steel in high temperature lithium borate buffer solution , 2009 .

[11]  D. Mills Corrosion in the nuclear power industry , 2007 .

[12]  Chien-chang Lin A review of corrosion product transport and radiation field buildup in boiling water reactors , 2009 .

[13]  I. Sutherland,et al.  On the oxide formation on stainless steels AISI 304 and incoloy 800H investigated with XPS , 1987 .

[14]  M. Hanson,et al.  Corrosion behavior of 304 stainless steel in high temperature, hydrogenated water , 2001 .

[15]  E. Han,et al.  The oxidation behaviour of 304 stainless steel in oxygenated high temperature water , 2010 .

[16]  Y. Sugita,et al.  Synergy Effect of Simultaneous Zinc and Nickel Addition on Cobalt Deposition onto Stainless Steel in Oxygenated High Temperature Water , 2003 .

[17]  E. Han,et al.  Effect of nickel ion from autoclave material on oxidation behaviour of 304 stainless steel in oxygenated high temperature water , 2011 .

[18]  P. Andresen,et al.  Data Quality, Issues, and Guidelines for Electrochemical Corrosion Potential Measurement in High-Temperature Water , 2003 .

[19]  E. Han,et al.  Microstructural characteristics of the oxide scale formed on 304 stainless steel in oxygenated high temperature water , 2010 .

[20]  J. Robertson The mechanism of high temperature aqueous corrosion of steel , 1989 .

[21]  B. Beverskog,et al.  Revised pourbaix diagrams for iron at 25–300 °C , 1996 .

[22]  Takahiro Miyazawa,et al.  Effects of Hydrogen Peroxide on Corrosion of Stainless Steel, (V) Characterization of Oxide Film with Multilateral Surface Analyses , 2006 .

[23]  Young-Jin Kim Analysis of Oxide Film Formed on Type 304 Stainless Steel in 288°C Water Containing Oxygen, Hydrogen, and Hydrogen Peroxide , 1999 .

[24]  T. Devine,et al.  Influence of Oxygen Concentration of 288°C Water and Alloy Composition on the Films Formed on Fe-Ni-Cr Alloys , 2007 .

[25]  M. Hanson,et al.  Zinc treatment effects on corrosion behavior of 304 stainless steel in high temperature, hydrogenated water , 2001 .

[26]  E. Han,et al.  The mechanism of oxide film formation on Alloy 690 in oxygenated high temperature water , 2011 .

[27]  R. Davidson,et al.  The mechanism and kinetics of corrosion product release from stainless steel in lithiated high temperature water , 1987 .

[28]  E. Han,et al.  Effect of alternately changing the dissolved Ni ion concentration on the oxidation of 304 stainless steel in oxygenated high temperature water , 2011 .

[29]  B. Stellwag The mechanism of oxide film formation on austenitic stainless steels in high temperature water , 1998 .

[30]  M. Walls,et al.  Influence of pH on Properties of Oxide Films Formed on Type 316L Stainless Steel, Alloy 600, and Alloy 690 in High-Temperature Aqueous Environments , 2003 .

[31]  Z. Xia,et al.  The composition and properties of oxide films on type 304 stainless steel on exposure to lithiated water at 100–350°C , 1991 .

[32]  P. Andresen,et al.  Effect of Zinc Additions on Oxide Rupture Strain and Repassivation Kinetics of Iron-Based Alloys in 288°C Water , 1996 .