Influence of heat treatment on the microstructure and tensile properties of Ni-base superalloy Haynes 282

The effect of heat treatment on the microstructure and mechanical properties of Ni-base superalloy Haynes 282 was investigated. Applying a standard two-step ageing (1010 °C/2 h +788 °C/8 h) to the as-received, mill annealed, material resulted in a the presence of discrete grain boundary carbides and finely dispersed intragranular γ′, with an average size of 43 nm. This condition showed excellent room temperature strength and ductility. The introduction of an additional solution treatment at 1120 °C resulted in grain growth, interconnected grain boundary carbides and coarse (100 nm) intragranular γ′. The coarser γ′ led to a significant reduction in the strength level, and the interconnected carbides resulted in quasi-brittle fracture with a 50% reduction in ductility. Reducing the temperature of the stabilization step to 996 °C during ageing of the mill annealed material produced a bi-modal γ′ distribution, and grain boundaries decorated by discrete carbides accompanied by γ′. This condition showed very similar strength and ductility levels as the standard ageing of mill-annealed material. This is promising since both grain boundary γ′ and a bi-modal intragranular γ′ distribution can be used to tailor the mechanical properties to suit specific applications. The yield strength of all three conditions could be accurately predicted by a unified precipitation strengthening model.

[1]  G. Mccarthy,et al.  Low temperature carbide precipitation in a nickel base superalloy , 1985 .

[2]  A. Deruyttere,et al.  Multi-component solid solution hardening , 1977 .

[3]  M. Mills,et al.  Measurements of antiphase boundary and complex stacking fault energies in binary and B-doped Ni3Al using TEM , 1993 .

[4]  T. Gabb,et al.  Effect of Microstructure on Time Dependent Fatigue Crack Growth Behavior In a P/M Turbine Disk Alloy , 2008 .

[5]  G. G. Stokes "J." , 1890, The New Yale Book of Quotations.

[6]  E. G. Richards,et al.  Factors Influencing the Stability of Nickel-Base High-Temperature Alloys , 1968 .

[7]  C. Rae,et al.  On the prediction of the yield stress of unimodal and multimodal γ′ Nickel-base superalloys , 2015 .

[8]  P. Flewitt,et al.  The influence of temperature and grain boundary volume on the resistivity of nanocrystalline nickel , 2015 .

[9]  R. Mirshams,et al.  Influence of various heat treatments on the microstructure of polycrystalline IN738LC , 1997 .

[10]  Tomoo Suzuki,et al.  Solid Solution Hardening of Nickel —Role of Transition Metal and B-subgroup Solutes— , 1986 .

[11]  J. Embury,et al.  The influence of precipitation on the work-hardening behavior of the aluminum alloys AA6111 and AA7030 , 2003 .

[12]  W. C. Johnson,et al.  Influence of coherency stress on microstructural evolution in model Ni-Al-Mo alloys , 1995 .

[13]  R. Reed,et al.  Heat treatment of UDIMET 720Li: the effect of microstructure on properties , 1999 .

[14]  L. M. Pike DEVELOPMENT OF A FABRICABLE GAMMA-PRIME (γ') STRENGTHENED SUPERALLOY , 2008 .

[15]  E. Nembach,et al.  The critical resolved shear stress of γ′-strengthened nickel-based superalloys with γ′-volume fractions between 0.07 and 0.47 , 1992 .

[16]  E. Nembach,et al.  The antiphase boundary energy of γ precipitates in nickel-based superalloys , 1992 .

[17]  Anders Wretland,et al.  The effect of grain size and hardness of Waspaloy on the wear of cemented carbide tools , 2010 .

[18]  H. Karnthaler,et al.  The influence of the fault energies on the anomalous mechanical behaviour of Ni3Al alloys , 1996 .

[19]  R. Doherty Role of interfaces in kinetics of internal shape changes , 1982 .

[20]  S. Hwang,et al.  M23C6 precipitation behavior and grain boundary serration in Ni-based Alloy 690 , 2014 .

[21]  R. Hu,et al.  Correlation between grain boundary misorientation and M23C6 precipitation behaviors in a wrought Ni-based superalloy , 2013 .

[22]  M. Vittori,et al.  On the antiphase boundary energy of Ni3(Al, Ti) particles , 1985 .

[23]  Anders Wretland,et al.  The effect of grain size and hardness of wrought Alloy 718 on the wear of cemented carbide tools , 2010 .

[24]  P. Veyssiére,et al.  On the presence of super lattice intrinsic stacking faults in plastically deformed Ni3Al , 1985 .

[25]  Tresa M. Pollock,et al.  Strengthening Mechanisms in Polycrystalline Multimodal Nickel-Base Superalloys , 2009 .

[26]  A. Picasso,et al.  Work-hardening in Inconel X-750: study of stage II , 1998 .

[27]  G. K. Dey,et al.  Role of dislocation density in raising the stage II work-hardening rate of Alloy 625 , 2009 .

[28]  R. Reed The Superalloys: Fundamentals and Applications , 2006 .

[29]  G. Sastry,et al.  Work-Hardening Behavior of the Ni-Fe Based Superalloy IN718 , 2008 .

[30]  D. Dimiduk,et al.  The compositional dependence of antiphase-boundary energies and the mechanism of anomalous flow in Ni3 Al alloys , 1993 .

[31]  David Kinderlehrer,et al.  Morphological Stability of a Particle Growing by Diffusion or Heat Flow , 1999 .

[32]  Michael D. Uchic,et al.  Size-affected single-slip behavior of pure nickel microcrystals , 2005 .

[33]  Roderick I. L. Guthrie,et al.  Study of microstructure and mechanical properties of high performance Ni-base superalloy GTD-111 , 2002 .

[34]  H. Collins RELATIVE STABILITY OF CARBIDE AND INTERMETALLIC PHASES IN NICKEL-BASE SUPERALLOYS , 1968 .

[35]  H. White,et al.  Weldability of HAYNES 282 alloy for new fabrications and after service exposure , 2009 .

[36]  H. Karnthaler,et al.  Three alternative experimental methods to determine the antiphase-boundary energies of the γ′ precipitates in superalloys , 2002 .

[37]  Miyoung Kim,et al.  The effect of grain boundary serration on creep resistance in a wrought nickel-based superalloy , 2009 .

[38]  E. Nembach,et al.  The effect of grain size on the yield strength of the γ′-hardened superalloy NIMONIC PE16 , 1989 .

[39]  E. Kozeschnik,et al.  Yield strength prediction in Ni-base alloy 718Plus based on thermo-kinetic precipitation simulation , 2014 .

[40]  D. Locq,et al.  On the Role of Tertiary γ' Precipitates in the Creep Behaviour at 700C of a PM Disk Superalloy , 2004 .

[41]  R. C. Ecob,et al.  The growth of γ′ precipitates in nickel-base superalloys , 1983 .

[42]  R. Stickler,et al.  Microstructure of Nickel-Based Superalloys , 1969 .

[43]  T. Kruml,et al.  Temperature dependence of dislocation microstructure in Ni3(Al,Hf) , 1997 .