Correction of image drift and distortion in a scanning electron microscopy

Continuous research on small‐scale mechanical structures and systems has attracted strong demand for ultrafine deformation and strain measurements. Conventional optical microscope cannot meet such requirements owing to its lower spatial resolution. Therefore, high‐resolution scanning electron microscope has become the preferred system for high spatial resolution imaging and measurements. However, scanning electron microscope usually is contaminated by distortion and drift aberrations which cause serious errors to precise imaging and measurements of tiny structures. This paper develops a new method to correct drift and distortion aberrations of scanning electron microscope images, and evaluates the effect of correction by comparing corrected images with scanning electron microscope image of a standard sample. The drift correction is based on the interpolation scheme, where a series of images are captured at one location of the sample and perform image correlation between the first image and the consequent images to interpolate the drift–time relationship of scanning electron microscope images. The distortion correction employs the axial symmetry model of charged particle imaging theory to two images sharing with the same location of one object under different imaging fields of view. The difference apart from rigid displacement between the mentioned two images will give distortion parameters. Three‐order precision is considered in the model and experiment shows that one pixel maximum correction is obtained for the employed high‐resolution electron microscopic system.

[1]  Uwe Glatzel,et al.  Measurement of the lattice misfit in the single crystal nickel based superalloys CMSX-4, SRR99 and SC16 by convergent beam electron diffraction , 1998 .

[2]  C. G. Frase,et al.  Model-Based Correction of Image Distortion in Scanning Electron Microscopy , 2010 .

[4]  L. Kourkoutis,et al.  Electron Microscopy of Biological Materials at the Nanometer Scale , 2012 .

[5]  K. A. Padmanabhan,et al.  Strain mapping in a deformation-twinned nanocrystalline Pd grain , 2010 .

[6]  Xide Li,et al.  Full field and microregion deformation measurement of thin films using electronic speckle pattern interferometry and array microindentation marker method , 2005 .

[7]  M. Graef,et al.  A method for measuring microstructural-scale strains using a scanning electron microscope: Applications to γ-titanium aluminides , 2003 .

[8]  Anand Asundi,et al.  Two-dimensional digital image correlation for in-plane displacement and strain measurement: a review , 2009 .

[10]  Jean-Marie Tarascon,et al.  In situ SEM study of the interfaces in plastic lithium cells , 1999 .

[11]  Sounkalo Dembélé,et al.  Fast image drift compensation in scanning electron microscope using image registration , 2013, 2013 IEEE International Conference on Automation Science and Engineering (CASE).

[12]  E. Sudarshan,et al.  Quantum theory of magnetic electron lenses based on the Dirac equation. , 1989 .

[13]  J. Barnes,et al.  Strain measurement at the nanoscale: Comparison between convergent beam electron diffraction, nano-beam electron diffraction, high resolution imaging and dark field electron holography. , 2013, Ultramicroscopy.

[14]  R. Shimizu,et al.  Third-order spherical aberration correction using multistage self-aligned quadrupole correction-lens systems. , 2010, Journal of electron microscopy.

[15]  J. Gerber,et al.  Evidence for electron orbital dependence of ion-beam induced attenuations of transient magnetic fields , 1991 .

[16]  Lijun Xu,et al.  Geometric distortion correction for sinusoidally scanned images , 2011 .

[17]  Martin P. Seah,et al.  Simplified drift characterization in scanning probe microscopes using a simple two-point method , 2009 .

[18]  K. C. A. Smith,et al.  An automatic focusing and astigmatism correction system for the SEM and CTEM , 1982 .

[19]  Jean-Marie Tarascon,et al.  In situ Scanning Electron Microscopy (SEM) observation of interfaces within plastic lithium batteries , 1998 .

[20]  M. Sutton,et al.  Scanning Electron Microscopy for Quantitative Small and Large Deformation Measurements Part II: Experimental Validation for Magnifications from 200 to 10,000 , 2007 .

[21]  C. Auth,et al.  45nm High-k + metal gate strain-enhanced transistors , 2008, 2008 Symposium on VLSI Technology.

[22]  T. Everhart,et al.  Wide-band detector for micro-microampere low-energy electron currents , 1960 .

[23]  Michael A. Sutton,et al.  Scanning Electron Microscopy for Quantitative Small and Large Deformation Measurements Part I: SEM Imaging at Magnifications from 200 to 10,000 , 2007 .

[24]  David Casasent,et al.  Geometric correction of SEM images , 2000, SPIE Defense + Commercial Sensing.

[25]  Masayuki Abe,et al.  Drift-compensated data acquisition performed at room temperature with frequency modulation atomic force microscopy , 2007 .

[27]  T R Bürglin A two‐channel four‐dimensional image recording and viewing system with automatic drift correction , 2000, Journal of microscopy.

[28]  Stéphane Roux,et al.  Characterization of SEM speckle pattern marking and imaging distortion by digital image correlation , 2013 .

[29]  J. Orteu,et al.  Quantitative Stereovision in a Scanning Electron Microscope , 2011 .

[30]  E. Zschech,et al.  In situ SEM observation of electromigration phenomena in fully embedded copper interconnect structures , 2002 .

[31]  F. Sachs,et al.  Drift-free atomic force microscopy measurements of cell height and mechanical properties. , 2007, The Review of scientific instruments.