Recent developments in two fundamental aspects of electron backscatter diffraction

Two very different aspects of electron backscatter diffraction (EBSD) are considered in this paper. Firstly, the use of the technique for the measurement of grain size is discussed with particular reference to the development of international standards to help ensure reproducible and repeatable measurements. In particular the lessons learnt for both calibration of the complete SEM-EBSD system and in choice of the correct data acquisition and processing parameters from an international round robin are summarized. Secondly, extending the capability of EBSD through development of new detectors is discussed. New shadow casting methods provide a means to achieve better accuracy in definition of sample-pattern geometry, while increased detail can be obtained by larger cameras and ultimately direct electron detection.

[1]  C. Davidson,et al.  Grain Size Measurements in Mg-Al High Pressure Die Castings Using Electron Back-Scattered Diffraction (EBSD) , 2004 .

[2]  K. Mingard,et al.  Towards high accuracy calibration of electron backscatter diffraction systems. , 2011, Ultramicroscopy.

[3]  T. Quested,et al.  A comparison of grain imaging and measurement using horizontal orientation and colour orientation contrast imaging, electron backscatter pattern and optical methods , 1999, Journal of microscopy.

[4]  N. Gao,et al.  A comparison of grain size determination by light microscopy and EBSD analysis , 2005 .

[5]  J. Abrahams,et al.  Low energy electron microscopy imaging using Medipix2 detector , 2011 .

[6]  J. N. Chapman,et al.  A CCD-based image recording system for the CTEM , 1982 .

[7]  A. Bell,et al.  Electron backscatter diffraction as a domain analysis technique in BiFeO3-PbTiO3 single crystals , 2008, IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control.

[8]  M. Vaudin,et al.  Report on VAMAS round robin of ISO 13067 :: microbeam analysis - electron backscatter diffraction - measurement of average grain size , 2011 .

[9]  A. Kirkland,et al.  Direct detection of electron backscatter diffraction patterns. , 2013, Physical review letters.

[10]  A. Wilkinson,et al.  Factors affecting the accuracy of high resolution electron backscatter diffraction when using simulated patterns. , 2010, Ultramicroscopy.

[11]  A. Wilkinson,et al.  High-resolution elastic strain measurement from electron backscatter diffraction patterns: new levels of sensitivity. , 2006, Ultramicroscopy.

[12]  P. Houtte,et al.  Textures of Materials ICOTOM 14 , 2005 .

[13]  J. Fundenberger,et al.  Using EBSD and TEM‐Kikuchi patterns to study local crystallography at the domain boundaries of lead zirconate titanate , 2008, Journal of microscopy.

[14]  Carol Trager-Cowan,et al.  Many-beam dynamical simulation of electron backscatter diffraction patterns. , 2007, Ultramicroscopy.

[15]  R Barkman,et al.  ASTM. 1999. Standard practice for conducting an interlaboratory study to determine the precision of a test method. ASTM E691-92. In: Annual Book of ASTM Standards. Philadelphia, PA:American Society for Testing and Materials. , 2006 .

[16]  Stuart I. Wright,et al.  A Parametric Study of Electron Backscatter Diffraction based Grain Size Measurements , 2010 .

[17]  R. Fortunier,et al.  Accuracy assessment of elastic strain measurement by EBSD , 2009, Journal of microscopy.

[18]  F. J. Humphreys Quantitative metallography by electron backscattered diffraction , 1999, Journal of microscopy.