PEPT measurements of solid–liquid flow field and spatial phase distribution in concentrated monodisperse stirred suspensions

The technique of positron emission particle tracking (PEPT) has been used to determine the two-phase flow field and spatial phase distribution in a stirred vessel containing coarse glass particles suspended in water. The Lagrangian flow data provided by PEPT have been converted to give a detailed Eulerian description of the two-phase flow generated by a pitched blade turbine (PBT) operating in up-pumping or down-pumping mode. For the first time, it has been possible to determine the full 3D velocity and concentration fields of both the liquid and the solid phase within an opaque dense slurry of this type containing up to 40 wt% solids. The detailed PEPT measurements have also enabled the solids mass balance and the mass continuity of the two phases to be accurately verified throughout the vessel. The data show that the pumping effectiveness of the PBT is unaffected at moderate solid fractions, but is considerably reduced at high fractions and even more so in the up-pumping mode. A uniformity index based on the variance of the local solids concentration in the vessel shows that, overall, a down-pumping PBT achieves a significantly better homogeneity than an up-pumping PBT.

[1]  A. Cipollina,et al.  Dense solid–liquid off-bottom suspension dynamics: Simulation and experiment , 2009 .

[2]  Milorad P. Dudukovic,et al.  Flow field of suspended solids in a stirred tank reactor by Lagrangian tracking , 2007 .

[3]  Xianfeng Fan,et al.  Labelling a single particle for positron emission particle tracking using direct activation and ion-exchange techniques , 2006 .

[4]  Laurent Falk,et al.  Characterization of stirred vessel hydrodynamics by three dimensional trajectography , 1998 .

[5]  Th.N. Zwietering Suspending of solid particles in liquid by agitators , 1958 .

[6]  P. Ayazi Shamlou,et al.  Processing of Solid–Liquid Suspensions , 1993 .

[7]  David Parker,et al.  A Langrangian Study of Solids Suspension in a Stirred Vessel by Positron Emission Particle Tracking (PEPT) , 2002 .

[8]  A. Barresi,et al.  Solid dispersion in an agitated vessel , 1987 .

[9]  M. R. Hawkesworth,et al.  Positron emission particle tracking - a technique for studying flow within engineering equipment , 1993 .

[10]  Chiara Galletti,et al.  An Impedance Probe for the Measurements of Flow Characteristics and Mixing Properties in Stirred Slurry Reactors , 2004 .

[11]  Alvin W. Nienow,et al.  Positron emission particle tracking (PEPT) compared to particle image velocimetry (PIV) for studying the flow generated by a pitched-blade turbine in single phase and multi-phase systems , 2009 .

[12]  R. Mann,et al.  Development of a networks-of-zones fluid mixing model for an unbaffled stirred vessel used for precipitation , 2006 .

[13]  David Parker,et al.  Enhancing 18F uptake in a single particle for positron emission particle tracking through modification of solid surface chemistry , 2006 .

[14]  David Parker,et al.  Positron emission particle tracking in a mechanically agitated solid–liquid suspension of coarse particles , 2009 .

[15]  M. Barigou Particle Tracking in Opaque Mixing Systems: An Overview of the Capabilities of PET and PEPT , 2004 .

[16]  P. Fowles,et al.  Positron emission particle tracking using the new Birmingham positron camera , 2002 .

[17]  Z. Nagy,et al.  Application of fluorescent PIV and digital image analysis to measure turbulence properties of solid–liquid stirred suspensions , 2009 .