Ferroelectric polymorph of lead metaniobate (PbNb2O6) exhibits an orthorhombic structure, which is metastable at room temperature and can only be obtainable by quenching from high temperatures (∼1200 °C). In this letter, we report a ferroelectric PbNb2O6 thin film doped with SrTiO3 (Pb0.95Sr0.05(Nb2)0.98Ti0.05O6) with orthorhombic structure on Pt/Ti/Si substrate, which was prepared via a sol-gel route. The orthorhombic structure was developed at 900 °C at a normal heating rate of 5 °C/min and cooling rate of 10 °C/min. The PbNb2O6 film exhibited a remanent polarization (Pr) of 12.3 μC/cm2 and a coercive field (Ec) of 39 kV/cm, respectively, when measured at an applied field of 143 kV/cm. The leakage current density was 1.02×10−5 A/cm2 at 100 kV/cm. The room-temperature dielectric constant and dissipation factor was stable (∼325 and ∼1.5%, respectively) over a frequency range of 1 kHz to 1 MHz.
[1]
H. Lee,et al.
Effects of Microstructure on the Dielectric and Piezoelectric Properties of Lead Metaniobate
,
1998
.
[2]
M. Sayer,et al.
Ferroelectric lead niobate films by pulsed thermal processing
,
1992
.
[3]
E. Subbarao,et al.
Solid Solutions Based on Ferroelectric PbNb2,O6
,
1962
.
[4]
M. Francombe.
Polymorphism in lead metaniobate
,
1956
.
[5]
G. Goodman.
Ferroelectric Properties of Lead Metaniobate
,
1953
.
[6]
A. Tsuzuki,et al.
Preparation and properties of rapidly quenched films in the PbONb2O5 system
,
1989
.