Stress-induced magnetic and structural anisotropy of nanocrystalline Fe-based alloys

The structural anisotropy of Fe–Si–B–Nb–Cu nanocrystalline alloys annealed under tensile stress was studied by x-ray diffraction techniques with transmission geometry. A clear difference was observed in the peak positions of the Fe–Si crystals under two different conditions: with the diffraction vector parallel or perpendicular to the applied stress. The strains calculated from the anisotropy of the peak positions show a linear response to the applied stress, independent of Si content, indicating that the observed structural anisotropy is due to a quenching of the elastic strain, not in the directional ordering of the Fe–Si pair. The induced magnetic anisotropy energy is well explained by the residual strains and their magnetostrictions.

[1]  A. Zhukov,et al.  Round table discussion: Present and future applications of nanocrystalline magnetic materials , 2005 .

[2]  Y. Yoshizawa,et al.  Induced Magnetic Anisotropy and Thickness Dependence of Magnetic Properties in Nanocrystalline Alloy "Finemet" , 1990, IEEE Translation Journal on Magnetics in Japan.

[3]  J. Petzold,et al.  Advantages of softmagnetic nanocrystalline materials for modern electronic applications , 2002 .

[4]  B. Hofmann,et al.  Stress-induced magnetic anisotropy in nanocrystalline FeCuNbSiB alloy , 1996 .

[5]  G. Herzer Creep induced magnetic anisotropy in nanocrystalline Fe-Cu-Nb-Si-B alloys , 1994 .

[6]  H. Fukunaga,et al.  Direct evidence for structural origin of stress-induced magnetic anisotropy in Fe–Si–B–Nb–Cu nanocrystalline alloys , 2003 .

[7]  G. Herzer Magnetic field induced anisotropy in nanocrystalline FeCuNbSiB alloys , 1994 .

[8]  Mark R. Daymond,et al.  Use of Rietveld refinement for elastic macrostrain determination and for evaluation of plastic strain history from diffraction spectra , 1997 .

[9]  Y. Yoshizawa,et al.  New Fe-based soft magnetic alloys composed of ultrafine grain structure , 1988 .

[10]  Masaki Nakano,et al.  Origin of the magnetic anisotropy induced by stress annealing in Fe-based nanocrystalline alloy , 2005 .

[11]  M. Nakano,et al.  Nanostructured soft magnetic material with low loss and low permeability , 2000 .

[12]  O. Heczko,et al.  Magnetic anisotropy in as-quenched and stress-annealed amorphous and nanocrystalline Fe73.5Cu1Nb3Si13.5B9 alloys , 1992 .

[13]  G. Herzer,et al.  Grain structure and magnetism of nanocrystalline ferromagnets , 1989, International Magnetics Conference.