X-ray microtomography of materials

AbstractX-ray microtomography allows imaging of the interior microstructure of materials non- destructively and with spatial resolution which can approach that of optical microscopy (typically, no better than 1 μm in samples whose cross-sectional diameter is on the order of 1 mm, and 10 &µm for 10 mm specimens). First, X-ray microtomography's origin in medical imaging and the physics behind computed tomography are reviewed. Summaries of apparatus, radiation sources, data collection schemes, and of materials applications follow. To date, most materials applications fall into one of four areas: inorganic matrix composites, transport in porous media, calcified tissue, and fatigue crack closure. Details of studies in each area highlight the advantages X-ray microtomography brings, and the final section focuses on future directions suggested by recent work using imaging modalities other than X-ray attenuation.

[1]  H. Graafsma,et al.  Applications of high-energy synchrotron radiation for structural studies of polycrystalline materials. , 1997, Journal of synchrotron radiation.

[2]  S. Dover,et al.  X‐ray microscopy using computerized axial tomography , 1985, Journal of microscopy.

[3]  Steve Webb From the Watching of Shadows: The Origins of Radiological Tomography , 1990 .

[4]  R E Guldberg,et al.  Mechanical Stimulation of Tissue Repair in the Hydraulic Bone Chamber , 1997, Journal of bone and mineral research : the official journal of the American Society for Bone and Mineral Research.

[5]  D. McDowell,et al.  Fracture mechanics : twenty-second symposium , 1992 .

[6]  Nicos Martys,et al.  Transport in sandstone: A study based on three dimensional microtomography , 1996 .

[7]  L. Grodzins,et al.  Critical absorption tomography of small samples: Proposed applications of synchrotron radiation to computerized tomography II , 1983 .

[8]  M. C. Nichols,et al.  X-Ray Tomographic Microscopy (XTM) Using Synchrotron Radiation , 1992 .

[9]  Katsuhisa Usami,et al.  Improvement of Spatial Resolution of Monochromatic X-ray CT Using Synchrotron Radiation , 1988 .

[10]  T. Starr Advances in Modeling of the Chemical Vapor Infiltration Process , 1991 .

[11]  J. Kinney,et al.  The topology of percolating porosity in woven fiber ceramic matrix composites , 1994 .

[12]  A. Cormack Representation of a Function by Its Line Integrals, with Some Radiological Applications , 1963 .

[13]  Rosenfeld Damage Tolerance in Aircraft Structures , 1971 .

[14]  W. D. Friedman,et al.  Review of dual-energy computed tomography techniques , 1990 .

[15]  B. Cullity,et al.  Elements of X-ray diffraction , 1957 .

[16]  Sangbeom Lee Nondestructive examination of chemical vapor infiltration of 0°/90° SiC/Nicalon composites , 1993 .

[17]  T Sato,et al.  X-ray tomography for microstructural objects. , 1981, Applied optics.

[18]  S. Goldstein,et al.  The direct examination of three‐dimensional bone architecture in vitro by computed tomography , 1989, Journal of bone and mineral research : the official journal of the American Society for Bone and Mineral Research.

[19]  H. D. Zeman,et al.  COMPUTED TOMOGRAPHY USING SYNCHROTRON RADIATION , 1984 .

[20]  D D Peters,et al.  Microcomputed tomography: an advanced system for detailed endodontic research. , 1995, Journal of endodontics.

[21]  L. Grodzins,et al.  Optimum energies for x-ray transmission tomography of small samples. Applications of synchrotron radiation to computerized tomography I , 1983 .

[22]  U. Bonse,et al.  Optimization of CCD-based energy-modulated x-ray microtomography , 1989 .

[23]  S. Stock,et al.  Micro-, Meso- and Macro-Texture and Fatigue Crack Roughness in Al-Li 2090 T8E41 , 1998 .

[24]  Stuart R. Stock,et al.  Nondestructive investigation of damage in composites using x-ray tomographic microscopy (XTM) , 1990 .

[25]  Jin Kogure,et al.  Computed tomography for measuring the annual rings of a live tree , 1984 .

[26]  S. Nutt,et al.  Silicon carbide filaments: Microstructure , 1985 .

[27]  T. Breunig Nondestructive evaluation of damage in SiC/Al metal matrix composite using x-ray tomographic microscopy , 1994 .

[28]  D. McDowell,et al.  X-ray microbeam quantification of grain subdivision accompanying large deformations of copper , 1998 .

[29]  D. H. Phillips,et al.  X-ray computed tomography for the testing and evaluation of ceramic processes , 1993 .

[30]  William N. Sharpe Micromechanics : experimental techniques : presented at the Winter Annual Meeting of the American Society of Mechanical Engineers, San Francisco, California, December 10-15, 1989 , 1989 .

[31]  S. Suresh,et al.  Oxide-Induced Crack Closure: An Explanation for Near-Threshold Corrosion Fatigue Crack Growth Behavior , 1981 .

[32]  X-ray computed tomography with 50-μm resolution , 1985 .

[33]  Stuart R. Stock,et al.  Damage in aligned-fibre SiC/Al quantified using a laboratory X-ray tomographic microscope , 1993 .

[34]  Nicos Martys,et al.  Transport and diffusion in three-dimensional composite media , 1994 .

[35]  S. Goldstein,et al.  Predictive value of proximal femoral bone densitometry in determining local orthogonal material properties. , 1996, Journal of Biomechanics.

[36]  W. C. Röntgen,et al.  Ueber eine neue Art von Strahlen , 1898 .

[37]  J. Jones,et al.  On the variation of fatigue-crack-opening load with measurement location , 1979 .

[38]  J. Kinney,et al.  Evidence of critical scaling behavior during vapor phase synthesis of continuous filament composites , 1997 .

[39]  J. C. Elliott,et al.  X‐ray microtomography , 1982, Journal of microscopy.

[40]  S. Goldstein,et al.  Evaluation of a microcomputed tomography system to study trabecular bone structure , 1990, Journal of orthopaedic research : official publication of the Orthopaedic Research Society.

[41]  W. V. Enckevort,et al.  Photoluminescence tomography as a method to image point-defect distributions in crystals: Nitrogen-vacancy pairs in synthetic diamonds , 1988 .

[42]  J. A. Grant,et al.  Monochromatic microtomographic imaging of osteoporotic bone. , 1997, Physics in medicine and biology.

[43]  B. Lerch,et al.  As-received microstructure of a SiC/Ti-15-3 composite , 1988 .

[44]  J. N. Otis,et al.  Evaluation of synchrotron X-rays for transvenous coronary angiography , 1984 .

[45]  T. Hirano,et al.  In situ x-ray CT under tensile loading using synchrotron radiation , 1995 .

[46]  J. C. Elliott,et al.  X-ray microtomography: nondestructive three-dimensional imaging for in vitro endodontic studies. , 1997, Oral surgery, oral medicine, oral pathology, oral radiology, and endodontics.

[47]  Keith W. Jones,et al.  X‐ray microtomography studies of nascent polyolefin particles polymerized over magnesium chloride‐supported catalysts , 1993 .

[48]  F. Wong,et al.  X-ray microtomography of bones and teeth. , 1996, Physiological measurement.

[49]  Keith W. Jones,et al.  Synchrotron computed microtomography of porous media: Topology and transports. , 1994, Physical review letters.

[50]  L. Cooley,et al.  Fatigue-crack growth in 2090 AlLi alloy , 1989 .

[51]  M. C. Nichols,et al.  X-ray Tomographic Study of Chemical Vapor Infiltration Processing of Ceramic Composites , 1993, Science.

[52]  S A Goldstein,et al.  The relationship between the structural and orthogonal compressive properties of trabecular bone. , 1994, Journal of biomechanics.

[53]  Brian P. Flannery,et al.  Observational strategies for three‐dimensional synchrotron microtomography , 1987 .

[54]  F. Wong,et al.  Application of scanning microradiography and x-ray microtomography to studies of bones and teeth. , 1994, Journal of X-ray science and technology.

[55]  H. Gundersen,et al.  Quantification of connectivity in cancellous bone, with special emphasis on 3-D reconstructions. , 1993, Bone.

[56]  B. Derby,et al.  X‐ray microtomographic studies of metal matrix composites using laboratory X‐ray sources , 1995 .

[57]  A. Guvenilir Investigation into asperity induced closure in an Al-Li alloy using x-ray tomography , 1995 .

[58]  F. H. Séguin,et al.  The largest and smallest X-ray computed tomography systems , 1984 .

[59]  David L. McDowell,et al.  Mixed-mode crack behavior , 1999 .

[60]  Ulrich Bonse,et al.  X-ray computed microtomography (μCT) using synchrotron radiation (SR) , 1996 .

[61]  S. Stock,et al.  Characterization of Conductive Anodic Filament (Caf) by X-Ray Microtomography and by Serial Sectioning , 1993 .

[62]  S A Goldstein,et al.  Morphometric and anisotropic symmetries of the canine distal femur , 1990, Journal of orthopaedic research : official publication of the Orthopaedic Research Society.

[63]  Geoffrey H. Campbell,et al.  X-ray tomographic microscopy investigation of the ductile rupture of an aluminum foil bonded between sapphire blocks , 1995 .

[64]  John H. Kinney,et al.  Elastic constants of cellular structures , 1997 .

[65]  J. Kinney,et al.  Pore geometry in woven fiber structures: 0°/90° plain-weave cloth layup preform , 1998 .

[66]  J. C. Elliott,et al.  Three dimensional mineral distribution in the enamel of a rat incisor measured by x-ray microtomography , 1995 .

[67]  M. D. Butts Nondestructive examination of nicalon fiber composite preforms using x-ray tomographic microscopy , 1993 .

[68]  U. Bonse,et al.  X-ray tomographic microscopy of fibre-reinforced materials , 1991 .

[69]  F Busch,et al.  X-ray microtomography (microCT) using phase contrast for the investigation of organic matter. , 1997, Journal of computer assisted tomography.

[70]  M. Hahn,et al.  High Spatial Resolution Imaging of Bone Mineral Using Computed Microtomography: Comparison with Microradiography and Undecalcified Histologic Sections , 1993, Investigative radiology.

[71]  S. Dover,et al.  Three-dimensional distribution of mineral in bone at a resolution of 15 micron determined by x-ray microtomography. , 1984, Metabolic bone disease & related research.

[72]  J. Kinney,et al.  In vivo, three‐dimensional microscopy of trabecular bone , 1995, Journal of bone and mineral research : the official journal of the American Society for Bone and Mineral Research.

[73]  P. Spanne,et al.  In vivo animal models of body composition in aging. , 1993, The Journal of nutrition.

[74]  S. Stock,et al.  High resolution synchrotron x-ray diffraction tomography of polycrystalline samples , 1995 .