Operation planning in the rectification of essential oils

Abstract This paper proposes a methodology that uses a recently developed shortcut model to represent each individual separation task, for planning the operation of a batch distillation column. For a given column and recycle policy, optimization of the recoveries of two key components at each separation renders the set of optimal reflux ratios and advances in each separation. The methodology is specially expedite for systems with a large number of components and whose performance can be upgraded by recycling intermediate cuts, as is the case in the rectification of essential oils. We illustrate the methodology by planning the rectification of crude orange oil to produce an oil essence depleted from light terpenes, which are responsible for rancidity of oils.

[1]  I. Grossmann,et al.  Global optimization of bilinear process networks with multicomponent flows , 1995 .

[2]  Omar Chiotti,et al.  SELECTION OF MULTICOMPONENT BATCH DISTILLATION SEQUENCES , 1993 .

[3]  R. Sargent,et al.  A general algorithm for short-term scheduling of batch operations */I , 1993 .

[4]  Jorge M. Montagna,et al.  A Simulation Approach to the Design and Operation of Multiproduct Batch Plants , 1997 .

[5]  Enrique Salomone,et al.  Shortcut Method for Multiple Task Batch Distillations , 1998 .

[6]  Omar Chiotti,et al.  SHORTCUT DESIGN PROCEDURE FOR BATCH DISTILLATION , 1997 .

[7]  Omar Chiotti,et al.  Short-Cut Design Procedure for Batch Distillations , 1997 .

[8]  James M. Douglas,et al.  Conceptual Design of Chemical Processes , 1988 .

[9]  Peng Wang,et al.  Compositional simulation of reservoir performance by a reduced thermodynamic model , 1994 .

[10]  Sandro Macchietto,et al.  An optimal recycle policy for multicomponent batch distillation , 1992 .

[11]  R. L. Geddes A general index of fractional distillation power for hydrocarbon mixtures , 1958 .

[12]  L. Biegler,et al.  Dynamic Optimization in the Design and Scheduling of Multiproduct Batch Plants , 1996 .

[13]  Iqbal M. Mujtaba,et al.  Optimal operation of multicomponent batch distillation—multiperiod formulation and solution , 1993 .

[14]  Jeffery S. Logsdon,et al.  On the simultaneous optimal design and operation of batch distillation columns , 1990 .

[15]  P. Floquet,et al.  Recycling of slop cuts in multicomponent batch distillation , 1994 .