A review of modern instrumental techniques for measurements of ice cream characteristics.

There is an increasing demand of the food industries and research institutes to have means of measurement allowing the characterization of foods. Ice cream, as a complex food system, consists of a frozen matrix containing air bubbles, fat globules, ice crystals, and an unfrozen serum phase. Some deficiencies in conventional methods for testing this product encourage the use of alternative techniques such as rheometry, spectroscopy, X-ray, electro-analytical techniques, ultrasound, and laser. Despite the development of novel instrumental applications in food science, use of some of them in ice cream testing is few, but has shown promising results. Developing the novel methods should increase our understanding of characteristics of ice cream and may allow online testing of the product. This review article discusses the potential of destructive and non-destructive methodologies in determining the quality and characteristics of ice cream and similar products.

[1]  S. Mortazavi,et al.  Study of Ice Cream Freezing process after Treatment with Ultrasound , 2008 .

[2]  Julien Andrieu,et al.  Experimental data and modelling of thermal properties of ice creams , 2003 .

[3]  P. Frisullo,et al.  Fat microstructure of yogurt as assessed by x-ray microtomography. , 2011, Journal of dairy science.

[4]  F. Mariette,et al.  NMR signal analysis to attribute the components to the solid/liquid phases present in mixes and ice creams. , 2005, Journal of agricultural and food chemistry.

[5]  C. Soukoulis,et al.  Enrichment of ice cream with dietary fibre: Effects on rheological properties, ice crystallisation and glass transition phenomena , 2009 .

[6]  H. Goff,et al.  STRUCTURAL DEVELOPMENT IN ICE CREAM—DYNAMIC RHEOLOGICAL MEASUREMENTS , 1995 .

[7]  Eric Dufour,et al.  A rapid method based on front-face fluorescence spectroscopy for the monitoring of the texture of meat emulsions and frankfurters. , 2004, Meat science.

[8]  Erich J. Windhab,et al.  Impact of disperse microstructure on rheology and quality aspects of ice cream , 2004 .

[9]  Chris Clarke,et al.  The Science of Ice Cream , 2005 .

[10]  E. Windhab,et al.  Air cell microstructuring in a high viscous ice cream matrix , 2005 .

[11]  D Matteuzzi,et al.  Detection of microbial concentration in ice-cream using the impedance technique. , 2008, Biosensors & bioelectronics.

[12]  E. J. Mann Ice cream. II , 1990 .

[13]  T. Ohshima,et al.  Identification and characterisation of headspace volatiles of fish miso, a Japanese fish meat based fermented paste, with special emphasis on effect of fish species and meat washing , 2010 .

[14]  C Granger,et al.  Short communication: impact of formulation on ice cream microstructures: an oscillation thermo-rheometry study. , 2004, Journal of dairy science.

[15]  J. Andrieu,et al.  Experimental study and modelling of the ice crystal morphology of model standard ice cream. Part I: Direct characterization method and experimental data , 2001 .

[16]  M. Lanzoni,et al.  Total Bacterial Count in Soft-Frozen Dairy Products by Impedance Biosensor System , 2009, IEEE Sensors Journal.

[17]  E. H. Marth,et al.  Update of the fourteenth edition of Standard Methods for the Examination of Dairy Products. , 2004 .

[18]  Mostafa Mazaheri Tehrani,et al.  Application and Functions of Stabilizers in Ice Cream , 2011 .

[19]  R. Hartel,et al.  Effect of Sweetener, Stabilizer, and Storage Temperature on Ice Recrystallization in Ice Cream , 1996 .

[20]  M. Cansell,et al.  Influence of formulation on the structural networks in ice cream , 2005 .

[21]  J. Toutain,et al.  Mapping of ice cream formulation using front-face fluorescence spectroscopy , 2006 .

[22]  D Matteuzzi,et al.  An embedded portable biosensor system for bacterial concentration detection. , 2010, Biosensors & bioelectronics.

[23]  Sandrine Rouimi,et al.  Foam stability and interfacial properties of milk protein–surfactant systems , 2005 .

[24]  M. Johns,et al.  Fast emulsion droplet sizing using NMR self-diffusion measurements. , 2004, Journal of colloid and interface science.

[25]  P. Fryer,et al.  A Novel Technique for Ice Crystal Visualization in Frozen Solids Using X‐Ray Micro‐Computed Tomography , 2005 .

[26]  M. Johns,et al.  Characterisation of emulsion systems using NMR and MRI , 2007 .

[27]  Josse De Baerdemaeker,et al.  A review of the analytical methods coupled with chemometric tools for the determination of the quality and identity of dairy products , 2007 .

[28]  M. M. Youssef,et al.  Applications of ultrasound in analysis, processing and quality control of food: A review , 2012 .

[29]  M. Lanzoni,et al.  Automatic ice-cream characterization by impedance measurements for optimal machine setting , 2012 .

[30]  S. Bolliger,et al.  Correlation between colloidal properties of ice cream mix and ice cream , 2000 .

[31]  Theodore P. Labuza,et al.  Evaluation of front-face fluorescence for assessing thermal processing of milk , 2006 .

[32]  Hanne Christine Bertram,et al.  Direct measurement of phase transitions in milk fat during cooling of cream—a low-field NMR approach , 2005 .

[33]  François Mariette,et al.  NMR assessment of ice cream: Effect of formulation on liquid and solid fat , 2005 .

[34]  Y. Vodovotz,et al.  Physical properties of ice cream containing milk protein concentrates. , 2005, Journal of dairy science.

[35]  A. Riaublanc,et al.  Potentiality of spectroscopic methods for the characterisation of dairy products. I. Front-face fluorescence study of raw, heated and homogenised milks , 1997 .

[36]  S. Lovatt,et al.  Additional thermal conductivity values of foods measured by a guarded hot plate , 1998 .

[37]  Michael C. Petty,et al.  Application of electrical admittance measurements to the quality control of milk , 2002 .

[38]  S. Bolliger,et al.  Relationships between ice cream mix viscoelasticity and ice crystal growth in ice cream. , 2000 .

[39]  Bruce Campbell,et al.  Evaluation of the precision of drop-size determination in oil/water emulsions by low-resolution NMR spectroscopy. , 2004, Langmuir : the ACS journal of surfaces and colloids.

[40]  François Mariette,et al.  Investigations of food colloids by NMR and MRI , 2009 .

[41]  D. Levieux,et al.  Front-face fluorescence spectroscopy allows the characterization of mild heat treatments applied to milk. Relations with the denaturation of milk proteins. , 2005, Journal of agricultural and food chemistry.

[42]  S. Ablett,et al.  Relationship between ice recrystallisation rates and the glass transition in frozen sugar solutions , 2002 .

[43]  Mikiya Muramatsu,et al.  Transient process in ice creams evaluated by laser speckles , 2010 .

[44]  Bruno Ricco,et al.  A novel technique to control ice cream freezing by electrical characteristics analysis , 2011 .

[45]  Syed S. H. Rizvi,et al.  Use of non-invasive X-ray microtomography for characterizing microstructure of extruded biopolymer foams , 2005 .

[46]  H. Heymann,et al.  Sensory and physical properties of ice creams containing milk fat or fat replacers. , 1998, Journal of dairy science.

[47]  H. Goff,et al.  Basil seed gum as a novel stabilizer for structure formation and reduction of ice recrystallization in ice cream , 2013 .

[48]  R. Pethig,et al.  Determining the fat content of milk and cream using AC conductivity measurements , 1993 .

[49]  G. Palleschi,et al.  14 – Rapid on-line analysis to ensure the safety of milk , 2003 .

[50]  K. Segall,et al.  A modified ice cream processing routine that promotes fat destabilization in the absence of added emulsifier , 2002 .

[51]  S. Razavi,et al.  Rheological Characterization and Sensory Evaluation of a Typical Soft Ice Cream Made with Selected Food Hydrocolloids , 2010, Food science and technology international = Ciencia y tecnologia de los alimentos internacional.

[52]  H. Goff,et al.  Phase separation in soft-serve ice cream mixes: rheology and microstructure , 2005 .

[53]  H. Goff,et al.  Serum separation in soft-serve ice cream mixes , 2004 .

[54]  S. Arntfield,et al.  Textural analysis of fat reduced vanilla ice cream products , 2001 .

[55]  F. Mariette,et al.  NMR assessment of mix and ice cream. Effect of formulation on liquid water and ice , 2005 .

[56]  J. Wold,et al.  Nondestructive measurement of light-induced oxidation in dairy products by fluorescence spectroscopy and imaging. , 2002, Journal of dairy science.

[57]  D. Wilson,et al.  An NMR study of the freezing of emulsion-containing drops. , 2004, Journal of colloid and interface science.

[58]  C. Javanaud,et al.  Applications of ultrasound to food systems , 1988 .

[59]  D. Mcclements,et al.  Influence of Flocculation on Optical Properties of Emulsions , 2001 .

[60]  S. Matsukawa,et al.  Relationship between Recrystallization Rate of Ice Crystals in Sugar Solutions and Water Mobility in Freeze-Concentrated Matrix , 2006 .

[61]  R. A. Flores,et al.  MECHANISMS OF ICE CRYSTALLIZATION AND RECRYSTALLIZATION IN ICE CREAM: A REVIEW , 2000 .

[62]  J. Toutain,et al.  Direct quantification of protein partitioning in oil-in-water emulsion by front-face fluorescence: avoiding the need for centrifugation. , 2005, Colloids and surfaces. B, Biointerfaces.

[63]  M. Cansell,et al.  Influence of formulation on the thermal behavior of ice cream mix and ice cream , 2005 .

[64]  S. Bolliger,et al.  In-line use of near infrared spectroscopy to measure structure parameters of frozen model sorbet , 1998 .

[65]  B. W. Tharp,et al.  Tharp and Young on Ice Cream: An Encyclopedic Guide to Ice Cream Science and Technology , 2012 .

[66]  D. Mcclements,et al.  Front-face fluorescence spectroscopy study of globular proteins in emulsions: influence of droplet flocculation. , 2003, Journal of agricultural and food chemistry.

[67]  B. Cindio,et al.  Characterisation of dairy emulsions by NMR and rheological techniques , 2009 .

[68]  C. Genot,et al.  Partition of Adsorbed and Nonadsorbed Bovine Serum Albumin in Dodecane-in-Water Emulsions Calculated from Front-Face Intrinsic Fluorescence Measurements , 1996 .

[69]  Laura Otero,et al.  Ice content and temperature determination from ultrasonic measurements in partially frozen foods , 2008 .

[70]  T. Higuchi,et al.  Three-dimensional measurement of ice crystals in frozen dilute solution , 2004 .

[71]  T. Hagiwara,et al.  Thermal, Mechanical, and Molecular Relaxation Properties of Frozen Sucrose and Fructose Solutions Containing Hydrocolloids , 2007 .