Mechanics of single pass equal channel angular extrusion of powder in tubes

In the current study powder in tubes (PITs) are processed through single pass equal channel angular extrusion (ECAE), for two different powders by using three different tube materials. Studies were conducted for the first time to understand the processing mechanism of ECAE of PITs. In the case of hard brittle intermetallic magnesium boride (MgB2) powder, the process was found to primarily involve compaction and shear-sliding of the powder, and localized-deformation of the tube. Reasons for localized-deformation occurring during ECAE were discussed in detail. Compaction efficiency was understood to depend not only on the material of the tube but also on the homogeneity of stress and strain in the composite PIT. Various frictional stresses and mechanisms of localized-deformation were found to be the reasons for stress-strain inhomogeneity. In the case of copper powder, even though localized-deformation occurred, higher inter-particle friction and low yield strength of the powder helped in the complete densification of the powders.

[1]  Terence G. Langdon,et al.  The process of grain refinement in equal-channel angular pressing , 1998 .

[2]  Daniel B. Miracle,et al.  Compaction of amorphous aluminum alloy powder by direct extrusion and equal channel angular extrusion , 2005 .

[3]  H. Matsuzawa,et al.  Shock wave consolidated MgB2 bulk samples , 2004 .

[4]  A. V. Nagasekhar,et al.  Optimal tool angles for equal channel angular extrusion of strain hardening materials by finite element analysis , 2004 .

[5]  Terence G. Langdon,et al.  An investigation of microstructural evolution during equal-channel angular pressing , 1997 .

[6]  A. Sulpice,et al.  Effect of sintering temperature on properties of MgB2 wire sheathed by low carbon steel tube , 2005 .

[7]  V. Segal Materials processing by simple shear , 1995 .

[8]  S. L. Semiatin,et al.  The effect of material properties and tooling design on deformation and fracture during equal channel angular extrusion , 2000 .

[9]  P. Prangnell,et al.  The effect of strain path on the development of deformation structures in severely deformed aluminium alloys processed by ECAE , 2000 .

[10]  R. Valiev,et al.  Bulk nanostructured materials from severe plastic deformation , 2000 .

[11]  K. Hartwig,et al.  FORMATION/CONSOLIDATION OF WC-Co CERMETS BY SIMPLE SHEAR , 2000 .

[12]  K. Cooper The state of fundamental applied research in amorphous metals , 2002 .

[13]  Ibrahim Karaman,et al.  Microstructure evolution and mechanical behavior of bulk copper obtained by consolidation of micro- and nanopowders using equal-channel angular extrusion , 2004 .

[14]  Ian Baker,et al.  An experimental study of equal channel angular extrusion , 1997 .

[15]  I. Karaman,et al.  The effect of temperature and extrusion speed on the consolidation of zirconium-based metallic glass powder using equal-channel angular extrusion , 2004 .

[16]  S. Semiatin,et al.  Hot working of Ti-6Al-4V via equal channel angular extrusion , 1999 .

[17]  J. Kusui,et al.  Microstructural characteristics and superplastic-like behavior in aluminum powder alloy consolidated by equal-channel angular pressing , 2000 .

[18]  K. Xia,et al.  Back pressure equal channel angular consolidation of pure Al particles , 2005 .

[19]  V. Segal Equal channel angular extrusion: from macromechanics to structure formation , 1999 .

[20]  Yuri Estrin,et al.  Producing bulk ultrafine-grained materials by severe plastic deformation , 2006 .

[21]  V. Segal,et al.  Slip line solutions, deformation mode and loading history during equal channel angular extrusion , 2003 .

[22]  I. Karaman,et al.  Consolidation of amorphous copper based powder by equal channel angular extrusion , 2003 .

[23]  D. Miracle,et al.  Equal channel angular extrusion compaction of semi-amorphous Al85Ni10Y2.5La2.5 alloy powder , 2004 .

[24]  S. Dou,et al.  Influence of Ag, Cu and Fe sheaths on MgB2 superconducting tapes , 2002 .

[25]  R. Goforth,et al.  Workability of commercial-purity titanium and 4340 steel during equal channel angular extrusion at cold-working temperatures , 1999 .

[26]  Sun Ig Hong,et al.  On the die corner gap formation in equal channel angular pressing , 2000 .

[27]  P. Venugopal,et al.  Candidature of equal channel angular pressing for processing of tubular commercial purity-titanium , 2006 .