Fabrication of a New Electrochemical Sensor Based on Bimetal Oxide for the Detection of Furazolidone in Biological Samples

This study utilized a simple hydrothermal method to synthesize nickel molybdenum oxide (NMO) for the detection of furazolidone (FZE). Our synthesized NMO was characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), field emission scanning electron spectroscopy (FE-SEM), and energy dispersive X-ray spectroscopy (EDX). The cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used to detect the FZE. Under optimized conditions, the obtained results showed that the NMO had an excellent electrocatalytic property towards FZE. As a result, NMO/GCE showed a good linear range of 0.001–1765 µM, an excellent detection limit (LOD) of 0.02 µM, and sensitivity of 0.2042 µA µM−1 cm−2.

[1]  C. Bhuvaneswari,et al.  Nanoarchitecture and surface engineering strategy for the construction of 3D hierarchical CuS-rGO/g-C3N4 nanostructure: An ultrasensitive and highly selective electrochemical sensor for the detection of furazolidone drug , 2022, Journal of Electroanalytical Chemistry.

[2]  Shen-ming Chen,et al.  Ultrasensitive electrochemical detection of furazolidone in biological samples using 1D-2D BiVO4@MoS2 hierarchical nano-heterojunction composites armed electrodes. , 2021, Environmental research.

[3]  Shen-ming Chen,et al.  Simple sonochemical synthesis of flake-ball shaped bismuth vanadate for voltammetric detection of furazolidone , 2021, Journal of Alloys and Compounds.

[4]  Shen-ming Chen,et al.  Electrochemical sensor for detection of tryptophan in the milk sample based on MnWO4 nanoplates encapsulated RGO nanocomposite , 2021 .

[5]  Shen-ming Chen,et al.  Solvothermal Synthesis of Carbon incorporated MnS2 Spheres; High Sensing Performance towards the Detection of Furazolidone in Bio-Fluids , 2021 .

[6]  Shen-ming Chen,et al.  Highly Selective Electrochemical Sensor Based on Gadolinium Sulfide Rod-Embedded RGO for the Sensing of Carbofuran. , 2021, Journal of agricultural and food chemistry.

[7]  Sea-Fue Wang,et al.  Cobalt molybdate nanorods decorated on boron-doped graphitic carbon nitride sheets for electrochemical sensing of furazolidone , 2020, Microchimica Acta.

[8]  S. Ji,et al.  A high Faraday efficiency NiMoO4 nanosheet arrays catalyst by adjusting the hydrophilicity for overall water splitting. , 2020, Chemistry.

[9]  P. Subramanian,et al.  Hierarchical core-shell structured Ni3S2/NiMoO4 nanowires: a high-performance and reusable electrochemical sensor for glucose detection. , 2019, The Analyst.

[10]  S. Suthanthiraraj,et al.  Synthesis, Characterization, and Improvement of Supercapacitor Properties of NiMoO4 Nanocrystals with Polyaniline , 2019, Journal of Inorganic and Organometallic Polymers and Materials.

[11]  D. Dhakal,et al.  Rapid degradation of naproxen by AgBr-α-NiMoO4 composite photocatalyst in visible light: Mechanism and pathways , 2018, Chemical Engineering Journal.

[12]  S. Dadfarnia,et al.  Chemiluminescence determination of furazolidone in poultry tissues and water samples after selective solid phase microextraction using magnetic molecularly imprinted polymers , 2018 .

[13]  Jung Sang Cho,et al.  Scalable synthesis of NiMoO4 microspheres with numerous empty nanovoids as an advanced anode material for Li-ion batteries , 2018 .

[14]  Dingsheng Yuan,et al.  Facile synthesis of graphene@NiMoO4 nanosheet arrays on Ni foam for a high-performance asymmetric supercapacitor , 2017, Journal of Materials Science.

[15]  Baoshan He,et al.  A simple and sensitive electrochemical detection of furazolidone based on an Au nanoparticle functionalized graphene modified electrode , 2017 .

[16]  H. Rajak,et al.  Novel UV spectrophotometer methods for quantitative estimation of metronidazole and furazolidone using mixed hydrotropy solubilization , 2017 .

[17]  Victor Malgras,et al.  Synthesis and Characterization of α‐­NiMoO4 Nanorods for Supercapacitor ­Application , 2015 .

[18]  R. Halden,et al.  Does the Recent Growth of Aquaculture Create Antibiotic Resistance Threats Different from those Associated with Land Animal Production in Agriculture? , 2015, The AAPS Journal.

[19]  Q. Li,et al.  High performance NiMoO4 nanowires supported on carbon cloth as advanced electrodes for symmetric supercapacitors , 2014 .

[20]  B. Liu,et al.  Comparison of the electrochemical performance of NiMoO4 nanorods and hierarchical nanospheres for supercapacitor applications. , 2013, ACS applied materials & interfaces.

[21]  L. Rodziewicz.  Determination of nitrofuran metabolites in milk by liquid chromatography-electrospray ionization tandem mass spectrometry. , 2008, Journal of chromatography. B, Analytical technologies in the biomedical and life sciences.

[22]  G. R. Stehly,et al.  Liquid chromatographic determination of furazolidone in shrimp. , 1994, Journal of AOAC International.

[23]  Shen-ming Chen,et al.  Electrochemical investigation of zinc tungstate nanoparticles; a robust sensor platform for the selective detection of furazolidone in biological samples , 2021 .

[24]  M. Minakshi,et al.  Nano α-NiMoO4 as a new electrode for electrochemical supercapacitors , 2013 .