Field-Cycling NMR Relaxometry

The main objective of field-cycling experiments [231, 367] is to obtain information on the spectral density of the fluctuating spin interactions in a frequency range as wide as possible.1 Typical examples are discussed in Chaps. 14 and 16 (see Figs. 12.1 and 14.2, for instance). The origin of the fluctuations is normally molecular dynamics so that these can be characterized in a direct and quantitative way.

[1]  J. Pope,et al.  A pulsed NMR study of nuclear spin-lattice relaxation in the off resonance rotating frame , 1974 .

[2]  S. Stapf,et al.  Nuclear spin-lattice relaxation and theories of polymer dynamics☆ , 1994 .

[3]  F. Grinberg,et al.  A new formalism for the evaluation of order-fluctuation modes in liquid crystals from field-cycling NMR-relaxometry data. , 1998, Journal of magnetic resonance.

[4]  K. Dušek,et al.  Thermotropic Mesophases in Element-Organic Polymers , 1989 .

[5]  A. Pines,et al.  High−Resolution Studies of Deuterium by Time−Domain Zero−Field NQR , 1986 .

[6]  R. Kimmich NMR: Tomography, Diffusometry, Relaxometry , 2001 .

[7]  R. Kimmich,et al.  Ultrasound-order director fluctuations interaction in nematic liquid crystals: A nuclear magnetic resonance relaxometry study , 2003 .

[8]  Surface fractals probed by adsorbate spin-lattice relaxation dispersion. , 1999, Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics.

[9]  R. Kimmich,et al.  Deuteron spectroscopy and deuteron field-cycling nuclear magnetic resonance relaxometry of the hydration water of lipid bilayers: The corrugated-sheet model for interface molecular dynamics in the ripple phase , 2000 .

[10]  R. Y. Dong Relaxation and the dynamics of molecules in the liquid crystalline phases , 2002 .

[11]  V. Pollak,et al.  Instrumentation for the Earth's Field NMR Technique , 1971 .

[12]  P. Bendel Spin-lattice relaxation by translational diffusion. Correlation times from off-resonance T1ϱ measurements in glycerol and camphene , 1981 .

[13]  F. M. Leslie,et al.  SOME CONSTITUTIVE EQUATIONS FOR ANISOTROPIC FLUIDS , 1966 .

[14]  John W. Goodby,et al.  Handbook of liquid crystals , 1998 .

[15]  R. Kimmich,et al.  Spin-lock field-cycling imaging relaxometry , 1995 .

[16]  F. Noack,et al.  Proton Spin Relaxation Dispersion for Some Nematic Homologues of the Liquid Crystal PAA , 1983 .

[17]  G. G. Stokes "J." , 1890, The New Yale Book of Quotations.

[18]  Nuclear quadrupole proton magnetic cross relaxation spectra analysis in a smectic A mesophase , 2000 .

[19]  S. Stapf,et al.  Influence of Cross-Link Density and Deformation on the NMR Relaxation Dispersion of Natural Rubber , 2002 .

[20]  S. H. Koenig,et al.  Nuclear magnetic relaxation dispersion in protein solutions. II. Transferrin. , 1969, The Journal of biological chemistry.

[21]  Seymour H. Koenig,et al.  Field-cycling relaxometry of protein solutions and tissue: Implications for MRI , 1990 .

[22]  E. Purcell,et al.  Relaxation Effects in Nuclear Magnetic Resonance Absorption , 1948 .

[23]  R. Kimmich,et al.  Optimisation of magnetic coils for NMR field-cycling experiments , 1985 .

[24]  R. Bryant,et al.  High-resolution magnetic relaxation dispersion measurements of solute spin probes using a dual-magnet system. , 1999, Journal of magnetic resonance.

[25]  G. Ferrante,et al.  Magnetic field compensation for field-cycling NMR Relaxometry in the ULF band , 2003 .

[26]  R. Kimmich,et al.  Solid-state NMR study of protein/polypeptide backbone fluctuations interpreted by multiple trapping diffusion of dilating defects , 1988 .

[27]  J. W. Doane,et al.  Field controlled light scattering from nematic microdroplets , 1986 .

[28]  C. A. Sholl,et al.  A relationship between nuclear spin relaxation in the laboratory and rotating frames for dipolar and quadrupolar relaxation , 1992 .

[29]  F Noack,et al.  Investigation of protein hydration by proton spin relaxation time measurements. , 1970, Biochimica et biophysica acta.

[30]  S. Stapf,et al.  NMR relaxation dispersion of vulcanized natural rubber. , 2004, Solid state nuclear magnetic resonance.

[31]  F. C. Frank,et al.  I. Liquid crystals. On the theory of liquid crystals , 1958 .

[32]  P A Rinck,et al.  The effect of aging and storage conditions on excised tissues as monitored by longitudinal relaxation dispersion profiles , 1989, Magnetic resonance in medicine.

[33]  A. G. Anderson,et al.  NUCLEAR SPIN-LATTICE RELAXATION IN METALS , 1959 .

[34]  H. Carr,et al.  The Principles of Nuclear Magnetism , 1961 .

[35]  S. Rast,et al.  Mechanisms of the Intermolecular Nuclear Magnetic Relaxation Dispersion of the (CH3)4N+ Protons in Gd3+ Heavy-Water Solutions. Interest for the Theory of Magnetic Resonance Imaging , 2001 .

[36]  M. Möller,et al.  Field-cycling NMR relaxometry of polymers confined to artificial tubes: verification of the exponent 3/4 in the spin–lattice relaxation dispersion predicted by the reptation model , 1999 .

[37]  J. Struppe,et al.  Angular and frequency dependent spin relaxation study of liquid crystalline cyanobiphenyls , 1996 .

[38]  G. Matson,et al.  Rotating frame spin-lattice relaxation in the presence of an off-resonance radiofrequency field. Scalar relaxation of31P in PBr3 , 1979 .

[39]  J. Freed,et al.  End-to-end correlation for a C-12 hydrocarbon chain. , 2003, Journal of magnetic resonance.

[40]  C. Slichter,et al.  Nuclear Relaxation in Superconducting Aluminum , 1957 .

[41]  R. Kimmich,et al.  Defect diffusion in crystalline lipid lamellae and nuclear magnetic relaxation behavior , 1975 .

[42]  D. Adams,et al.  Magnetic field dependence of 1/T1 of protons in tissue. , 1984, Investigative radiology.

[43]  Robin K. Harris,et al.  Encyclopedia of nuclear magnetic resonance , 1996 .

[44]  Ziherl,et al.  Nematic order director fluctuations and nuclear magnetic relaxation of a confined liquid crystal. , 1995, Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics.

[45]  D. Edmonds Nuclear quadrupole double resonance , 1977 .

[46]  J. W. Doane,et al.  Proton spin–lattice relaxation in nematic microdroplets , 1988 .

[47]  R. Kimmich,et al.  Field-cycling NMR relaxometry of water in synthetic saponites: Lévy walks on finite planar surfaces , 1999 .

[48]  S. Becker,et al.  Order fluctuations of the director in nematic thermotropic liquid crystals studied by nuclear magnetic resonance dipolar relaxation , 1998 .

[49]  T. N. Khazanovich Theory of nuclear magnetic relaxation in liquid-phase polymers☆ , 1963 .

[50]  R. Kimmich,et al.  The twice-renormalized Rouse formalism of polymer dynamics: Segment diffusion, terminal relaxation, and nuclear spin-lattice relaxation , 2000 .

[51]  R. Bryant,et al.  Translational diffusion of liquids at surfaces of microporous materials: Theoretical analysis of field-cycling magnetic relaxation measurements , 1997 .

[52]  E. Anoardo,et al.  Local molecular order in the biaxial smectic mesophase of HpAB:A proton−14N cross relaxation study , 1997 .

[53]  H. Zimmermann,et al.  NMR field−cycling study of proton and deuteron spin relaxation in the nematic liquid crystal 4−n−pentyl−4'−cyanobiphenyl , 1993 .

[54]  S. Dvinskikh,et al.  A field-cycling NMR study of nematic 4-pentyl-4′-cyanobiphenyl confined in porous glasses , 1998 .

[55]  F. Noack,et al.  N.M.R. study of collective molecular motions in smectogen liquid crystals , 1989 .

[56]  R. Kimmich Dynamic processes in aqueous protein systems. Molecular theory and NMR relaxation , 1990 .

[57]  W. Weiss,et al.  Relaxation dispersion and zero-field spectroscopy of thermotropic and lyotropic liquid crystals by fast field-cycling N.M.R. , 1988 .

[58]  R. Kimmich,et al.  Enhancement of order fluctuations in a nematic liquid crystal by sonication , 2002 .

[59]  J. Litster,et al.  Light-Scattering Studies of Liquid Crystals , 1979 .

[60]  Jean-Pierre Korb,et al.  The physical basis for the magnetic field dependence of proton spin-lattice relaxation rates in proteins , 2001 .

[61]  Rainer Kimmich,et al.  Strange kinetics, porous media, and NMR , 2002 .

[62]  S. Rast,et al.  Theories of structural and dynamic properties of ions in discrete solvents. Application to magnetic resonance imaging , 2001 .

[63]  S. Stapf,et al.  TRANSLATIONAL VERSUS ROTATIONAL MOLECULAR DYNAMICS IN PLASTIC CRYSTALS STUDIED BY NMR RELAXOMETRY AND DIFFUSOMETRY , 1997 .

[64]  G. Schnur,et al.  Spin-lattice relaxation and lineshape parameters in nuclear magnetic resonance of lamellar lipid systems: Fluctuation spectroscopy of disordering mechanisms , 1983 .

[65]  J. Voitländer,et al.  Pulsed EPR with Field Cycling and a Bridged Loop–Gap Resonator Made by Chemical Deposition of Silver , 1997 .

[66]  D. Montgomery The generation of high magnetic fields , 1963 .

[67]  M. Möller,et al.  Field-Cycling NMR Relaxation Spectroscopy of Poly(di-n-alkylsiloxanes) in Solid, Mesomorphic Liquid, and Isotropic Liquid Phases , 1994 .

[68]  Nuclear magnetic resonance spectrometer with a frequency range extended below the megahertz region , 2000 .

[69]  Sergey Petryakov,et al.  Development of a PEDRI free‐radical imager using a 0.38 T clinical MRI system , 2002, Magnetic resonance in medicine.

[70]  C. A. Sholl Nuclear spin relaxation by translational diffusion in liquids and solids: high- and low-frequency limits , 1981 .

[71]  M. Möller,et al.  Intra- and inter-chain fluctuations in entangled polymer melts in bulk and confined to pore channels , 1999 .

[72]  J. W. Emsley,et al.  Nuclear magnetic resonance of liquid crystals , 1984 .

[73]  C. Slichter,et al.  Nuclear spin relaxation in normal and superconducting aluminum , 1959 .

[74]  I. Bertini,et al.  Application of NMRD to hydration of rubredoxin and a variant containing a (Cys-S)3FeIII(OH) site. , 2003, Biophysical journal.

[75]  J. Freed Stochastic‐molecular theory of spin–relaxation for liquid crystals , 1977 .

[76]  W. H. Jeu,et al.  Thermotropic Liquid Crystals, Fundamentals , 1988 .

[77]  A. Redfield,et al.  Field-cycling method with central transition readout for pure quadrupole resonance detection in dilute systems. , 2004, Journal of magnetic resonance.

[78]  R. Kimmich Reorientation mediated by translational diffusion as a mechanism for nuclear magnetic relaxation of molecules confined in surface layers , 1991 .

[79]  Jean Jeener,et al.  Nuclear Magnetic Resonance in Solids: Thermodynamic Effects of a Pair of rf Pulses , 1967 .

[80]  M. Huggins Viscoelastic Properties of Polymers. , 1961 .

[81]  Warner Fite,et al.  Precision High Speed Current Regulators for Occasionally Switched Inductive Loads , 1968 .

[82]  E. Anoardo,et al.  Fast-field-cycling NMR: Applications and instrumentation , 2001 .

[83]  R. Kimmich,et al.  Chain fluctuations in the amorphous regions of polyethylene as indicated in proton relaxation spectroscopy , 1980 .

[84]  E. Montroll,et al.  Fractal random walks , 1982 .

[85]  John C. Lindon,et al.  Encyclopedia of spectroscopy and spectrometry , 2000 .

[86]  S. Laurent,et al.  A multinuclear MR study of Gd‐EOB‐DTPA: Comprehensive preclinical characterization of an organ specific MRI contrast agent , 1997, Magnetic resonance in medicine.

[87]  S. Stapf,et al.  Molecular dynamics in confined monomolecular layers. A field-cycling nuclear magnetic resonance relaxometry study of liquids in porous glass , 1995 .

[88]  D. I. Hoult,et al.  The NMR receiver: A description and analysis of design , 1978 .

[89]  G. Crawford,et al.  NUCLEAR MAGNETIC RESONANCE FIELD-CYCLING PROTON RELAXATION STUDY OF POLYMER DISPERSED LIQUID CRYSTALS , 1996 .

[90]  S. H. Koenig,et al.  A unified view of relaxation in protein solutions and tissue, including hydration and magnetization transfer , 1993, Magnetic resonance in medicine.

[91]  M. Shlesinger,et al.  Beyond Brownian motion , 1996 .

[92]  Martin Blanz,et al.  A fast field-cycling NMR/NQR spectrometer , 1993 .

[93]  J. Kowalewski,et al.  Nuclear spin relaxation in paramagnetic systems with zero-field splitting and arbitrary electron spinElectronic Supplementary Information available. See http://www.rsc.org/suppdata/cp/b1/b106659p/ , 2001 .

[94]  R. Kimmich,et al.  Apparent low-field spin-lattice dispersion in the smectic-A mesophase of thermotropic cyanobiphenyls. , 2003, Physical review. E, Statistical, nonlinear, and soft matter physics.

[95]  S. Žumer,et al.  Theory of nuclear spin relaxation by translational self-diffusion in liquid crystals: Nematic phase , 1978 .

[96]  L. Nordenskiöld,et al.  Theory of nuclear spin relaxation in paramagnetic systems in solution , 1985 .

[97]  W. H. Toliver,et al.  Liquid Crystals , 1912, Nature.

[98]  M. Howard,et al.  Studies on the origin of sonically induced narrowing of solid-state nuclear magnetic resonance spectra , 1993 .

[99]  Charles S. Johnson,et al.  Diffusion-Ordered 2D NMR in the Fringe Field of a Superconducting Magnet , 1995 .

[100]  Nuclear magnetic resonance study of the vapor phase contribution to diffusion in nanoporous glasses partially filled with water and cyclohexane , 2003 .

[101]  I. Bertini,et al.  Nuclear and Electron Relaxation: The Magnetic Nucleus-Unpaired Electron Coupling in Solution , 1991 .

[102]  P. Pincus Nuclear relaxation in a nematic liquid crystal , 1969 .

[103]  Corrected equations for susceptibility-induced T2-shortening. , 1999, Journal of magnetic resonance.

[104]  J. Hennel,et al.  Proton Magnetic Relaxation and Protein Hydration , 1963, Nature.

[105]  F. Bitter Water Cooled Magnets , 1962 .

[106]  A. Pines,et al.  Zero field NMR and NQR with selective pulses and indirect detection , 1985 .

[107]  R. Porter,et al.  THE RHEOLOGY OF LIQUID CRYSTALS , 1967 .

[108]  G. R. Luckhurst,et al.  The Molecular Dynamics of Liquid Crystals , 1994 .

[109]  R. T. Schumacher Dynamics of Interacting Spin Systems , 1958 .

[110]  G. Schnur,et al.  Fluctuations, exchange processes, and water diffusion in aqueous protein systems: A study of bovine serum albumin by diverse NMR techniques. , 1990, Biophysical journal.

[111]  B. Santo,et al.  Solid State , 2012 .

[112]  L. Banci Nuclear and electron relaxation , 1991 .

[113]  T. Margulies,et al.  Attenuation and Dispersion of Acoustic Waves in Nematic Liquid Crystals , 1988 .

[114]  R. Blinc,et al.  13C N.M.R. and 14N N.Q.R. in ferroelectric liquid crystals Polar versus quadrupolar ordering , 1988 .

[115]  R. Kimmich,et al.  Chain dynamics in entangled polymers: Power laws of the proton and deuteron spin-lattice relaxation dispersions , 1998 .

[116]  Kenneth S. Schweizer,et al.  Microscopic theory of the dynamics of polymeric liquids: General formulation of a mode–mode‐coupling approach , 1989 .

[117]  Enzo Terreno,et al.  Lanthanide(III) chelates for NMR biomedical applications , 1998 .

[118]  R. Ullman Nuclear Magnetic Relaxation of Polymer Solutions , 1965 .

[119]  Robert B. Meyer,et al.  Piezoelectric Effects in Liquid Crystals , 1969 .

[120]  E. Anoardo,et al.  Spin-lattice dispersion in nematic and smectic-A mesophases in the presence of ultrasonic waves: a theoretical approach. , 2003, Physical review. E, Statistical, nonlinear, and soft matter physics.

[121]  W. J. A. Goossens,et al.  Bulk, Interfacial and Anchoring Energies of Liquid Crystals , 1985 .

[122]  R. Kimmich,et al.  Geometrical Restrictions of Incoherent Transport of Water by Diffusion in Protein of Silica Fineparticle Systems and by Flow in a Sponge. A Study of Anomalous Properties Using an NMR Field-Gradient Technique , 1992 .

[123]  R. Kimmich,et al.  Spin lattice relaxation of dipole nuclei (I = 1/2) coupled to quadrupole nuclei (S = 1) , 1982 .

[124]  E. Rommel,et al.  A powerful NMR field-cycling device using GTOs and MOSFETs for relaxation dispersion and zero-field studies , 1986 .

[125]  G. Pake,et al.  The physical principles of electron paramagnetic resonance , 1973 .

[126]  S. Burgard ISR , 1999 .

[127]  R. Davies Spin-Temperature and Nuclear-Spin Relaxation in Matter , 1980 .

[128]  Shen,et al.  Surface memory effect at the liquid-crystal-polymer interface. , 1992, Physical review letters.

[129]  F. Grinberg,et al.  Pore size dependence of the dipolar‐correlation effect on the stimulated echo in liquid crystals confined in porous glass , 1996 .

[130]  E. Khozina,et al.  Self-diffusion in fluids in porous glass: confinement by pores and liquid adsorption layers. , 1996, Magnetic resonance imaging.

[131]  W. H. Jeu,et al.  MOLECULAR-STRUCTURE AND ELASTIC-CONSTANTS OF NEMATIC LIQUID-CRYSTALS , 1979 .

[132]  O. Bychuk,et al.  Anomalous surface diffusion: A numerical study , 1994 .

[133]  F. Noack,et al.  NMR field-cycling spectroscopy: principles and a]lications , 1986 .

[134]  W. Węglarz,et al.  Observation of Coupling Across the Ice Water Interface by 2D Time Domain NMR , 1997 .

[135]  D Melville,et al.  Solenoid Magnet Design , 1970 .

[136]  R. Kimmich,et al.  Nuclear spin‐lattice relaxation dispersion and segment diffusion in entangled polymers. Renormalized Rouse formalism , 1994 .

[137]  R. Kimmich,et al.  Protein backbone fluctuations and NMR field-cycling relaxation spectroscopy , 1990 .

[138]  R. Kimmich,et al.  14N1H and 2H1H cross-relaxation in hydrated proteins. , 1985, Biophysical journal.

[139]  Andrew G. Glen,et al.  APPL , 2001 .

[140]  Structure and polymorphism of the hydrocarbon chains of lipids: a study of lecithin-water phases. , 1973 .

[141]  C. Gähwiller The viscosity coefficients of a room-temperature liquid crystal (MBBA) , 1971 .

[142]  M. J. Bradshaw,et al.  The Elastic Constants and Electric Permittivities of Mixtures Containing Terminally Cyano Substituted Nematogens , 1983 .

[143]  Rainer Kimmich,et al.  Nuclear magnetic relaxation dispersion in lecithin bilayers , 1979 .

[144]  S. Kiihne,et al.  Protein-bound water molecule counting by resolution of (1)H spin-lattice relaxation mechanisms. , 2000, Biophysical journal.

[145]  Miss A.O. Penney (b) , 1974, The New Yale Book of Quotations.

[146]  S. Jurga,et al.  Studies of gelation process investigated by fast field cycling relaxometry and dynamical rheology: the case of aqueous low methoxyl pectin solution. , 2004, Solid state nuclear magnetic resonance.

[147]  R. Vold,et al.  Nuclear spin relaxation and quasicoherent fluctuations in ordered fluids: A different expression for the high‐frequency cutoff , 1988 .

[148]  S. F. Lienin,et al.  Efficient scalar spin relaxation in the rotating frame for matched radio-frequency fields , 1998 .

[149]  A. Pines,et al.  Zero-field nuclear magnetic resonance , 1983 .

[150]  D. Dunmur,et al.  Physical Properties of Liquid Crystals , 2002 .

[151]  R. Valiullin,et al.  Lévy walks of strong adsorbates on surfaces: Computer simulation and spin-lattice relaxation , 1997 .

[152]  K. H Schweikert,et al.  A high-field air-cored magnet coil design for fast-field-cycling NMR , 1988 .

[153]  D. Johnson,et al.  Spin-lattice relaxation in the nematic liquid crystalline phase , 1970 .

[154]  R. Kimmich,et al.  Double-diffuisve fluctuations and the v 3/4 -law of proton spin-lattice relaxation in biopolymers , 1985 .

[155]  J. Visintainer,et al.  Proton Spin-Lattice Relaxation in Liquid Crystals , 1969 .

[156]  S. Stapf,et al.  Field-Cycling Nuclear Magnetic Resonance Relaxometry and Field-Gradient Nuclear Magnetic Resonance Diffusometry of Polymers Confined in Porous Glasses: Evidence for a Restricted-Geometry Effect , 1996 .

[157]  J. Blackman,et al.  Solid state , 1974, Nature.

[158]  A. J. Horsewill Quantum tunnelling aspects of methyl group rotation studied by NMR , 1999 .

[159]  R. Kimmich,et al.  In vivo NMR field-cycling relaxation spectroscopy reveals 14N1H relaxation sinks in the backbones of proteins. , 1984, Physics in medicine and biology.

[160]  R. Kimmich,et al.  Nuclear magnetic relaxation spectroscopy of polymers and anomalous segment diffusion. Reorientations mediated by translational displacements , 1993 .

[161]  P. Levitz,et al.  Probing the Morphology of Laponite Clay Colloids by Atomic Force Microscopy , 2003 .

[162]  A. Redfield Shuttling device for high‐resolution measurements of relaxation and related phenomena in solution at low field, using a shared commercial 500 MHz NMR instrument , 2003 .

[163]  F. Casanova,et al.  Intramolecular character of the intrapair dipolar order relaxation in the methyl deuterated nematic para-azoxyanisole , 2002 .

[164]  Weber,et al.  NMR relaxation and the orientational structure factor. , 1993, Physical review. B, Condensed matter.

[165]  D. Kerwood,et al.  A sample-shuttling device suitable for two-dimensional low-field NMR , 1987 .

[166]  S. Nagai,et al.  Ultrasonic investigation of nematic liquid crystals in the isotropic and nematic phases , 1976 .

[167]  R. Blinc,et al.  Mechanisms for spin-lattice relaxation in nematic liquid crystals , 1972 .

[168]  R. Kimmich,et al.  NMR study of diffusion in protein hydration shells , 1990 .

[169]  R. Blinc,et al.  Angular dependence of the proton spin-spin and spin-lattice relaxation in nematic MBBA-EBBA mixtures , 1976 .

[170]  A. Darke,et al.  Nuclear relaxation (T1) measurements of lecithin-water systems , 1971 .

[171]  K. Okano,et al.  Theory of anomalous ultrasonic absorption and dispersion of nematic liquid crystals just above the clearing point , 1973 .

[172]  Ericka Stricklin-Parker,et al.  Ann , 2005 .

[173]  G. Shipley,et al.  Temperature and compositional dependence of the structure of hydrated dimyristoyl lecithin. , 1979, The Journal of biological chemistry.

[174]  H. C. Torrey Nuclear Spin Relaxation by Translational Diffusion , 1953 .

[175]  H. Yokoyama Surface Anchoring of Nematic Liquid Crystals , 1988 .

[176]  Martin Möller,et al.  Segment diffusion in polymers confined in nanopores: A fringe-field NMR diffusometry study , 1999 .

[177]  R. Kimmich,et al.  Interactions and Fluctuations Deduced from Proton Field-Cycling Relaxation Spectroscopy of Polypeptides, DNA, Muscles, and Algae , 1986 .

[178]  P. Sheng,et al.  Introduction to Liquid Crystals , 1976 .

[179]  R. Kimmich,et al.  Deuteron field-cycling relaxation spectroscopy and translational water diffusion in protein hydration shells. , 1988, Biophysical journal.

[180]  F. Grinberg,et al.  Proton spin-lattice relaxation in a liquid crystal-Aerosil complex above the bulk isotropization temperature , 2004 .

[181]  Constantin Job,et al.  Fast field‐cycling nuclear magnetic resonance spectrometer , 1996 .

[182]  F. Grinberg,et al.  Order fluctuations in the mesophase of polydiethylsiloxane as studied by the dipolar‐correlation effect on the stimulated echo , 1996 .

[183]  S. Meiboom,et al.  Nuclear magnetic resonance in liquid crystals. , 1968, Science.

[184]  T F Nonnenmacher,et al.  Propagator representation of anomalous diffusion: the orientational structure factor formalism in NMR. , 1999, Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics.

[185]  G. Fredrickson The theory of polymer dynamics , 1996 .

[186]  R. Blinc,et al.  Spin Relaxation and Self-Diffusion in Liquid Crystals , 1969 .

[187]  P. Gennes Reptation of a Polymer Chain in the Presence of Fixed Obstacles , 1971 .

[188]  Weber,et al.  Spin-lattice relaxation of polymers: The memory-function formalism. , 1993, Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics.

[189]  I. Kuntz,et al.  Rotating frame spin-lattice relaxation in the presence of an off-resonance radio frequency field. Investigation of intermediate molecular motions , 1977 .

[190]  S. Dvinskikh,et al.  Magnet design with high B(0) homogeneity for fast-field-cycling NMR applications. , 2001, Journal of magnetic resonance.

[191]  R. Kimmich,et al.  Segment diffusion and nuclear magnetic resonance spin-lattice relaxation of polymer chains confined in tubes: Analytical treatment and Monte Carlo simulation of the crossover from Rouse to reptation dynamics , 2002 .

[192]  R. Kimmich,et al.  Anomalous segment diffusion in polymers and NMR relaxation spectroscopy , 1993 .

[193]  R. Kimmich,et al.  Molecular theory for nuclear magnetic relaxation in protein solutions and tissue: Surface diffusion and free-volume analogy , 1990 .

[194]  O. Bychuk,et al.  Anomalous diffusion of surface-active species at liquid-fluid and liquid-solid interfaces , 1994 .

[195]  D. Look,et al.  Nuclear Magnetic Dipole—Dipole Relaxation Along the Static and Rotating Magnetic Fields: Application to Gypsum , 1966 .

[196]  P. Meier,et al.  Proton spin relaxation dispersion studies of phospholipid membranes , 1988 .

[197]  H. Grubin The physics of semiconductor devices , 1979, IEEE Journal of Quantum Electronics.

[198]  G. R. Luckhurst,et al.  The Molecular physics of liquid crystals , 1979 .

[199]  Jean-Pierre Korb,et al.  Magnetic field dependence of proton spin‐lattice relaxation times , 2002, Magnetic resonance in medicine.

[200]  R. Kimmich,et al.  Low-frequency molecular dynamics studied by spin-lock field cycling imaging. , 2000, Journal of magnetic resonance.

[201]  R. Kimmich,et al.  NMR field-cycling relaxation spectroscopy, transverse NMR relaxation, self-diffusion and zero-shear viscosity: Defect diffusion and reptation in non-glassy amorphous polymers , 1982 .

[202]  P. E. Rouse A Theory of the Linear Viscoelastic Properties of Dilute Solutions of Coiling Polymers , 1953 .

[203]  R. Kimmich,et al.  Geometrical restrictions of water diffusion in aqueous protein systems. A study using NMR field-gradient techniques , 1993 .

[204]  G. Jones Spin-Lattice Relaxation in the Rotating Frame: Weak-Collision Case , 1966 .

[205]  J M Hutchison,et al.  Design, construction and use of a large-sample field-cycled PEDRI imager , 1998 .

[206]  A. Genack,et al.  Theory of nuclear spin diffusion in a spatially varying magnetic field , 1975 .

[207]  M. Schadt,et al.  Synthesis, Physical Properties and Structural Relationships of New, End-Chain Substituted Nematic Liquid Crystals , 1987 .

[208]  F. Noack,et al.  Frequency dependent NMR spin relaxation studies of deuterons and protons in nematic liquid crystals , 1992 .

[209]  S. Žumer,et al.  Nuclear magnetic relaxation in small nematic droplets induced by molecular self‐diffusion , 1989 .

[210]  J. Grandjean Interaction of poly(ethylene glycol) monoalkyl ethers with synthetic saponites in aqueous suspensions : A multinuclear magnetic resonance-study , 1998 .

[211]  R. Kimmich,et al.  The anomalous adsorbate dynamics at surfaces in porous media studied by nuclear magnetic resonance methods. The orientational structure factor and Lévy walks , 1998 .

[212]  G. Schauer,et al.  NMR field cycling with a superconducting magnet , 1987 .

[213]  B. L. Willis,et al.  Condition for Sudden Passage in the Earth's-Field NMR Technique , 1995 .

[214]  G. Schnur,et al.  The tube concept of macromolecular liquids in the light of NMR experiments , 1988 .

[215]  P. Pershan Cross Relaxation in LiF , 1960 .

[216]  M. Vilfan,et al.  Molecular dynamics in tilted bilayer smectic phases: A proton nuclear magnetic resonance relaxometry study , 2001 .

[217]  P. Levitz,et al.  Slow dynamics of embedded fluid in mesoscopic confining systems as probed by NMR relaxometry , 2003, The European physical journal. E, Soft matter.

[218]  M. Muller,et al.  Field-cycling nuclear magnetic resonance relaxometry of thermoreversible polybutadiene networks , 1997 .

[219]  D. Suter,et al.  Radiofrequency-pulse excitation in time-domain zero field magnetic resonance , 1986 .

[220]  E. Burnell,et al.  NMR of ordered liquids , 2003 .

[221]  B. Halle,et al.  Magnetic relaxation dispersion studies of biomolecular solutions. , 2001, Methods in enzymology.

[222]  Stapf,et al.  Proton and deuteron field-cycling NMR relaxometry of liquids in porous glasses: Evidence for Lévy-walk statistics. , 1995, Physical review letters.

[223]  R. Lathe Phd by thesis , 1988, Nature.